Effect of Ground Freezing with Liquid Nitrogen on Freezing Rate and Mechanical Properties of Coastal Clayey Silt

2021 ◽  
Vol 147 (9) ◽  
pp. 04021057
Author(s):  
Hyun-Jun Choi ◽  
Jongmuk Won ◽  
Dongseop Lee ◽  
Hyobum Lee ◽  
Hangseok Choi
2018 ◽  
Vol 36 (6) ◽  
pp. 1609-1628 ◽  
Author(s):  
Chengzheng Cai ◽  
Feng Gao ◽  
Yugui Yang

Liquid nitrogen is a type of super-cryogenic fluid, which can cause the reservoir temperature to decrease significantly and thereby induce formation rock damage and cracking when it is injected into the wellbore as fracturing fluid. An experimental set-up was designed to monitor the acoustic emission signals of coal during its contact with cryogenic liquid nitrogen. Ultrasonic and tensile strength tests were then performed to investigate the effect of liquid nitrogen cooling on coal cracking and the changes in mechanical properties thereof. The results showed that acoustic emission phenomena occurred immediately as the coal sample came into contact with liquid nitrogen. This indicated that evident damage and cracking were induced by liquid nitrogen cooling. During liquid nitrogen injection, the ring-down count rate was high, and the cumulative ring-down counts also increased rapidly. Both the ring-down count rate and the cumulative ring-down counts during liquid nitrogen injection were much greater than those in the post-injection period. Liquid nitrogen cooling caused the micro-fissures inside the coal to expand, leading to a decrease in wave velocity and the deterioration in mechanical strength. The wave velocity, which was measured as soon as the sample was removed from the liquid nitrogen (i.e. the wave velocity was recorded in the cooling state), decreased by 14.46% on average. As the cryogenic samples recovered to room temperature, this value increased to 18.69%. In tensile strength tests, the tensile strengths of samples in cooling and cool-treated states were (on average) 17.39 and 31.43% less than those in initial state. These indicated that both during the cooling and heating processes, damage and cracking were generated within these coal samples, resulting in the acoustic emission phenomenon as well as the decrease in wave velocity and tensile strength.


2021 ◽  
pp. 1-10
Author(s):  
Menglin Du ◽  
Feng Gao ◽  
Chengzheng Cai ◽  
Shanjie Su ◽  
Zekai Wang

Abstract Exploring the damage differences between different coal rank coal reservoirs subjected to liquid nitrogen (LN2) cooling is of great significance to the rational development and efficient utilization of coalbed methane. For this purpose, the mechanical properties, acoustic emission (AE) characteristics and energy evolution law of lignite and bituminous coal subjected to LN2 cooling were investigated based on the Brazilian splitting tests. Then, pore structure changes were analyzed to reveal the difference in the microscopic damage between lignite and bituminous coal after LN2 cooling. The results showed that compared with bituminous coal, the pore structure of lignite coal changed more obviously, which was manifested as follows: significant increases in porosity, pore diameters, and pore area; a larger transformation from micropores and transition pores to mesopores and macropores. After LN2 cooling, the thermal damage inside lignite and bituminous coal was 0.412 and 0.069, respectively. The thermal damage reduced the cohesive force between mineral particles, leading to the deterioration of the macroscopic physical and mechanical properties. Simultaneously, denser AE ringing counts and larger accumulated ringing counts were observed after LN2 cooling. Moreover, the random distribution of thermal damage enhanced the randomness of the macrocrack propagation direction, resulting in an increase in the crack path tortuosity. With more initial defects inside coal, a more obvious thermal damage degree and wider damage distribution will be induced by LN2 cooling, leading to more complicated crack formation paths and a higher fragmentation degree, such as that of lignite coal.


2012 ◽  
Vol 584 ◽  
pp. 556-560 ◽  
Author(s):  
B. Gopi ◽  
N. Naga Krishna ◽  
K. Sivaprasad ◽  
K. Venkateswarlu

The present work investigates the effect of rolling temperature on the mechanical properties and microstructural evolution of an Al-Mg-Si alloy with 3wt% TiB2 in-situ composite that was fabricated by stir casting route. The composite was rolled to a true strain of ≈0.7 at three different temperatures viz; room temperature (RT), liquid propanol (LP) and liquid nitrogen (LN) temperatures. Tensile tests revealed that the samples rolled at liquid nitrogen temperature exhibited improved properties compared to the samples rolled at other two temperatures. A tensile strength and ductility of 291 MPa and 8% respectively were exhibited by the liquid nitrogen rolled sample. The strength is observed to be ≈12% higher and ductility is ≈60% more when compared to the room temperature rolled sample. X ray diffraction peaks indicated that rolled samples exhibited considerable increase in peak broadening compared to the unrolled one, which is attributed to the increase of the lattice strain due to distortion and the decrease in grain size of the material. The enhanced mechanical properties of the liquid nitrogen rolled samples were attributed to the combined effect of grain refinement and accumulation of higher dislocation density.


This study examines the influence of varied conditions of cooling and different rotations of tool on the accuracy of weld of aluminum samples taken out by friction stir welding process. The aim of this study was to check the effects on samples of aluminum alloy of A356 grades that were welded by friction stir welding under various conditions of cooling like cooling by water, cooling by air, cooling by nitrogen gas and cooling by lubrication oil at two varied rotating speed of tool at 900 revolution per minute and 1100 revolution per minute. These readings were being carried by experimental investigations. The influence of these different parameters on micro structural and mechanical properties of these joint are discussed. Cooling the different specimens by lubrication oil or liquid nitrogen showed to reduce the input heat in processing which reduce the improvement of grains in between the process. The reduction in input heat showed in decreasing the microscopic defects in the specimen found to gain in micro hardness and betterment of tensile properties. It was observed that best machining properties was found when the rotational speed is higher and no condition of cooling is used i.e. friction stir welding is applied in air. Also, the better findings found out from all the specimens when cooling by liquid nitrogen under rotating speed of tool at 1100 rpm as it represents higher tensile.


2020 ◽  
Vol 10 (17) ◽  
pp. 6055
Author(s):  
Zhao Liu ◽  
Youhong Sun ◽  
Bingge Wang ◽  
Qiang Li

The application of conventional artificial ground freezing (AGF) has two disadvantages: low freezing rate and small frozen range. In this study, a new method with natural cold gas injection was proposed, whereby the shallow soils and water can be frozen rapidly due to the effect of the heat convection. Cold gas from −15 °C to −10 °C, in the winter of northeast China, was injected into the laboratory-scale sand pipe; evolution of the induced frozen front and water migration were studied, and then, the feasibility of the new method was analyzed. According to the evolution of the induced frozen front, the freezing process was divided into an initial cooling stage, phase transition stage, and subcooled stage. The results showed that the increase of initial water content at the beginning of the experiments had little effect on the time required for completing the initial cooling stage, while the time required for the phase transition would increase in nearly the same proportion. In addition, the increase of the cold gas flow rate could not only strengthen the cooling rate of the initial cooling stage but also shorten the phase transition time; thereby, the freezing rate was increased. The freezing rate could reach 0.18–0.61 cm/min in the direction of cold gas flow, and compared to the conventional AGF (months are required for approximately 1 m), the freezing efficiency was greatly improved.


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