Structural and magnetic study of the Ti4+-doped barium hexaferrite ceramic samples: Theoretical and experimental results

2011 ◽  
Vol 406 (17) ◽  
pp. 3130-3136 ◽  
Author(s):  
P.A. Mariño-Castellanos ◽  
A.C. Moreno-Borges ◽  
G. Orozco-Melgar ◽  
J.A. García ◽  
E. Govea-Alcaide
1996 ◽  
Vol 430 ◽  
Author(s):  
Zhou Jian ◽  
Cheng Jiping ◽  
Tang Yuling ◽  
Qiu Jinyu

AbstractIn this paper, a resonant cavity method is developed and some experimental results for measuring dielectric constants of ceramic samples (e. g. Al2O3) under different sintering temperatures are reported. The experiments show that this method has higher precision and good prospects of in—line monitoring the high temperature dielectric constant in the process of raising the temperature of the samples. These results provide some scientific experimental basis for physical research of ceramic materials.


2013 ◽  
Vol 114 (24) ◽  
pp. 243910 ◽  
Author(s):  
A. M. Alsmadi ◽  
I. Bsoul ◽  
S. H. Mahmood ◽  
G. Alnawashi ◽  
K. Prokeš ◽  
...  

2021 ◽  
pp. 44-50
Author(s):  
V.I. Butenko ◽  
S.N. Dubniuk ◽  
A.F. Dyachenko ◽  
K.V. Pavlii ◽  
B.V. Zajtsev

Facility for the tribological characteristics studying of a metal – ceramics pair and parameters of ceramic samples irradiation on the helium ions linear accelerator with energies 0.12 and 4 MeV are resulted. Profiles of damageability and occurrence of target atoms along of helium ions range are calculated for the irradiated TiO2 and Al2O3. Sputtering ratios and dependence of the sputtered atoms quantity on samples thickness are received. Calculations on density change of the irradiated samples are made. Experimental results of a sliding friction factor measurement depending on cycle’s quantity, temperature and irradiation doses are presented. On the basis of microscopic researches and calculation data conclusions are drawn about irradiation influence on interacting pair’s tribological characteristics.


2000 ◽  
Vol 619 ◽  
Author(s):  
S.A. Oliver ◽  
I. Kozulin ◽  
N.E. Mcgruer ◽  
S.D. Yoon ◽  
C. Vittoria

ABSTRACTExperimental results are shown for the structural and stress behaviors of c-axis oriented barium hexaferrite films on c-plane sapphire (Al2O3) substrates as a function of oxygen growth pressure and film thickness. It is shown that films deposited at 20 mTorr crack and delaminate at thicknesses above 15 µm, but that evidence for these large stresses is not apparent in either substrate curvature measurements or distortion of the c-axis lattice constant for thinner films (< 2 µm). In contrast, films (< 4 µm) deposited at 300 mTorr show large substrate curvatures that relax with increasing film thickness, in tandem with the formation of first large outgrowths, and then polycrystalline grains as the original c-axis film texture is randomized. Correlations between these observations are made to explain the complex evolution of properties in these films.


1988 ◽  
Vol 102 ◽  
pp. 357-360
Author(s):  
J.C. Gauthier ◽  
J.P. Geindre ◽  
P. Monier ◽  
C. Chenais-Popovics ◽  
N. Tragin ◽  
...  

AbstractIn order to achieve a nickel-like X ray laser scheme we need a tool to determine the parameters which characterise the high-Z plasma. The aim of this work is to study gold laser plasmas and to compare experimental results to a collisional-radiative model which describes nickel-like ions. The electronic temperature and density are measured by the emission of an aluminium tracer. They are compared to the predictions of the nickel-like model for pure gold. The results show that the density and temperature can be estimated in a pure gold plasma.


