scholarly journals Got LiZnP? Solution phase synthesis of filled tetrahedral semiconductors in the nanoregime

2016 ◽  
Vol 52 (17) ◽  
pp. 3497-3499 ◽  
Author(s):  
Miles A. White ◽  
Michelle J. Thompson ◽  
Gordon J. Miller ◽  
Javier Vela
Keyword(s):  
Low Temperature ◽  
Solution Phase ◽  
Phase Method ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Tetrahedral Semiconductors ◽  
Solution Phase Method

Nanocrystalline LiZnP was synthesized using a flexible low temperature solution phase method that is generally applicable to other Nowotny–Juza phases.

Advances in nanoscale alloys and intermetallics: low temperature solution chemistry synthesis and application in catalysis

2015 ◽  
Vol 44 (43) ◽  
pp. 18692-18717 ◽  
Author(s):  
Subhra Jana
Keyword(s):  
Low Temperature ◽  
Solution Chemistry ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Size And Shape ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Made In

Advances made in the synthesis of size and shape-tunable nanoscale alloys and intermetallics using the low-temperature solution-phase synthesis approaches have been discussed in this perspective, keeping a focus on the utility of these nanomaterials in understanding the catalysis.

Synthesis of Casein-Related Peptides and Phosphopeptides. I. Solution-Phase Synthesis and 13C N.M.R.-Spectroscopy of the N-α-Acetyl Octapeptide N-Methylamide Corresponding to Region 14-21 of Bovine β-Casein A2

1987 ◽  
Vol 40 (2) ◽  
pp. 257 ◽  
Author(s):  
JW Perich ◽  
PF Alewood ◽  
RB Johns
Keyword(s):  
Solution Phase ◽  
Phase Method ◽  
Peptide Fragments ◽  
Mixed Anhydride ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Coupling Procedure ◽  
Fragment Condensation ◽  
High Yields ◽  
Solution Phase Method

The octapeptide, Ac-Glu-Ser-Leu-Ser-Ser-Ser-Glu-Glu-NHMe (I), was synthesized by the solution-phase method by using the mixed anhydride coupling procedure for the fragment condensation of the Nα-acetyl tripeptide, Ac-Glu(OBut)-Ser(But)-Leu-OH, with the pentapeptide N-methylamide hydrochloride, Cl.H2-Ser(But)-Ser(But)-Ser(But)-Glu(OBzl)-Glu(OBzl)-NHMe, followed by palladium-catalysed hydrogenolysis of Ac-Glu(OBut)-Ser(But)-Leu-Ser(But)-Ser(But)- Ser(But) Glu(OBzl)Glu(OBzl NHMe in trifluoroacetic acid. The synthesis of the two peptide fragments was accomplished in high yields and purity by using the repetitive excess mixed anhydride procedure and the isobutoxycarbonyl mixed anhydride of acetic acid for the rapid and high yielding N-acetylation of the tripeptide fragment. 13C n.m.r. spectroscopy was routinely used to monitor the efficiency of the coupling steps and to confirm the structure of octapeptide (1), signal assignments being possible for both the protected tri- and penta-peptides.

Solvent-Dependent, Low-Temperature Solution Phase Synthesis of FePt Nanowires

2008 ◽  
Vol 8 (7) ◽  
pp. 3379-3385 ◽  
Author(s):  
Kai-Ming Chi ◽  
Pei-Yu Chen
Keyword(s):  
Thermal Decomposition ◽  
Low Temperature ◽  
Reaction Temperature ◽  
Average Diameter ◽  
Solution Phase ◽  
Synthetic Approach ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution

Preparation of FePt nanowires by thermal decomposition of the solution mixture of equimolar Fe(CO)5 and Pt(acac)2 in n-octylamine will be presented in this account. The nanowires with the average diameter about 2 nm and the length of several hundred nanometers were characterized by TEM, EDS, XRD. It is believed that FePt nanowires were generated via the catalytic solution-liquid-solid (S-L-S) synthetic approach. This process is strongly dependent on the solvent and barely on the reaction temperature and the concentrations of precursors.

Low-Temperature Solution-Phase Synthesis of Quantum Well Structured CdSe Nanoribbons

2006 ◽  
Vol 128 (17) ◽  
pp. 5632-5633 ◽  
Author(s):  
Jin Joo ◽  
Jae Sung Son ◽  
Soon Gu Kwon ◽  
Jung Ho Yu ◽  
Taeghwan Hyeon
Keyword(s):  
Low Temperature ◽  
Quantum Well ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution

Porous cobalt oxide thin films from low temperature solution phase synthesis for electrochromic electrode

2008 ◽  
Vol 516 (23) ◽  
pp. 8573-8578 ◽  
Author(s):  
Hee-Sang Shim ◽  
Vaishali R. Shinde ◽  
Hae Jin Kim ◽  
Yung-Eun Sung ◽  
Won Bae Kim
Keyword(s):  
Thin Films ◽  
Low Temperature ◽  
Cobalt Oxide ◽  
Solution Phase ◽  
Oxide Thin Films ◽  
Phase Synthesis ◽  
Solution Phase Synthesis ◽  
Temperature Solution

Low-temperature solution-phase route to sub-10 nm titanium oxide nanocrystals having super-enhanced photoreactivity

2018 ◽  
Vol 42 (13) ◽  
pp. 10947-10952 ◽  
Author(s):  
Bilal Akram ◽  
Khalil Ahmad ◽  
Jahanzeb Khan ◽  
Bilal Ahmad Khan ◽  
Javeed Akhtar
Keyword(s):  
Low Temperature ◽  
Titanium Oxide ◽  
High Purity ◽  
Solution Phase ◽  
Phase Method ◽  
Temperature Solution ◽  
Solution Phase Method ◽  
Surfactant Assisted

High-purity anatase nanocrystals were prepared by using a low-temperature surfactant-assisted solution-phase method.

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework for high-resolution chromatographic separation

2015 ◽  
Vol 51 (61) ◽  
pp. 12254-12257 ◽  
Author(s):  
Cheng-Xiong Yang ◽  
Chang Liu ◽  
Yi-Meng Cao ◽  
Xiu-Ping Yan
Keyword(s):  
High Resolution ◽  
Surface Area ◽  
Chromatographic Separation ◽  
Room Temperature ◽  
Solution Phase ◽  
Phase Synthesis ◽  
Covalent Organic Framework ◽  
Solution Phase Synthesis ◽  
Temperature Solution ◽  
Organic Framework

Facile room-temperature solution-phase synthesis of a spherical covalent organic framework with large surface area and good stability for high-resolution chromatographic separation.

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