scholarly journals Aging Methods—An Evaluation of Their Influence on Bond Strength

2021 ◽  
Author(s):  
Gabriela Simões Teixeira ◽  
Gabriel Kalil Rocha Pereira ◽  
Alexandre Henrique Susin
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Third Molars ◽  
Thermal Cycles ◽  
Universal Adhesive ◽  
Etch And Rinse ◽  
Strength Tests ◽  
Post Hoc ◽  
Microshear Bond Strength ◽  
Self Etch

Abstract Objectives To evaluate the effect of different artificial aging methods on the bond strength of a resin composite associated with a universal adhesive (Scotchbond Universal) used under two etching approaches (self-etch [SE] or etch-and-rinse [ER]) to enamel and dentin substrates. Materials and Methods A total of 96 noncarious human third molars were prepared and randomly divided according to three factors (n = 6): substrate (enamel and dentin), adhesive approach (SE and ER), and aging method (water storage for 24 hours, 6 months, or 1 year; subjected to 10,000, 20,000, or 30,000 thermal cycles; and sodium hypochlorite [NaOCl] storage for 1 or 5 hours). Statistical Analysis Microshear bond strength tests were conducted, and the collected data (MPa) were subjected to three-way analysis of variance (ANOVA) with post hoc Bonferroni tests (p < 0.05) and Weibull analysis. The failure pattern was also evaluated. Results Three-way ANOVA revealed that the factors “substrate” (p = 0.00) and “aging method” (p = 0.00) had a significant effect on the bond strength, but the factor “adhesive approach” did not (p = 0.84). The bond strength in the enamel group for the SE approach was negatively affected under 20,000 and 30,000 thermal cycles. Weibull presented the highest m in the NaOCl storage for the 5 hours group to enamel using the SE and to dentin using ER approaches. Adhesive/mixed failures were predominant for all groups. Conclusion Thermocycling aging (20,000 and 30,000 cycles) significantly reduced the bond strength to enamel using the SE approach. On the contrary, storage with the NaOCl method proved to increase bond strength under the evaluated conditions.

scholarly journals Influence of Conditioning Time of Universal Adhesives on Adhesive Properties and Enamel-Etching Pattern

2016 ◽  
Vol 41 (5) ◽  
pp. 481-490 ◽  
Author(s):  
AM Cardenas ◽  
F Siqueira ◽  
J Rocha ◽  
AL Szesz ◽  
M Anwar ◽  
...  
Keyword(s):  
Bond Strength ◽  
Degree Of Conversion ◽  
Adhesive Properties ◽  
Universal Adhesive ◽  
Etching Pattern ◽  
Etch And Rinse ◽  
Universal Adhesives ◽  
Microshear Bond Strength ◽  
Self Etch

SUMMARY Objectives: To evaluate the effect of application protocol in resin–enamel microshear bond strength (μSBS), in situ degree of conversion, and etching pattern of three universal adhesive systems. Methods and Materials: Sixty-three extracted third molars were sectioned in four parts (buccal, lingual, and proximals) and divided into nine groups, according to the combination of the main factors—Adhesive (Clearfil Universal, Kuraray Noritake Dental Inc, Tokyo, Japan; Futurabond U, VOCO, Cuxhaven, Germany; and Scotchbond Universal Adhesive, 3M ESPE, St Paul, MN, USA)—and enamel treatment/application time (etch-and-rinse mode [ER], self-etch [SE] application for 20 seconds [SE20], and SE application for 40 seconds [SE40]). Specimens were stored in water (37°C/24 h) and tested at 1.0 mm/min (μSBS). The degree of conversion of the adhesives at the resin–enamel interfaces was evaluated using micro-Raman spectroscopy. The enamel-etching pattern was evaluated under a scanning electron microscope. Data were analyzed with two-way analysis of variance and Tukey test (α=0.05). Results: In general, the application of the universal adhesives in the SE40 produced μSBS and degree of conversion that were higher than in the SE20 (p&lt;0.01) and similar to the ER mode. The deepest enamel-etching pattern was obtained in the ER mode, followed by the SE40. Conclusions: The active and prolonged application of universal adhesives in the SE mode may be a viable alternative to increase the degree of conversion, etching pattern, and resin–enamel bond strength.

