Implication of initial grain size on DRX mechanism and grain refinement in super-304H SS in a wide range of strain rates during large-strain hot deformation

Author(s):  
K. Arun Babu ◽  
Yahya H. Mozumder ◽  
C.N. Athreya ◽  
V.Subramanya Sarma ◽  
Sumantra Mandal
2011 ◽  
Vol 690 ◽  
pp. 323-326 ◽  
Author(s):  
Lutz Krüger ◽  
Friederike Schwarz ◽  
Ulrich Martin ◽  
Hans Jørgen Roven

Three alloys of the magnesium AZ-series (AZ31, AZ61 and AZ91) were processed by multi-temperature equal channel angular pressing (ECAP) with five passes using route BC. The ECAP temperature was decreased from 275 °C to 250 °C during the process for better grain refinement. The mechanical behaviour was investigated over a wide range of strain rates (10-3s-1up to 103s-1) under compressive loading at room temperature. The investigations show that significant grain refinement takes place during the ECAP-process. The initial grain size of 12 μm, 9 μm and 5.8 μm for extruded AZ31, AZ61 and AZ91, respectively, could be refined to 2.5 μm. The grain refinement occurs by dynamic recrystallisation. Compared to extruded initial Mg-alloys, the yield stress increases slightly for all selected alloys after ECAP processing, while the amount of strain hardening decreases at the same time, due to reduced grain size and texture effects. Furthermore, the flow stress of extruded and ECAPed material is less affected by strain rates within a range of 10-3s-1to 10-1s-1.


Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1978 ◽  
Author(s):  
Xianqiang Fan ◽  
Zhipeng Guo ◽  
Xiaofeng Wang ◽  
Jie Yang ◽  
Jinwen Zou

A pre-hot-deformation process was applied for a polycrystalline nickel-base superalloy to active deformation twins and dislocations, and subsequent slow cooling treatment was used to achieve grain refinement and microstructure homogenization. The microstructural evolution of the alloy was investigated, and the corresponding underlying mechanism was discussed. It was found that twinning mainly occurred in large grains during pre-hot-deformation owing to the stress concentration surrounding the large grains. High density dislocations were found in large grains, and the dislocation density increased approaching the grain boundary. The average grain size was refined from 30 μm to 13 μm after slow cooling with a standard deviation of grain size decreasing from 10.8 to 2.8, indicating a homogeneous microstructure. The grain refinement and microstructure homogenization during cooling process could be achieved via (i) static recrystallization (SRX), (ii) interaction of twin tips and γ’ precipitates, and (iii) grain coarsening hindered by γ’ precipitates in grain boundaries.


2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Ramzi Othman

In several industrial applications, metallic structures are facing impact loads. Therefore, there is an important need for developing constitutive equations which take into account the strain rate sensitivity of their mechanical properties. The Johnson-Cook equation was widely used to model the strain rate sensitivity of metals. However, it implies that the yield and flow stresses are linearly increasing in terms of the logarithm of strain rate. This is only true up to a threshold strain rate. In this work, a three-constant constitutive equation, assuming an apparent activation volume which decreases as the strain rate increases, is applied here for some metals. It is shown that this equation fits well the experimental yield and flow stresses for a very wide range of strain rates, including quasi-static, high, and very high strain rates (from 10−5to 5 × 104 s−1). This is the first time that a constitutive equation is showed to be able to fit the yield stress over a so large strain rate range while using only three material constants.


