Improved Electron Beam Scanning System for Electron Microprobe X‐Ray Analyzers

1968 ◽  
Vol 39 (12) ◽  
pp. 1804-1806 ◽  
Author(s):  
Richard N. Kniseley ◽  
Francis C. Laabs ◽  
Dean Van Zuuk
2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
Andrii Sofiienko ◽  
Chad Jarvis ◽  
Ådne Voll

Monte Carlo simulations were used to study photon production in a panoramic X-ray tube with a conical tungsten target to determine the optimal characteristics of the target shape and electron beam configuration. Several simulations were performed for accelerating potentials equal to 250 kV, 300 kV, and 500 kV with electron beams of various radii and anode sizes. The angular distribution of the photon intensity was analysed by numerical calculations for an assembly composed of an X-ray tube and an external collimator with a cylindrical hole to simulate a panoramic scanning system with an X-ray pencil beam.


2020 ◽  
Vol 41 (1) ◽  
pp. 167-170 ◽  
Author(s):  
Kang An ◽  
Yifan Yin ◽  
Fukun Li ◽  
Limin Shi ◽  
Xiaolong Hu ◽  
...  

1961 ◽  
Vol 5 ◽  
pp. 538-553 ◽  
Author(s):  
David B. Wittry ◽  
Ray Fitzgerald

AbstractA versatile beam-scanning system has been developed for use with the Electron Microprobe X-ray Analyzer manufactured by Applied Research Laboratories, Inc. It provides for the display of X-ray intensities from any of three spectrometers, three nondispersive detectors (either counters or scintiallation counters), as well as the current collected by the target or the current backscattered by the target. The electrostatic deflection system does not interfere with the use of the optical-viewing system and provides a maximum scanning area of only slightly less than field of view of the optical-viewing system.A stepping motor, controlled from the readout console, has also been developed which permits automatic point-by-point analysis of a specimen with minimum operator attention. In the use of this attachement, measurements may be made for fixed time, fixed charge, or fixed counts (integrated intensity) at each point. As a result, the step-scanning motor facilitates accurate measurement of one-dimensional concentration fluctuations and is particularly useful for phase identification and studies of diffusion and segregation.


2001 ◽  
Vol 7 (S2) ◽  
pp. 146-147
Author(s):  
Colin M. MacRae ◽  
N.C. Wilson ◽  
M. Otsuki

When an electron beam interacts with a solid target a number of interactions occur which produce electrons, x-rays and light. Typically in an electron microprobe analyser (EPMA) both the electron and x-ray signals are collected for analysis and imaging. However, if the EPMA is equipped with an optical spectrometer then all three signals can be collected. Commonly, the optical or CathodoLuminescence (CL) spectrometer is a monochromator type and can only collect a single frequency or small range of frequencies at a time. Simultaneous collection of the complete visible spectrum is not possible. The collection optics associated with the spectrometer often must be moved into place to start collection, this then obscures the other detectors and prevents simultaneous collection. At CSIRO Minerals an optical spectrometer has been integrated into a JEOL 8900R EPMA and allows simultaneous collect of all light, x-rays and electron signals. This form of mapping, termed Holistic Mapping, has significant advantages over traditional mapping in that it removes the need to have a priori knowledge about what the important frequencies are that will provide the solution to the problem at hand.


Author(s):  
R. Sinclair ◽  
B.E. Jacobson

INTRODUCTIONThe prospect of performing chemical analysis of thin specimens at any desired level of resolution is particularly appealing to the materials scientist. Commercial TEM-based systems are now available which virtually provide this capability. The purpose of this contribution is to illustrate its application to problems which would have been intractable until recently, pointing out some current limitations.X-RAY ANALYSISIn an attempt to fabricate superconducting materials with high critical currents and temperature, thin Nb3Sn films have been prepared by electron beam vapor deposition [1]. Fine-grain size material is desirable which may be achieved by codeposition with small amounts of Al2O3 . Figure 1 shows the STEM microstructure, with large (∽ 200 Å dia) voids present at the grain boundaries. Higher quality TEM micrographs (e.g. fig. 2) reveal the presence of small voids within the grains which are absent in pure Nb3Sn prepared under identical conditions. The X-ray spectrum from large (∽ lμ dia) or small (∽100 Ǻ dia) areas within the grains indicates only small amounts of A1 (fig.3).


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