scholarly journals Self-etch or etch-and-rinse mode did not affect the microshear bond strength of a universal adhesive to primary dentin

2016 ◽  
Vol 35 (2) ◽  
pp. 174-179 ◽  
Author(s):  
Benjaporn THANARATIKUL ◽  
Busayarat SANTIWONG ◽  
Choltacha HARNIRATTISAI
Keyword(s):  
Bond Strength ◽  
Universal Adhesive ◽  
Etch And Rinse ◽  
Microshear Bond Strength ◽  
Self Etch

scholarly journals Microshear Bond Strength of Scotchbond Universal Adhesive to Primary and Permanent Dentin: A Six-Month In Vitro Study

2019 ◽  
Author(s):  
Masoud Fallahinejad Ghajari ◽  
Amir Ghasemi ◽  
Mohammadreza Badiee ◽  
Zahra Abdolazimi ◽  
Alireza Akbarzadeh Baghban
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Permanent Teeth ◽  
Universal Adhesive ◽  
Mode Of Application ◽  
Etch And Rinse ◽  
Microshear Bond Strength ◽  
Self Etch

Objectives: This study aimed to assess the microshear bond strength (MSBS) of Scotchbond Universal adhesive, used in self-etch and etch-and-rinse modes, to primary and permanent dentin at 24 hours and six months. Materials and Methods: A total of 88 composite micro-cylinders were divided into eight groups (n=11) as follows: (A) Etch-and-rinse, 24 hours, primary dentin; (B) Self-etch, 24 hours, primary dentin; (C) Etch-and-rinse, six months, primary dentin; (D) Self-etch, six months, primary dentin; (E) Etch-and-rinse, 24 hours, permanent dentin; (F) Self-etch, 24 hours, permanent dentin; (G) Etch-and-rinse, six months, permanent dentin; (H) Self-etch, six months, permanent dentin. The MSBS was measured by a testing machine at a crosshead speed of 0.5 mm/minute. Data were analyzed using three-way analysis of variance (ANOVA). Results: The mean MSBS was 12.3±2.3 MPa in A, 18.8±4.1 MPa in B, 11.9±3.7 MPa in C, 16±2.9 MPa in D, 19.1±2.7 MPa in E, 22.8±4.1 MPa in F, 16.2±2.6 MPa in G, and 17.2±4.4 MPa in H. In the self-etch mode, the MSBS was significantly higher than that in the etch-and-rinse mode (P<0.001). The MSBS in permanent teeth was significantly higher than primary teeth (P<0.001). At six months, the MSBS significantly decreased in all groups (P<0.001). Conclusion: The micro-shear bond strength of Scotchbond Universal adhesive decreases over time and depends on the type of tooth and the mode of application of the adhesive.

scholarly journals Effect of Different Adhesion Protocols on the Shear Bond Strength of Universal Adhesive Systems to Sound and Artificial Caries-Affected Dentin

2021 ◽  
Author(s):  
Omnia M. Sami ◽  
Essam A. Naguib ◽  
Rasha H. Afifi ◽  
Shaymaa M. Nagi
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Resin Composite ◽  
Single Bond ◽  
Adhesive Systems ◽  
Universal Adhesive ◽  
Etch And Rinse ◽  
Significant Difference ◽  
Self Etch

