A Cutting Edge Technology in Reological Studies of Thermal Processing of Polymers: Measuring Response to High Temperature Treatment using a High Pressure Cell

1996 ◽  
Vol 220 (1-3) ◽  
pp. 149-157 ◽  
Author(s):  
V.D. Blank ◽  
S.G. Buga ◽  
N.R. Serebryanaya ◽  
G.A. Dubitsky ◽  
S.N. Sulyanov ◽  
...  

1998 ◽  
Vol 547 ◽  
Author(s):  
J.-H. Park ◽  
P.M. Woodward ◽  
J.B. Parise ◽  
I. Lubomirsky ◽  
O. Stafsudd

AbstractA new perovskite was recovered from the high pressure-high temperature treatment of the α-TlSbO3 form of Na2SnTeO6 at 7 GPa and 950 °C for 30 minutes. Synchrotron x-ray powder diffraction data show the space group is P21/n with a=5.40361 (5), b=5.46152(5), c=7.69288(7) Å and ß=90.034(3)°. Using disk samples of both polymorphs, the dielectric properties were measured as a function of temperature. At ambient conditions, the perovskite form has a more than 1.5 fold enhancement in dielectric constant compared to the α-TlSbO3 form while the molar volume and the molecular polarizability decrease.


2011 ◽  
Vol 197-198 ◽  
pp. 499-502
Author(s):  
Zheng He Hua ◽  
Heng Zhang ◽  
Ju Peng

Superconducting SmFeAsO0.8F0.2 compound was successfully synthesized by high pressure high temperature treatment with pressure of 6 G Pa at 1400 °C for 2 hours. The X-ray diffraction pattern of the sample indicates the formation of the tetragonal ZrCuSiAs-type SmFeAsO0.8F0.2 with lattice parameters a=3.932 Å and c=8.490 Å. The electrical transport study shows that the sample has a rather high transition temperature Tc of about 52 K, and magnetic field effect on the resistance reveals a rather high upper critical field HC2 of about 65 T.


1998 ◽  
Vol 248 (5-6) ◽  
pp. 415-422 ◽  
Author(s):  
V.D. Blank ◽  
N.R. Serebryanaya ◽  
G.A. Dubitsky ◽  
S.G. Buga ◽  
V.N. Denisov ◽  
...  

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