Author(s):  
Y. Harada ◽  
T. Goto ◽  
H. Koike ◽  
T. Someya

Since phase contrasts of STEM images, that is, Fresnel diffraction fringes or lattice images, manifest themselves in field emission scanning microscopy, the mechanism for image formation in the STEM mode has been investigated and compared with that in CTEM mode, resulting in the theory of reciprocity. It reveals that contrast in STEM images exhibits the same properties as contrast in CTEM images. However, it appears that the validity of the reciprocity theory, especially on the details of phase contrast, has not yet been fully proven by the experiments. In this work, we shall investigate the phase contrast images obtained in both the STEM and CTEM modes of a field emission microscope (100kV), and evaluate the validity of the reciprocity theory by comparing the experimental results.


Author(s):  
A. Ourmazd ◽  
G.R. Booker ◽  
C.J. Humphreys

A (111) phosphorus-doped Si specimen, thinned to give a TEM foil of thickness ∼ 150nm, contained a dislocation network lying on the (111) plane. The dislocation lines were along the three <211> directions and their total Burgers vectors,ḇt, were of the type , each dislocation being of edge character. TEM examination under proper weak-beam conditions seemed initially to show the standard contrast behaviour for such dislocations, indicating some dislocation segments were undissociated (contrast A), while other segments were dissociated to give two Shockley partials separated by approximately 6nm (contrast B) . A more detailed examination, however, revealed that some segments exhibited a third and anomalous contrast behaviour (contrast C), interpreted here as being due to a new dissociation not previously reported. Experimental results obtained for a dislocation along [211] with for the six <220> type reflections using (g,5g) weak-beam conditions are summarised in the table below, together with the relevant values.


Author(s):  
Chung-kook Lee ◽  
Yolande Berta ◽  
Robert F. Speyer

Barium hexaferrite (BaFe12O19) is a promising candidate for high density magnetic recording media due to its superior magnetic properties. For particulate recording media, nano-sized single crystalline powders with a narrow size distribution are a primary application requirement. The glass-crystallization method is preferred because of the controllability of crystallization kinetics, hence, particle size and size distribution. A disadvantage of this method is the need to melt raw materials at high temperatures with non-reactive crucibles, e.g. platinum. However, in this work, we have shown that crystal growth of barium hexaferrite occurred during low temperature heat treatment of raw batches.


Author(s):  
Scott Lordi

Vicinal Si (001) surfaces are interesting because they are good substrates for the growth of III-V semiconductors. Spots in RHEED patterns from vicinal surfaces are split due to scattering from ordered step arrays and this splitting can be used to determine the misorientation angle, using kinematic arguments. Kinematic theory is generally regarded to be inadequate for the calculation of RHEED intensities; however, only a few dynamical RHEED simulations have been attempted for vicinal surfaces. The multislice formulation of Cowley and Moodie with a recently developed edge patching method was used to calculate RHEED patterns from vicinal Si (001) surfaces. The calculated patterns are qualitatively similar to published experimental results and the positions of the split spots quantitatively agree with kinematic calculations.RHEED patterns were calculated for unreconstructed (bulk terminated) Si (001) surfaces misoriented towards [110] ,with an energy of 15 keV, at an incident angle of 36.63 mrad ([004] bragg condition), and a beam azimuth of [110] (perpendicular to the step edges) and the incident beam pointed down the step staircase.


Author(s):  
J.G. Wen ◽  
K.K. Fung

Bi-based superconducting phases have been found to be members of a structural series represented by Bi2Sr2Can−1Cun−1On+4, n=1,2,3, and are referred to as 2201, 2212, 2223 phases. All these phases are incommensurate modulated structures. The super space groups are P2/b, NBbmb 2201, 2212 phases respectively. Pb-doped ceramic samples and single crystals and Y-doped single crystals have been studied by transmission electron microscopy.Modulated structures of all Bi-based superconducting phases are in b-c plane, therefore, it is the best way to determine modulated structure and c parameter in diffraction pattern. FIG. 1,2,3 show diffraction patterns of three kinds of modulations in Pb-doped ceramic samples. Energy dispersive X-ray analysis (EDAX) confirms the presence of Pb in the three modulated structures. Parameters c are 3 0.06, 38.29, 30.24Å, ie 2212, 2223, 2212 phases for FIG. 1,2,3 respectively. Their average space groups are all Bbmb.


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