Design of a high-pressure and high-temperature cell for operando X-ray absorption spectroscopy in heterogeneous catalysis
Keyword(s):
X Ray
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A new X-ray absorption cell dedicated to in situ and operando experiments in heterogeneous catalysis has been built and tested. It allows measurement of X-ray absorption spectroscopy (XAS) spectra in transmission mode under the flow of various gas mixtures at elevated temperatures (600°C) and pressures (50 bar). The working conditions are representative of phenomena that take place in fixed bed reactors.
2013 ◽
Vol 84
(11)
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pp. 113107
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2004 ◽
Vol 108
(24)
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pp. 8148-8152
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