Room temperature interfacial reaction-directed synthesis of hierarchically porous ceria from a water-soluble precursor

2015 ◽  
Vol 3 (13) ◽  
pp. 7022-7028 ◽  
Author(s):  
Guozhu Chen ◽  
Qihui Xu ◽  
Yong Wang ◽  
Guolong Song ◽  
Weiliu Fan
Keyword(s):  
Interfacial Reaction ◽  
Room Temperature ◽  
Water Soluble ◽  
Preparation Process ◽  
Hierarchically Porous ◽  
Directed Synthesis

Hierarchically porous ceria was successfully synthesized via an interfacial reaction between the water-soluble Ce2(SO4)3 precursor and NaOH in ethanol. Neither additional surfactant molecules nor calcination was employed during the preparation process.

Tyrosine-Selective Bioconjugation with Iminoxyl Radicals

2020 ◽  
Author(s):  
Katsuya Maruyama ◽  
Takashi Ishiyama ◽  
Yohei Seki ◽  
Kounosuke Oisaki ◽  
Motomu Kanai
Keyword(s):  
Reaction Time ◽  
Steric Hindrance ◽  
Room Temperature ◽  
Water Soluble ◽  
Light Irradiation ◽  
Sodium Ascorbate ◽  
Iminoxyl Radical ◽  
Short Reaction Time ◽  
Modified Peptides ◽  
The Stability

A novel Tyr-selective protein bioconjugation using the water-soluble persistent iminoxyl radical is described. The conjugation proceeded with high Tyr-selectivity and short reaction time under biocompatible conditions (room temperature in buffered media under air). The stability of the conjugates was tunable depending on the steric hindrance of iminoxyl. The presence of sodium ascorbate and/or light irradiation promoted traceless deconjugation, restoring the native Tyr structure. The method is applied to the synthesis of a protein-dye conjugate and further derivatization to azobenzene-modified peptides.

Water-Soluble Imine Ligand/Palladium-Catalyzed Suzuki Reaction at Room Temperature

2010 ◽  
Vol 31 (10) ◽  
pp. 1277-1280
Author(s):  
Chun LIU ◽  
Qijian NI ◽  
Pingping HU ◽  
Hao YUAN ◽  
Zilin JIN
Keyword(s):  
Room Temperature ◽  
Suzuki Reaction ◽  
Water Soluble ◽  
Palladium Catalyzed

Dynamics of Anthracene Excimer Formation within a Water-Soluble Nanocavity at Room Temperature

2021 ◽  
Vol 143 (4) ◽  
pp. 2025-2036
Author(s):  
Aritra Das ◽  
Ashwini Danao ◽  
Shubhojit Banerjee ◽  
A. Mohan Raj ◽  
Gaurav Sharma ◽  
...  
Keyword(s):  
Room Temperature ◽  
Water Soluble ◽  
Excimer Formation

scholarly journals Facile synthesis of hierarchically porous carbon for supercapacitor derived from water-soluble pitch

2021 ◽  
Vol 631 ◽  
pp. 012101
Author(s):  
Jinliang Zhang ◽  
Junqing Liu ◽  
Danmiao Kang ◽  
Zhijiang Su ◽  
Wenbin Liang ◽  
...  
Keyword(s):  
Porous Carbon ◽  
Water Soluble ◽  
Facile Synthesis ◽  
Hierarchically Porous

Interfacial Reaction-Directed Synthesis of Ce-Mn Binary Oxide Nanotubes and Their Applications in CO Oxidation and Water Treatment

2012 ◽  
Vol 22 (18) ◽  
pp. 3914-3920 ◽  
Author(s):  
Guozhu Chen ◽  
Federico Rosei ◽  
Dongling Ma
Keyword(s):  
Water Treatment ◽  
Co Oxidation ◽  
Interfacial Reaction ◽  
Binary Oxide ◽  
Directed Synthesis

scholarly journals A Novel Photosynthesis of Carboxymethyl Starch-Stabilized Silver Nanoparticles

2014 ◽  
Vol 2014 ◽  
pp. 1-11 ◽  
Author(s):  
M. A. El-Sheikh
Keyword(s):  
Silver Nanoparticles ◽  
Room Temperature ◽  
Colloidal Solution ◽  
Synthesis Method ◽  
Silver Ions ◽  
Water Soluble ◽  
Synthesis Process ◽  
Carboxymethyl Starch ◽  
Round Shape ◽  
First Time

The water soluble photoinitiator (PI) 4-(trimethyl ammonium methyl) benzophenone chloride is used for the first time in the synthesis of silver nanoparticles (AgNPs). A new green synthesis method involves using PI/UV system, carboxymethyl starch (CMS), silver nitrate, and water. A mechanism of the reduction of silver ions to AgNPs by PI/UV system as well as by the newly born aldehydic groups was proposed. The synthesis process was assessed by UV-vis spectra and TEM of AgNPs colloidal solution. The highest absorbance was obtained using CMS, PI and AgNO3concentrations of 10 g/L, 1 g/L, and 1 g/L, respectively; 40°C; 60 min; pH 7; and a material : liquor ratio 1 : 20. AgNPs so-obtained were stable in aqueous solution over a period of three weeks at room temperature (~25°C) and have round shape morphology. The sizes of synthesized AgNPs were in the range of 1–21 nm and the highest counts % of these particles were for particles of 6–10 and 1–3 nm, respectively.

