Experimental investigation, modeling and scale-up of hydrophilic vapor permeation membranes: Separation of azeotropic dimethyl carbonate/methanol mixtures

2013 ◽  
Vol 118 ◽  
pp. 862-878 ◽  
Author(s):  
Johannes Holtbruegge ◽  
Matthias Wierschem ◽  
Simon Steinruecken ◽  
Dorothea Voss ◽  
Lubow Parhomenko ◽  
...  
2020 ◽  
Vol 32 (2) ◽  
pp. 113-136 ◽  
Author(s):  
Simeon Pesch ◽  
Rebecca Knopf ◽  
Anahita Radmehr ◽  
Claire B. Paris ◽  
Zachary M. Aman ◽  
...  

2014 ◽  
Vol 1048 ◽  
pp. 26-30 ◽  
Author(s):  
Xin Wang ◽  
Yuan Zhao ◽  
Hao Wang ◽  
Guang Ming Cai

Different spinnerets can be used to generate needleless electrospinning with the potential to scale up the production of nanofibers. However, the electrospinning performance, normally refers to the quality of the as-spun fiber and the production rate, is dramatically different from different spinnerets. This study focuses on the electric field of different spinnerets under the same experimental parameters so as to understand the key factors that affect the electrospinning performance of upward needleless electrospinning. Modeling analysis suggested that the electric field could be further concentrated by optimizing the geometry of spinneret. Experimental investigation on needleless electrospinning from different spinnerets proved that the electrospinning performance was improved greatly with the optimization of the electric field of spinneret. Understanding of the relationship between electric field and spinning performance would benefit the design and development of needleless electrospinning.


2018 ◽  
Vol 42 (8) ◽  
pp. 434-438
Author(s):  
Qifan Zhou ◽  
Fangyu Du ◽  
Yajie Shi ◽  
Wenqiang Liu ◽  
Dongdong Liu ◽  
...  

A practical four-step synthesis of pymetrozine is reported, starting from a green chemical dimethyl carbonate and using the key intermediate methyl (E)-1-(2-oxopropyl)-2-(pyridin-3-ylmethylene)hydrazine-1-carboxylate. The main advantages of the route include inexpensive starting materials, environmental friendliness, short synthetic route, easy-to-use synthetic method and acceptable overall yield. A scale-up experiment was carried out to provide pymetrozine with 99.84% purity in 53.2% total yield.


2016 ◽  
Vol 87 (3) ◽  
pp. 033902 ◽  
Author(s):  
Hyungchul Kim ◽  
Ankit Kumar Singh ◽  
Cheng-Yin Wang ◽  
Canek Fuentes-Hernandez ◽  
Bernard Kippelen ◽  
...  

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