Abstract Objective Bonding to different dentin substrates influences resin composite restoration outcomes. This study investigated the influence of different adhesion protocols on the shear bond strength of universal adhesive systems to sound and artificial caries-affected dentin (CAD). Materials and Methods Occlusal enamel of 80 premolars were wet grinded to obtain flat midcoronal dentin. Specimens were equally divided according to the substrate condition: sound and CAD by subjecting to pH-cycling for 14 days. Each dentin substrate was bonded with the adhesive systems used in this study: Single Bond universal adhesive or Prime&Bond universal (applied either in etch-and-rinse or self-etch adhesion protocol). Adhesive systems were utilized according to manufacturers’ instructions, then resin composite was built up. Specimens were tested for shear bond strength. The data were analyzed by three-way analysis of variance, and failure modes were determined using stereomicroscope. Results There was no statistically significant difference between the two tested adhesive systems on artificially created CAD with different adhesion protocols. On sound dentin, Single Bond universal, either in the etch-and-rinse or self-etch adhesion protocols, revealed higher statistically significant shear bond strength mean values compared with CAD. Conclusion Single Bond universal adhesive in an etch-and-rinse adhesion protocol improved only bonding to sound dentin, while no added positive effect for the etching step with Prime&Bond universal adhesive was found when bonded to both sound and CAD substrates. The influence of CAD on the performance of the universal adhesives was material-dependent.

scholarly journals Evaluation of Dentin Microroughness and Composite Bond Strength After Multiple Uses of Diamond Burs

2021 ◽  
pp. 353-365
Author(s):  
Melissa Jiménez-Hernández ◽  
Daniel Chavarría-Bolaños ◽  
Fabián Murillo-Gómez ◽  
José Vega-Baudrit ◽  
Amaury Pozos-Guillén ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Universal Adhesive ◽  
Diamond Bur ◽  
Diamond Crystals ◽  
Strength Tests ◽  
The Mean ◽  
Multiple Uses ◽  
Self Etch ◽  
Dental Burs

Using a bur multiple times to prepare dental structure may produce a smoother final surface on dentin than a new one. This superficial roughness may affect adhesion with resin-based materials by modifying the substrates’ characteristics. The aim of this study was to evaluate the effect of multiple uses of diamond burs on dentin’s superficial microroughness and bond strength with resin composite when using a self-etch adhesive. Diamond dental burs were used to simulate a preparation (dentin flat surface) on extracted third molars. Samples were distributed into groups according to burs’ number of previous uses as follows: 0, 1, 5 and 10. Scanning electron microscopy images at 70x, 350x, and 1000x were used to illustrate burs’ deformation. Each specimen’s dentin microroughness was measured three times to compare between experimental groups and the micro-shear bond strength test (n=15) was performed for the 0 and 10 uses groups using a universal adhesive in a self-etching mode. Diamond crystals wear and dislodgements were evident among groups where the burs were used more times. As the number of uses increased the mean microroughness of the dentin surface decreased with significant differences between the 0 and 10 uses groups. No statistical differences between experimental groups resulted from bond strength tests. When using a universal adhesive in a self-etching mode, the number of previous uses of a diamond bur seems to have no significant effect on dentin/resin composite bond strength.

scholarly journals Effect of caries-affected dentin on one-step universal and multi-step etch-and-rinse adhesives’ bond strength

2017 ◽  
Vol 46 (5) ◽  
pp. 273-277
Author(s):  
Clecila MÜLLER ◽  
Gabriela Cauduro da ROSA ◽  
Gabriela Simões TEIXEIRA ◽  
Ivo KREJCI ◽  
Tissiana BORTOLOTTO ◽  
...  
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Single Bond ◽  
Etch And Rinse ◽  
One Step ◽  
Post Hoc ◽  
Microshear Bond Strength ◽  
Application Protocols ◽  
Self Etch ◽  
Test Result

