Testing fire protective properties of intumescent coatings by in-line temperature measurements on a cone calorimeter

2010 ◽  
Vol 69 (4) ◽  
pp. 475-480 ◽  
Author(s):  
Zhidong Han ◽  
Alberto Fina ◽  
Giulio Malucelli ◽  
Giovanni Camino
Polymers ◽  
2020 ◽  
Vol 12 (4) ◽  
pp. 757 ◽  
Author(s):  
Abderrahman Aqlibous ◽  
Svetlana Tretsiakova-McNally ◽  
Talal Fateh

Flammability and combustion of softwood treated with intumescent coatings were studied in the present work. The formulations applied onto wood surfaces contained different ratios of industrial fillers, titanium dioxide TiO2 and aluminium trihydroxide Al(OH)3, and/or bio-fillers, eggshell and rice husk ash. Combustion behaviours of unprotected and protected wood samples have been examined with the aid of cone calorimetry performed under the varied levels of thermal flux ranging from 30 to 50 kW/m². The char residues obtained after the completion of cone calorimetry test at 40 kW/m² were analysed by the Raman spectroscopy. The fire protective properties of the studied coatings were strongly influenced by the nature of the fillers as well as by the intensity of thermal irradiance. The incorporation of bio-based fillers into the water-based intumescent formulations significantly improved fire resistance of wood substrates. For example, at 30 kW/m², the Effective Heat of Combustion was reduced by more than 40%, whilst the average Peak to Heat Release Rate had dropped from 193.2 to 150.3 kW/m² for the wood sample protected with the formulation incorporating two industrial and two bio-fillers. Moreover, an application of the studied coatings resulted in a notable reduction of the back surface temperature of the wood specimens.


Author(s):  
J. P. Feist ◽  
S. Karmaker Biswas ◽  
C. Pilgrim ◽  
P. Y. Sollazzo ◽  
S. Berthier

Temperature profiling of components in gas turbines is of increasing importance as engineers drive to increase firing temperatures and optimise component’s cooling requirements in order to increase efficiency and lower CO2 emissions. However, on-line temperature measurements and, particularly, temperature profiling are difficult, sometimes impossible, to perform due to inaccessibility of the components. A desirable alternative would be to record the exposure temperature in such a way that it can be determined later, off-line. The commercially available Thermal Paints are toxic in nature and come with a range of technical disadvantages such as subjective readout and limited durability. This paper proposes a novel alternative measurement technique which the authors call Thermal History Paints and Thermal History Coatings. These can be particularly useful in the design process, but further could provide benefits in the maintenance area where hotspots which occurred during operation can be detected during maintenance intervals when the engine is at ambient temperature. This novel temperature profiling technique uses optical active ions in a ceramic host material. When these ions are excited by light they start to phosphoresce. The host material undergoes irreversible changes when exposed to elevated temperatures and since these changes are on the atomic level they influence the phosphorescent properties such as the life time decay of the phosphorescence. The changes in phosphorescence can be related to temperature through calibration such that in-situ analysis will return the temperature experienced by the coating. A major benefit of this technique is in the automated interpretation of the coatings. An electronic instrument is used to measure the phosphorescence signal eliminating the need for a specialist interpreter and thus increasing readout speed. This paper reviews results from temperature measurements made with a water based paint for the temperature range 100°C to 800°C in controlled conditions. Repeatability of the tests and errors will be discussed. Further, some measurements are carried out using an electronic hand-held interrogation device which can scan a component surface and provide a spatial resolution of below 3mm. The instrument enables mobile measurements outside of laboratory conditions. Further a robust Thermal History Coating is introduced demonstrating the capability of the coating to withstand long term exposures. The coating is based on Thermal Barrier Coating architecture with a high temperature bondcoat and deposited using an air plasma spray process to manufacture a reliable long lasting coating. Such a coating could be employed over the life of the component to provide critical temperature information at regular maintenance intervals for example indicating hot spots on engine parts.


Fire Research ◽  
2019 ◽  
Vol 3 (1) ◽  
Author(s):  
Saket Singh ◽  
Sumit Shivani ◽  
Sudheer Siddapureddy ◽  
Siddini Venkatesh Prabhu

Accidental fire is a major concern in terms of safety of infrastructures and human lives. With the technological advancement, several novel methods are developed for minimizing the damages caused by the fire. One of the methods is to paint the base metals/ material with fire retardant coatings which can increase the lead time so that economic destruction and loss of human lives can be avoided. In this work, the performance of the intumescent coating (passive type fire retardant coatings) is studied with the help of cone calorimeter and open pool diesel fire as sources of heat. The transient temperature distribution for bare Stainless Steel 310 plate suggests that the cone calorimeter experiments alone cannot suffice for mimicking real life conditions. Comparison of the behavior of the available paints in cone calorimeter and open pool fire confirms that the performance of intumescent coatings in cone calorimeter is very different from that in open pool fire. The safe initial thickness of the intumescent coating is a function of heat release rate of the source. The effective thermal conductivity of the intumescent coatings is evaluated using one dimensional conduction heat equation with constant boundary temperature condition.


1995 ◽  
Vol 13 (8-9) ◽  
pp. 2123-2131
Author(s):  
C. Martinez-Vera ◽  
O. Galá-Domingo. ◽  
M. Vizcarra-Mendoza ◽  
R. Ruiz-Martinez

Sign in / Sign up

Export Citation Format

Share Document