Microstructure and room temperature fracture toughness of Nbss/Nb5Si3 in situ composites

2001 ◽  
Vol 9 (9) ◽  
pp. 827-834 ◽  
Author(s):  
Won-Yong Kim ◽  
Hisao Tanaka ◽  
Akio Kasama ◽  
Shuji Hanada
1994 ◽  
Vol 364 ◽  
Author(s):  
B. P. Bewlay ◽  
M. R. Jackson ◽  
W. J. Reeder ◽  
H. A. Lipsitt

AbstractIn-situ composites based on binary Nb-Si alloys and consisting of a Nb solid solution with Nb3Si or Nb5Si3 have shown a promising combination of low temperature and high temperature mechanical properties. The environmental resistance and room temperature fracture toughness of these composites can be further enhanced by additions such as Ti, Hf, Cr, and Al. In the present study, ternary Nb-Ti-Si alloys were prepared by directional solidification to generate aligned two and three phase composites containing a Nb solid solution with Nb3Si and/or Nb5Si3. The present paper will describe microstructures, phase equilibria and fracture toughness of these composites. The improvement in the room temperature fracture toughness over binary Nb-Nb5Si3 composites is discussed.


2006 ◽  
Vol 306-308 ◽  
pp. 941-946
Author(s):  
Sheng Wu Wang ◽  
Tatsuo Tabaru ◽  
Hisatoshi Hirai ◽  
Hideto Ueno

Nb-base in-situ composites with the base composition of Nb-18Si-2HfC were prepared by conventional arc-melting. Their microstructures and mechanical properties, such as high-temperature strength and room temperature fracture toughness, were investigated to elucidate the effects of Re alloying. The in-situ composites predominantly have eutectic microstructures consisting of an Nb solid solution (NbSS) and Nb5Si3. The compressive strength increased with the increasing Re contents at 1470K and not at 1670 K. The strengthening effect observed at 1470 K is higher than that by W and Mo. Re alloying of about 2 % is valuable for improving both the high temperature strength and room temperature fracture toughness of Nb-18Si-2HfC base materials.


2012 ◽  
Vol 21 (1) ◽  
pp. 18-25 ◽  
Author(s):  
Jian-Fei Zhang ◽  
Jun Shen ◽  
Zhao Shang ◽  
Zhou-Rong Feng ◽  
Ling-Shui Wang ◽  
...  

2012 ◽  
Vol 1516 ◽  
pp. 255-260 ◽  
Author(s):  
G. Zhang ◽  
L. Hu ◽  
W. Hu ◽  
G. Gottstein ◽  
S. Bogner ◽  
...  

ABSTRACTMo fiber reinforced NiAl in-situ composites with a nominal composition Ni-43.8Al-9.5Mo (at.%) were produced by specially controlled directional solidification (DS) using a laboratory-scale Bridgman furnace equipped with a liquid metal cooling (LMC) device. In these composites, single crystalline Mo fibers were precipitated out through eutectic reaction and aligned parallel to the growth direction of the ingot. Mechanical properties, i.e. the creep resistance at high temperatures (HT, between 900 °C and 1200 °C) and the fracture toughness at room temperature (RT) of in-situ NiAl-Mo composites, were characterized by tensile creep (along the growth direction) and flexure (four-point bending, vertical to the growth direction) tests, respectively. In the current study, a steady creep rate of 10-6s-1 at 1100 °C under an initial applied tensile stress of 150MPa was measured. The flexure tests sustained a fracture toughness of 14.5 MPa·m1/2at room temperature. Compared to binary NiAl and other NiAl alloys, these properties showed a remarkably improvement in creep resistance at HT and fracture toughness at RT that makes this composite a potential candidate material for structural application at the temperatures above 1000 °C. The mechanisms responsible for the improvement of the mechanical properties in NiAl-Mo in-situ composites were discussed based on the investigation results.


2004 ◽  
Vol 449-452 ◽  
pp. 753-756 ◽  
Author(s):  
Wei Li ◽  
Hai Bo Yang ◽  
Ai Dang Shan ◽  
Jian Sheng Wu

Nb/Nb5Si3 in-situ composites are very attractive structural materials for these materials perform a good balance in mechanical properties, including a high strength at high temperature (>1373K) and reasonably high fracture toughness at room temperature. Metastable phase Nb3Si plays an important role in the properties of Nb/Nb5Si3 composites by affecting microstructure and volume fracture of ductile phase. In this paper, Nb-10Si-xMo and Nb-18Si-xMo (x=0,5,15) are prepared by arc melting and annealed at 1473K for 100h. Single edge-notched bending (SENB) test was used to study the fracture toughness of Nb-Si-Mo alloys. The stability of metastable phase is analyzed by XRD. The room temperature fracture toughness of Nb-10Si is 10.47MPa(m)1/2 and higher than that of binary Nb-18Si alloys at near-eutectic compositions. The addition of Mo improves the fracture toughness of as cast Nb-Si alloys from 4.1 MPa(m)1/2 to 9.9MPa(m)1/2 at near-eutectic compositions and decreases it from 10.47 MPa(m)1/2 to 8.8MPa(m)1/2 at hypoeutectic compositions.


2018 ◽  
Vol 59 (4) ◽  
pp. 518-527 ◽  
Author(s):  
Shunichi Nakayama ◽  
Nobuaki Sekido ◽  
Sojiro Uemura ◽  
Sadahiro Tsurekawa ◽  
Kyosuke Yoshimi

2015 ◽  
Vol 47 (3) ◽  
pp. 311-317 ◽  
Author(s):  
F. Wang ◽  
N. Fan ◽  
J. Zhu ◽  
H. Jiang

Al2O3/TiAl composites were successfully fabricated from powder mixtures of Ti, Al, TiO2, Cr2O3 and Nb2O5 by a hot-press-assisted exothermic dispersion method. The effect of the Cr2O3 and Nb2O5 addition on the microstructures and mechanical properties of Al2O3/TiAl composites was characterized. The results showed that the specimens are mainly composed of TiAl, Ti3Al, Al2O3, NbAl3 and Cr2Al. The Vicker-hardness and density of Al2O3/TiAl composites increase gradually with the increase of Nb2O5 content. When the Nb2O5 content was 6.54 wt %, the flexural strength and fracture toughness of the composites have a maximum values of 789.79 MPa and 9.69 MPa?m1/2, respectively. The improvement of mechanical properties is discussed in detail.


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