One-Pot Synthesis of Water Soluble, Extremely Small-Sized Superparamagnetic Magnetite Nanoparticles

2012 ◽  
Vol 531 ◽  
pp. 219-222
Author(s):  
Li Hua Shen ◽  
Ting Shang ◽  
Jun Zhou ◽  
Dong Wang ◽  
Yu Han ◽  
...  
Keyword(s):  
Magnetite Nanoparticles ◽  
Room Temperature ◽  
Colloidal Stability ◽  
Aqueous Media ◽  
Mri Contrast Agents ◽  
Water Soluble ◽  
Potential Candidate ◽  
One Pot ◽  
Mri Contrast

Extremely small-sized superparamagnetic magnetite nanoparticles of 3Cit). The resulting Cit-coated magnetite nanoparticles exhibited long-term colloidal stability in aqueous media without any surface modification. Regarding the magnetic properties, the nanoparticles were superparamagnetic at room temperature, and might be the potential candidate for MRI contrast agents.

scholarly journals Shelf-life of Moroccan prickly pear (Opuntia ficus-indica) and argan (Argania spinosa) oils: a comparative study

2021 ◽  
Vol 72 (1) ◽  
pp. e397
Author(s):  
S. Gharby ◽  
D. Guillaume ◽  
I. Nounah ◽  
H. Harhar ◽  
A. Hajib ◽  
...  
Keyword(s):  
Shelf Life ◽  
Room Temperature ◽  
Seed Oil ◽  
Accelerated Aging ◽  
Ease Of Use ◽  
Preparation Process ◽  
Great Care ◽  
Argan Oil ◽  
Cosmetic Industry ◽  
Aging Conditions

Cactus seed oil is gaining considerable popularity in the cosmetic industry. To estimate cactus seed oil’ industrial as well as domestic ease of use, we investigated the oxidative stability of Moroccan cactus seed oil under accelerated aging conditions. In addition, we compared cactus seed oil stability to that of argan oil, a popular and well-established cosmetic oil, under the same conditions. Cactus seed oil is much more sensitive to oxidation than argan oil. Its shelf-life can be estimated to be no longer than 6 months at room temperature. Such instability means that the preparation process for cactus oil must be carried out with great care and cactus seed oil needs to be protected once extracted.

scholarly journals Formation of Water-Soluble Fullerenes [C60,C70] under Ultrasonication and Antioxidant Effect

2017 ◽  
Vol 5 (1) ◽  
pp. 61
Author(s):  
Weon-Bae Ko ◽  
Hong-Seok Jeong ◽  
Sung-Ho Hwang
Keyword(s):  
Hydrogen Peroxide ◽  
Room Temperature ◽  
Antioxidant Effect ◽  
Water Soluble ◽  
Maldi Tof Ms ◽  
Pc 12 Cells ◽  
Effect Of Water ◽  
Maldi Tof ◽  
Line Following ◽  
Tof Ms

<p>The water-soluble fullerenes [C<sub>60</sub>, C<sub>70</sub>] are prepared with fullerenes [C<sub>60</sub>, C<sub>70</sub>] and a mixture of oxidants (v/v) at the ratio of 3:1 under ultrasonic condition at room temperature. The MALDI-TOF MS confirmed that the water-soluble compounds were C<sub>60</sub> and C<sub>70</sub>. The antioxidant effect of water-soluble fullerenes [C<sub>60</sub>, C<sub>70</sub>] in the PC 12 cells (Rat pheochromocytoma) line following exposure to hydrogen peroxide (H<sub>2</sub>O<sub>2</sub>) was investigated.</p>

Water-Soluble N-Heterocyclic Carbene Platinum(0) Complexes: Recyclable Catalysts for the Hydrosilylation of Alkynes in Water at Room Temperature

2012 ◽  
Vol 31 (8) ◽  
pp. 3355-3360 ◽  
Author(s):  
Gustavo F. Silbestri ◽  
Juan Carlos Flores ◽  
Ernesto de Jesús
Keyword(s):  
Room Temperature ◽  
Water Soluble ◽  
Recyclable Catalysts
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