Performance optimisation of glass fibre mat reinforced polypropylene composites using statistical experimental design

1997 ◽  
Vol 16 (5) ◽  
pp. 497-506 ◽  
Author(s):  
Nam-Jeong Lee ◽  
Jyongsik Jang
2011 ◽  
Vol 236-238 ◽  
pp. 2773-2779
Author(s):  
Ying Cao Xu ◽  
Zhi Biao Feng ◽  
Chun Hong Liu

A statistical experimental design to plastein synthesis which was catalyzed by transglutaminase, using the mixture of soy protein isolate(SPI) hydrolysate and whey protein isolate (WPI) hydrolysate, was investigated. Enzyme/Substrate(E/S:5-25U/g), pH(5-9) and temperature (35-65°C) were selected as major operating variables. To investigate the effects of variables to yield of plastein, the statistical experiment of Box-Behnken design(BBD) and Response Surface methodology(RSM) was employed. Regression analysis showed that the experiment data accorded with the predicted values obtained from quadratic regression equation in BBD with R-Squared of 0.9866 and F-value of 102.51. The optimum results estimated by BBD were as follows: E/S(19.5U/g), pH(6.8), and temperature(50.0°C), gave a maximum plastein yield of 54%. In the present experiment, the preliminary study on plastein functions such as foaming, emulsifying, were showed that plastein had a good biological function.


2015 ◽  
Vol 30 (7) ◽  
pp. 986-1002 ◽  
Author(s):  
MR Islam ◽  
A Gupta ◽  
M Rivai ◽  
MDH Beg

Composites were prepared from recycled polypropylene (RPP), oil palm empty fruit bunch (EFB) and/or glass fibre (GF) using extrusion and injection moulding techniques. Two types of maleic anhydride-grafted polypropylene such as Polybond 3200 and Fusabond P 613 were used to improve the interfacial adhesion between fibres and matrix. The EFB: GF ratio was fixed as 70:30 and fibre loading was considered as 40 wt%. Microwave was used to treat the EFB fibre, which was soaked in a fixed mass concentration (12.5%) of alkali solution at different temperatures (70, 80 and 90°C) for a fixed period of time (60 min) and for different times (60, 90 and 120 min) at a fixed temperature (90°C). A magnetron controller was developed to control the time and temperature accurately for the treatment of fibre. Various characterization techniques such as density, melt flow index, tensile, Izod impact, flexural, field-emission scanning electron microscopy and water uptake testing were performed for the composites. Besides, thermogravimetric analysis and differential scanning calorimetry were also used to evaluate the thermal and crystalline properties of the composites, respectively. Result analyses revealed that microwave-treated fibre-based composites showed improved mechanical and thermal properties. EFB fibres treated at 90°C for 90 min were found to be suitable for better reinforcement into the composite in terms of mechanical, thermal and crystalline properties. Moreover, onset degradation temperature and water absorption properties were also found to be changed apparently due to treatment.


2005 ◽  
Vol 51 (4) ◽  
pp. 222-228 ◽  
Author(s):  
Neetu Dahiya ◽  
Rupinder Tewari ◽  
Ram Prakash Tiwari ◽  
Gurinder Singh Hoondal

1971 ◽  
Vol 97 (4) ◽  
pp. 393-407
Author(s):  
Paul M. Berthouex ◽  
William G. Hunter

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