Abstract Objective To evaluate the influence of caries-affected dentin on bond strength of a universal one-step and a multi-step etch-and-rinse adhesive system. Material and method Enamel of 60 third human molars with and without caries was removed to expose dentin. The teeth were randomly assigned to six groups: Single Bond Universal (3M ESPE, St. Paul, MN, USA) in etch-and-rinse and in self-etch mode and Prime & Bond NT (Dentsply Co, Konstanz, Germany), all on sound and caries-affected dentin. Smear layer of the 30 sound dentin specimens was standardized by polishing with 600-grit SiC paper under water cooling. Residual infected dentin of the 30 caries-affected specimens was removed with a number 4 CA carbide bur until no caries smooth tissue was detectable by tactile-visual inspection. Cylinders of a light cured composite resin (Filtek Z350 XT, 3M ESPE) were built up using starch tubes and microshear test was performed until failure. The data was analyzed by one-way ANOVA and Tukey’s post hoc test. Result Significant differences in microshear bond strength (μSBS) were observed for the caries-affected groups, but not for sound dentin. The μSBS of Single Bond Universal were not influenced by the application protocol on sound dentin, however they were lower in the caries-affected group with both application protocols. The μSBS for Prime & Bond NT was not influenced by the dentin conditions. Conclusion Caries-affected dentin decrease in bond strength of Single Bond Universal in comparison to sound dentin. The bond strength of Prime & Bond NT was not altered by substrate conditions.

Effect of Different Protocols in Preconditioning With EDTA in Sclerotic Dentin and Enamel Before Universal Adhesives Applied in Self-etch Mode

2017 ◽  
Vol 42 (3) ◽  
pp. 284-296 ◽  
Author(s):  
EC Martini ◽  
SO Parreiras ◽  
MF Gutierrez ◽  
AD Loguercio ◽  
A Reis
Keyword(s):  
Bond Strength ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Etching Pattern ◽  
Bonding Performance ◽  
Universal Adhesives ◽  
Microshear Bond Strength ◽  
Self Etch ◽  
Main Factor

SUMMARY Objectives: The aim of this study was to investigate the effect of different protocols of 17% ethylene diamine tetra-acetic acid (EDTA) conditioning on the etching pattern and immediate bond strength of universal adhesives to enamel and sclerotic dentin. Methods and Materials: Forty bovine teeth with sclerotic dentin and 20 human third molars were randomly divided into eight groups resulting from the combination of the main factors surface treatment (none, two-minute EDTA conditioning manual application, 30-second EDTA manual application, 30-second EDTA sonic application) and adhesives systems (Scotchbond Universal Adhesive [SBU] and Prime & Bond Elect [PBE]). Resin-dentin and enamel-dentin bond specimens were prepared and tested under the microtensile bond strength (μTBS) and microshear bond strength (μSBS) tests, respectively. The etching pattern produced on the unground enamel and the sclerotic dentin surfaces under the different protocols and adhesive systems was evaluated under scanning electron microscopy. Results: For enamel, only the main factor adhesive was significant (p&lt;0.0001), with SBU showing the highest μSBS. In sclerotic dentin, the lowest mean was observed for the group without EDTA application and the highest mean in the group with EDTA application with the sonic device for 30 seconds. Regardless of the EDTA protocol, the highest means of μTBS were observed for SBU (p&lt;0.05). Conclusions: EDTA conditioning improves the bonding performance of universal adhesives in the self-etch mode on sclerotic dentin, mainly when applied for 30 seconds with the aid of a sonic device. EDTA pretreatment also improves the retentive etching pattern of enamel, but it does not result in higher enamel bond strength.

scholarly journals Effects of Contamination by Hemostatic Agents and Use of Cleaning Agent on Etch-and-Rinse Dentin Bond Strength

2016 ◽  
Vol 27 (6) ◽  
pp. 688-692 ◽  
Author(s):  
César Rogério Pucci ◽  
Rodrigo Maximo de Araújo ◽  
Ana Julia Farias de Lacerda ◽  
Mirella Anjos de Souza ◽  
Maria Filomena Rocha Lima Huhtala ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Control Group ◽  
Hemostatic Agents ◽  
Diamond Bur ◽  
Mechanical Cycling ◽  
Etch And Rinse ◽  
Post Hoc ◽  
Push Out ◽  
Cleaning Protocol

