Effects of oxidation and abnormal grain growth on the magnetic properties of thin Fe–SiO2 granular films

1999 ◽  
Vol 85 (8) ◽  
pp. 6151-6153 ◽  
Author(s):  
J. N. Zhou ◽  
A. Butera ◽  
H. Jiang ◽  
D. H. Yang ◽  
J. A. Barnard
1992 ◽  
Vol 06 (19) ◽  
pp. 1197-1203 ◽  
Author(s):  
S. SZYMURA ◽  
H. BALA ◽  
YU. M. RABINOVICH ◽  
J. J. WYSLOCKI

The microstructure and magnetic properties of Nd 16-x X x Fe 70.5 Co 5 AlB 7.5 and Nd 14-x Dy 2 X x Fe 71 Co 5 B 8 ( X = Ca , Cl and C ) magnets with various x were examined. In magnets after sintering and heat treatment carbon-rich areas were produced within the non-magnets Nd -rich phase. However chlorine-rich and calcium-rich areas were present in both non-magnetic Nd -rich and B -rich phases. The contribution of C ≤0.35 at%, Cl ≤0.013 at% and Ca ≤0.09 at% had no influence on the magnetic properties (B r and i H c ), but higher concentration of these elements caused decrease in these properties. Abnormal grain growth was found in magnets containing Cl .


2012 ◽  
Vol 706-709 ◽  
pp. 2622-2627 ◽  
Author(s):  
Chun Kan Hou ◽  
Jian Ming Tzeng

Effects of three heating rates, 5, 20/min., and 300°C/sec and decarburization temperature, 700-850°C in primary annealing on the microstructure and magnetic properties of a grain oriented electrical steel were investigated. It was found that the oxide layer thickness and grain size increased with increasing decarburization temperature. However, they decreased with increasing heating rate. On the other hand, injection nitrogen content into steel sheets decreased with increasing decarburization temperature. The percentage of abnormal grain growth obtained a peak value at 800°C in the specimens treated with heating rate less than 20°C per minute. But specimens with rapid heating rate, percentage of abnormal grain growth increased with increasing decarburization temperature. As percentage of abnormal growth increased, magnetic properties got better.


2005 ◽  
Vol 475-479 ◽  
pp. 2193-2196 ◽  
Author(s):  
Haisheng Zhong ◽  
Qiang Li ◽  
Zhifeng Zhong ◽  
Ming Cheng

Ni-Zn ferrite ceramics were prepared from the blend of nano-sized powders and ultra-fine particles at the relative low sintering temperature (≤1200°C). The microstructure of the as-sintered samples characterized by SEM indicated that this process obstructed abnormal grain growth which often appeared in the Ni-Zn ferrite ceramics sintered from the nano-sized powders. The result of VSM measurements showed that the ratio of nano-sized powders to ultra-fine particles effected the initial permeability (μi) of the as-sintered samples. Optimum initial permeability can be obtained by adjusting the ratio as 1:1.


2007 ◽  
Vol 539-543 ◽  
pp. 4428-4433 ◽  
Author(s):  
Y. Arita ◽  
Yoshiyuki Ushigami

The effect of annealing temperature on grain growth, texture development and magnetic properties of Al-free and Al-1% added non-oriented electrical steel were investigated. Normal grain growth occurred in Al-free steel. On the other hand, abnormal grain growth occurred in Al-added steel which was annealed at 800°C for 24h. Precipitates in these two steels were different. TiN precipitated in Alfree steel, but in the case of Al-added steel, AlN and TiC precipitated. The TiC in Al-added steel was so fine that it inhibited the normal grain growth and finally caused the abnormal grain growth. Main textures of both steels were near {111}<112>, but the intensity of near {111}<112> in the abnormal grain growth was higher than that in the normal grain growth. Magnetic flux density (B50/Bs) was decreased by the grain growth. Especially B50/Bs in the abnormal grain growth was lower than that in normal grain growth. B50/Bs in these steels can be estimated by their three-dimensional textures in vector method.


2018 ◽  
Author(s):  
Risheng Pei ◽  
Sandra Korte-Kerzel ◽  
Talal Al-Samman

Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 504
Author(s):  
Huasong Liu ◽  
Yannan Dong ◽  
Hongguang Zheng ◽  
Xiangchun Liu ◽  
Peng Lan ◽  
...  

AlN precipitates are frequently adopted to pin the austenite grain boundaries for the high-temperature carburization of special gear steels. For these steels, the grain coarsening criterion in the carburizing process is required when encountering the composition optimization for the crack-sensitive steels. In this work, the quantitative influence of the Al and N content on the grain size after carburization is studied through pseudocarburizing experiments based on 20Cr steel. According to the grain structure feature and the kinetic theory, the abnormal grain growth is demonstrated as the mode of austenite grain coarsening in carburization. The AlN precipitate, which provides the dominant pinning force, is ripened in this process and the particle size can be estimated by the Lifshitz−Slyosov−Wagner theory. Both the mass fraction and the pinning strength of AlN precipitate show significant influence on the grain growth behavior with the critical values indicating the grain coarsening. These criteria correspond to the conditions of abnormal grain growth when bearing the Zener pinning, which has been analyzed by the multiple phase-field simulation. Accordingly, the models to predict the austenite grain coarsening in carburization were constructed. The prediction is validated by the additional experiments, resulting in accuracies of 92% and 75% for the two models, respectively. Finally, one of the models is applied to optimize the Al and N contents of commercial steel.


2020 ◽  
Vol 128 (18) ◽  
pp. 185109
Author(s):  
Christian Braun ◽  
Raphael A. Zeller ◽  
Hanadi Menzel ◽  
Jörg Schmauch ◽  
Carl E. Krill ◽  
...  

2021 ◽  
Vol 864 ◽  
pp. 158816
Author(s):  
Galina Kozhina ◽  
Valentin Mitrofanov ◽  
Olga Fedorova ◽  
Andrey Fetisov ◽  
Aidar Murzakaev ◽  
...  

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