Revealing structural evolution of PbS nanocrystal catalysts in electrochemical CO2 reduction using in situ synchrotron radiation X-ray diffraction
2019 ◽
Vol 7
(41)
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pp. 23775-23780
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Keyword(s):
X Ray
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In situ synchrotron radiation X-ray diffraction studies reveal reaction environment-induced PbS–PbCO3–Pb evolution under eCO2RR conditions. The produced Pb nanocatalyst exhibits 97.6% FE (−1.2 V) and 74.9 mA mgPb−1 MA (−1.4 V).