Abstract The aim of this study was to evaluate the influence of contamination by hemostatic agents and rinsing with chlorhexidine on bond strength between dentin and resin composite. Ninety-six bovine teeth were sectioned to expose a flat dentin surface area. A standardized cavity with 2.0 mm in thickness, superficial diameter of 4.0 mm and bottom diameter of 3.0 mm was prepared with a diamond bur in each dentin specimen. The teeth were divided into four groups according to the hemostatic employed: G1: control; G2: use of ViscoStat, Ultradent; G3: Hemosthasegel, FGM; and G4: Hemostop, Dentsply. The groups were divided into two subgroups according to the cleaning protocol method (n=12): A: without any further cleaning; and B: cleaning with chlorhexidine at 0.2%. All cavities were filled using a dentin adhesive and a resin composite, following the manufacturer's instructions. After 24 h, the specimens were aged by thermal and mechanical cycling. The bond strength was determined by the push out bond test (MPa), Statistical analysis was performed using two-way ANOVA and Tukey test (p<0.05). Statistically significant differences were detected among all groups treated with hemostatic agents and the control group. The post-hoc test showed that cleaning the cavity with chlorhexidine significantly improves the bond strength between dentin and resin composite. Our results suggested that the use of chlorhexidine can reestablish the bond strength between dentin and resin composite when a hemostatic agent was applied.

scholarly journals Influence of Etching Mode and Composite Type on Bond Strength to Biodentine Using a “No-Wait” Universal Adhesive

2021 ◽  
pp. 354-365
Author(s):  
Ayça Sarialioğlu Güngör ◽  
Betül Aycan Uysal
Keyword(s):  
Bond Strength ◽  
Failure Modes ◽  
High Viscosity ◽  
Resin Composites ◽  
Universal Adhesive ◽  
Low Viscosity ◽  
Composite Type ◽  
Etch And Rinse ◽  
No Wait ◽  
Post Hoc

The purpose of this study was to compare the shear bond strength (SBS) of four resin-based composite materials to a silicate-based cement using a “no-wait” universal bond with self-etch (SE) and etch-and-rinse (ER) modes. Acrylic blocks (n=80, 2mm depth, 5mm diameter central hole) were prepared. The holes were filled with BiodentineTM (BD) and divided into 4 main groups (n=20) according to the composite resin type used: Group FZ250: FiltekTM Z250 Universal Restorative (microhybrid), Group SDR: SDR Plus U Bulk Fill Flowable (low-viscosity bulk-fill), Group FBP: FiltekTM Bulk Fill Posterior (high-viscosity bulk-fill), Group EF: EsFlow™ Universal Flowable Composite (nanohybrid). A ‘no-wait’ universal bond (Clearfil Universal Bond Quick) was used for bonding application. Then each group was divided into 2 subgroups according to the etching mode applied (ER and SE). SBSs were measured and stereomicroscope was used to identify the failure modes. Selected samples of fracture surfaces were imaged by SEM. Tukey’s post-hoc and One-way ANOVA tests were used to analyze data. There were statistically significant differences among the composite groups (p<0.05). When SDR  showed the highest bond strength values in SE (17.13 ± 2.98 MPa) mode, FBP showed the lowest bond strength values in ER (8.89 ± 2.46 MPa) mode. The mean SBS was not different between the SE and ER modes (p> 0.05). The SBS of BD to the resin composites depends on the composite type but  application of the ‘no-wait’ universal bond in different etching modes is regardless of the SBS of BD to resin composites.

scholarly journals Microshear Bond Strength of Different Adhesive Systems to Dentin

2019 ◽  
Author(s):  
Sara Valizadeh ◽  
Aida Moradi ◽  
Mansooreh Mirazei ◽  
Hooman Amiri ◽  
Mohammad Javad Kharazifard
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Single Bond ◽  
Adhesive Systems ◽  
Etch And Rinse ◽  
Significant Difference ◽  
Microshear Bond Strength ◽  
Self Etch ◽  
Composite Cylinders

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.

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