Microstructure evolution in copper under severe plastic deformation detected by in situ X-ray diffraction using monochromatic synchrotron light

2009 ◽  
Vol 503 (1-2) ◽  
pp. 10-13 ◽  
Author(s):  
A.R. Kilmametov ◽  
G. Vaughan ◽  
A.R. Yavari ◽  
A. LeMoulec ◽  
W.J. Botta ◽  
...  
2016 ◽  
Vol 685 ◽  
pp. 525-529
Author(s):  
Zhanna G. Kovalevskaya ◽  
Margarita A. Khimich ◽  
Andrey V. Belyakov ◽  
Ivan A. Shulepov

The changes of the phase composition, structure and physicomechanical properties of Ti‑40 mas % Nb after severe plastic deformation are investigated in this paper. By the methods of microstructural, X-ray diffraction analysis and scanning electron microscopy it is determined that phase and structural transformations occur simultaneously in the alloy after severe plastic deformation. The martensitic structure formed after tempering disappears. The inverse α'' → β transformation occurs. The structure consisting of oriented refined grains is formed. The alloy is hardened due to the cold working. The Young modulus is equal to 79 GPa and it is less than that of initial alloy and close to the value obtained after tempering. It is possible that Young modulus is reduced by additional annealing.


2006 ◽  
Vol 114 ◽  
pp. 337-344 ◽  
Author(s):  
Bogusława Adamczyk-Cieślak ◽  
Jaroslaw Mizera ◽  
Krzysztof Jan Kurzydlowski

The texture of Al – 0.7 wt. % Li alloy processed by two different methods of severe plastic deformation (SPD) has been investigated by X-ray diffraction, and analyzed in terms of the orientation distribution function (ODF). It was found that severe plastic deformation by both Equal Channel Angular extrusion (ECAE) and Hydrostatic Extrusion (HE) resulted in an ultrafine grained structure in an Al – 0.7 wt. % Li alloy. The microstructure, grain shape and size, of materials produced by SPD strongly depend on the technological parameters and methods applied. The texture of the investigated alloy differed because of the different modes of deformation. In the initial state the alloy exhibited a very strong texture consisting of {111} fibre component. A similar fibrous texture characteristic was also found after HE whereas after the ECAE the initial texture was completely changed.


2016 ◽  
Vol 57 (9) ◽  
pp. 1447-1453 ◽  
Author(s):  
Hiroki Adachi ◽  
Yui Karamatsu ◽  
Shota Nakayama ◽  
Tomotaka Miyazawa ◽  
Masugu Sato ◽  
...  

2013 ◽  
Vol 333 ◽  
pp. 39-49 ◽  
Author(s):  
Jakub Čížek ◽  
František Lukáč ◽  
Marián Vlček ◽  
Martin Vlach ◽  
Ivan Procházka ◽  
...  

Hydrogen absorption and diffusivity in high quality ZnO crystals were investigated in this work by X-ray diffraction combined with slow positron implantation spectroscopy and electrical resistometry. ZnO crystals were covered by a thin Pd over-layer and electrochemically charged with hydrogen. It was found that absorbed hydrogen causes plastic deformation in a sub-surface region. The depth profile of hydrogen concentration introduced into the crystal was determined by nuclear reaction analysis. Enhanced hydrogen concentration was found in the sub-surface region due to excess hydrogen atoms trapped at defects introduced by plastic deformation. Hydrogen diffusion in ZnO crystals with various orientations was studied by in-situ electrical resistometry. It was found that hydrogen diffusion in the c-direction is faster than hydrogen diffusion in the a-direction most probably due to open channels existing in the wurtzite structure along the c-axis.


2008 ◽  
Vol 584-586 ◽  
pp. 655-660 ◽  
Author(s):  
Anton Hohenwarter ◽  
Richard Stock ◽  
Reinhard Pippan

Severe Plastic Deformation (SPD) is known to be an effective method of producing nanocrystalline materials, for instance by HPT and ECAP. These techniques are also capable of reproducing microstructures which arise naturally when high pressure and friction is involved, for example in wheel-rail contact problems. The resulting deformation layers build the origin point for fatigue cracks. For that reason the knowledge of the mechanical properties of these deformation layers are of vital importance. In the framework of this study a baintic rail steel quality was deformed by High Pressure Torsion up to distinctive equivalent strains at a nominal pressure of 6 GPa up to a final equivalent strain of 16. Afterwards the evolution of the resulting microstructure was investigated by Scanning Electron Microscopy, by microhardness measurements and X-ray diffraction. The bainitic structure showed a strong alignment and fragmentation into the shear direction with increasing strain, which was accompanied by an increase in hardness as well. X-ray diffraction measurements showed that the amount of retained austenite decreases dramatically after small amounts of strain, which indicates that retained austenite cannot be stabilized by high pressures. Torque measurements during deformation showed after strong hardening at the beginning, a saturation behaviour for higher strains, whereas for instance pearlitic rail steel qualities show further hardening.


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