One-Pot Synthesis and Large-Scale Production Strategies for Preparing Ultrafine Hard Magnetic Sm2Fe17N3 Nanoparticles

Author(s):  
Jimin Lee ◽  
Eun Jae Lee ◽  
Kangmo Koo ◽  
Min Kyu Kang ◽  
Han Sol Lee ◽  
...  
2019 ◽  
Vol 124 ◽  
pp. 838-845 ◽  
Author(s):  
Morgana Souza Marques ◽  
Κarine Modolon Zepon ◽  
Julia Maia Heckler ◽  
Fernando Dal Pont Morisso ◽  
Marcos Marques da Silva Paula ◽  
...  

2017 ◽  
Vol 21 (11) ◽  
pp. 1745-1751 ◽  
Author(s):  
Mohan Reddy Bodireddy ◽  
Kiran Krishnaiah ◽  
Prashanth Kumar Babu ◽  
Chaithanya Bitra ◽  
Madhusudana Rao Gajula ◽  
...  

2018 ◽  
Vol 15 (4) ◽  
pp. 572-575 ◽  
Author(s):  
Ponnusamy Kannan ◽  
Samuel I.D. Presley ◽  
Pallikondaperumal Shanmugasundaram ◽  
Nagapillai Prakash ◽  
Deivanayagam Easwaramoorthy

Aim and Objective: Itopride is a prokinetic agent used for treating conditions like non-ulcer dyspepsia. Itopride is administered as its hydrochloride salt. Trimethobenzamide is used for treating nausea and vomiting and administered as its hydrochloride salt. The aim is to develop a novel and environmental friendly method for large-scale production of itopride and trimethobenzamide. Materials and Methods: Itopride and trimethobenzamide can be prepared from a common intermediate 4- (dimethylaminoethoxy) benzyl amine. The intermediate is prepared from one pot synthesis using Phyrdroxybenzaldehye and zinc dust and further reaction of the intermediate with substituted methoxy benzoic acid along with boric acid and PEG gives itopride and trimethobenzamide. Results: The intermediate 4-(dimethylaminoethoxy) benzylamine is prepared by treating p-hydroxybenzaldehyde and 2-dimethylaminoethyl chloride. The aldehyde formed is treated with hydroxylamine hydrochloride. The intermediate is confirmed by NMR and the purity is analysed by HPLC. Conclusion: Both itopride and trimethobenzamide were successfully synthesized by this method. The developed method is environmental friendly, economical for large-scale production with good yield and purity.


2021 ◽  
Vol 20 (1) ◽  
Author(s):  
Zhijin Gong ◽  
Ge Yang ◽  
Chengchuan Che ◽  
Jinfeng Liu ◽  
Meiru Si ◽  
...  

AbstractRhamnolipids have recently attracted considerable attentions because of their excellent biosurfactant performance and potential applications in agriculture, environment, biomedicine, etc., but severe foaming causes the high cost of production, restraining their commercial production and applications. To reduce or eliminate the foaming, numerous explorations have been focused on foaming factors and fermentation strategies, but a systematic summary and discussion are still lacking. Additionally, although these studies have not broken through the bottleneck of foaming, they are conducive to understanding the foaming mechanism and developing more effective rhamnolipids production strategies. Therefore, this review focuses on the effects of fermentation components and control conditions on foaming behavior and fermentation strategies responded to the severe foaming in rhamnolipids fermentation and systematically summarizes 6 impact factors and 9 fermentation strategies. Furthermore, the potentialities of 9 fermentation strategies for large-scale production are discussed and some further strategies are suggested. We hope this review can further facilitate the understanding of foaming factors and fermentation strategies as well as conducive to developing the more effective large-scale production strategies to accelerate the commercial production process of rhamnolipids.


2011 ◽  
Vol 15 (6) ◽  
pp. 1382-1387 ◽  
Author(s):  
Navnath C. Niphade ◽  
Kunal M. Jagtap ◽  
Chandrashekhar T. Gaikawad ◽  
Madhukar N. Jachak ◽  
Vijayavitthal T. Mathad

2021 ◽  
Vol 25 ◽  
Author(s):  
Carmela G. Arena

: Aliphatic secondary and tertiary amines are widely used in the production of pharmaceuticals, agrochemicals, dyes, surfactants and rubber chemicals. Most traditional synthetic methods are often unsuitable for large-scale production due to poor selectivity, harsh reaction conditions and the cost of starting materials. In this context, hydroaminomethylation (HAM) is a very attractive catalytic process with high atom economy that starts from inexpensive reagents, such as alkenes. This review aims to provide an updated overview of hydroaminomethylation as a useful tool for synthesizing aliphatic secondary and tertiary amines. Therefore, the discussion will focus on both unsaturated starting compounds and the amines obtained by this one-pot reaction.


2021 ◽  
Author(s):  
M. K. Ravindra ◽  
Giriyapura Prabhukumara Darshan ◽  
D. R. Lavanya ◽  
K. M. Mahadevan ◽  
H. B. Premkumar ◽  
...  

Abstract Aggregation-induced emission based organic heterocyclic luminogens bearing conjugated electronic structure have paid much attention due to its excellent fluorescence in aggregation state. In this communication, novel conjugated blue light emitting imidazole molecule is synthesized by one pot multicomponent reaction route is reported for the first time. The prepared molecule exhibits a strong fluorescence in aggregation state have gain much attention owing to their unique properties, namely simple synthesis, high purity, inexpensive, eco-friendly, large scale production, high photostability, etc. By considering these advantages of the prepared luminogen, a new fluorescence based platform has been setup for in-situ visualization of latent fingerprints and its preservation by spray method followed by Poly(vinyl alcohol) masking. A clear and well defined fluorescence fingerprint images on variety of surfaces by revealing level 1–3 ridge characteristics upon ultraviolet 365 nm light are noticed. The dual nature of binding specificity as well as excellent fluorescence properties permits the visualization of latent fingerprints for longer durations (up to 365 days) with superior contrast, sensitivity, efficiency, selectivity and negligible background hindrance. We further fabricated unclonable invisible security ink and make it highly suitable for various printing modes on valuable goods for protection against forging. The developed labels are displaying uniform distribution of ink and exceptional stability under various atmospheric environments. The development of long preservative forensic information as well as invisible ink opens new avenue in advanced forensic and data security applications.


2016 ◽  
Vol 38 ◽  
pp. 73-85 ◽  
Author(s):  
Michael Löffler ◽  
Joana Danica Simen ◽  
Günter Jäger ◽  
Karin Schäferhoff ◽  
Andreas Freund ◽  
...  

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