Author(s):  
Maen Alkhader ◽  
Laurence Bodelot

High-strength low alloy steels (HSLA) have been designed to replace high-yield (HY) strength steels in naval applications involving impact loading as the latter, which contain more carbon, require complicated welding processes. The critical role of HSLA-100 steel requires achieving an accurate understanding of its behavior under dynamic loading. Accordingly, in this paper, we experimentally investigate its behavior, establish a model for its constitutive response at high-strain rates, and discuss its dynamic failure mode. The large strain and high-strain-rate mechanical constitutive behavior of high strength low alloy steel HSLA-100 is experimentally characterized over a wide range of strain rates, ranging from 10−3 s−1 to 104 s−1. The ability of HSLA-100 steel to store energy of cold work in adiabatic conditions is assessed through the direct measurement of the fraction of plastic energy converted into heat. The susceptibility of HSLA-100 steel to failure due to the formation and development of adiabatic shear bands (ASB) is investigated from two perspectives, the well-accepted failure strain criterion and the newly suggested plastic energy criterion [1]. Our experimental results show that HSLA-100 steel has apparent strain rate sensitivity at rates exceeding 3000 s−1 and has minimal ability to store energy of cold work at high deformation rate. In addition, both strain based and energy based failure criteria are effective in describing the propensity of HSLA-100 steel to dynamic failure (adiabatic shear band). Finally, we use the experimental results to determine constants for a Johnson-Cook model describing the constitutive response of HSLA-100. The implementation of this model in a commercial finite element code gives predictions capturing properly the observed experimental behavior. High-strain rate, thermomechanical processes, constitutive behavior, failure, finite elements, Kolsky bar, HSLA-100.


2008 ◽  
Vol 584-586 ◽  
pp. 203-208 ◽  
Author(s):  
Yulia Ivanisenko ◽  
Hans Jorg Fecht

We suggest a simple method to study the mechanical behaviour of nanocrystalline (nc) samples in compression-torsion mode. High applied pressure prevents the fracture of sample, and quantitative parameters of sample response during torsion test can be compared with developed microstructure. Here we present and discuss the results of systematic investigation of mechanical behaviour of nc Pd with a mean grain size of 12 nm in a wide range of shear strains (0<γ<200) and at strain rates γ& = 3 10-1 s-1 and 3 10-2 s-1. We show that in the studied shear strain range the notable changes in the microstructure, namely a strain induced grain growth occurs, and that controls the relevant deformation mechanisms. For lower strains when the grain size is still small enough, the plastic flow governs by twinning and probably grain boundary sliding. The flow stresses are lower as compared with the later stages of deformation, when the grain size becomes larger and deformation is controlled exceptionally by dislocation glide. Finally, a steady stage is achieved, when the grain size, dislocation density and flow stress are saturated.


2006 ◽  
Vol 509 ◽  
pp. 75-80 ◽  
Author(s):  
M.I. Cruz-Palacios ◽  
D. Hernández-Silva ◽  
L.A. Barrales-Mora ◽  
M.A. García-Bernal

In the present study the superplastic behavior of Al-6%Mg–0.5%Cu and Al–8%Mg– 0.5%Cu in a coarse grain size condition has been studied. The alloys are melted in an electrical furnace under argon atmosphere. The ingots (25 mm thick) are homogenized at 400 °C during 72 h and then rolled at 430 °C to a thickness of 5 mm. The mean grain size after rolling is 55 µm for the 6%Mg alloy and 61 µm for the 8%Mg alloy. Tensile test specimens are machined from the rolled plate in the rolling direction. Strain-rate-change tests at temperatures between 300 and 450 °C and strain rates between 1x10-4 and 1x10-1 s-1 are carried out to determine the strain rate sensitivity of the flow stress. Finally, elongation to failure tests are conducted at temperatures and strain rates where the alloys show a high strain rate sensitivity. Elongations higher than 390 % are obtained for the 8%Mg alloy. It is observed that the grip regions of the deformed samples show coarser grains than the regions near to the fracture surface. This means that grain refinement takes place during deformation, suggesting that the principal deformation mechanism is dislocation creep.


2017 ◽  
Author(s):  
Vladimir A. Skripnyak ◽  
Natalia V. Skripnyak ◽  
Evgeniya G. Skripnyak ◽  
Vladimir V. Skripnyak

2006 ◽  
Vol 503-504 ◽  
pp. 341-348 ◽  
Author(s):  
Krzysztof Jan Kurzydlowski

The paper describes hydrostatic extrusion (HE) as a method of grain refinement of metallic materials down to the nanometric scale. The main features of this method are: (a) large strain, (b) very high strain rates (even greater than 104 s-1), and (c) deformation homogeneity. HE offers also the opportunity of obtaining bulk materials in a variety of forms (rods and wires of complex cross-sections, small tubes). The study undertaken on 4 materials (aluminium, aluminium alloy, copper and titanium) has shown that significant grain refinement , down to nanometric scale in the case of titanium and aluminium alloy, occurred during HE processing. This grain refinement produces significantly improved mechanical properties. It has been found that HE offers good prospects for the production of nano-structured metals and alloys.


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