In-situ application of dc electric field on ferroelectric substances in an electron microscope
A technique of in-situ application of a dc electric field on a specimen in an electron microscope has been developed to directly observe dynamic phenomena due to the electric field. In the present technique a thickness of a specimen is so thin that a very high electric field can be applied; a few volt of the potential difference across the specimen of the order of 1000 Å thick gives a field as high as 105 V/cm. An additional field application electrode was incorporated not only in a specimen heating holder but also in a liquid helium cooling stage which had been constructed in our 1aboratory. Thus, the experiments could be performed in a wide temperature range of 13-1000K. Fig.la schematically depicts a specimen holder installed in the cooling stage. The detailed arrangement around a specimen is shown in Fig.1b. An electric potential is applied between electrodes of thin A1 films vacuum deposited on the both faces of the specimen.