Low temperature acoustic characterization of PMN single crystal

2017 ◽  
Vol 122 (8) ◽  
pp. 084103 ◽  
Author(s):  
E. Smirnova ◽  
A. Sotnikov ◽  
S. Ktitorov ◽  
H. Schmidt
2003 ◽  
Vol 58 (7) ◽  
pp. 672-677 ◽  
Author(s):  
Thomas Roßmeier ◽  
Nikolaus Korber

The compounds (NH4)3AsS4· 5 NH3 (1) and (NH4)3SbS4· 8 NH3 (2) were prepared by the reaction of Na3AsS4 and Na3SbS4 with a proton-charged ion exchange material in liquid ammonia and characterized by low temperature single crystal X-ray structure analysis. The ammonium-ammoniates show H3N-H···N-hydrogen bonds between the ammonium ion and ammonia molecules ranging from 1.86 to 2.55 Å (DHA-angles: 145 - 173°) and H3N-H···S-bonds to the thioanions between 2.36 and 2.97 Å (DHA-angles: 130 - 176°). The former of the interactions are responsible for the formation of [(NH3)2H]+, [(NH3)3H]+ and [(NH3)4H]+-complexes, the last two of which were characterized by X-ray analysis for the first time.


2008 ◽  
Vol 55 (3) ◽  
pp. 1228-1231 ◽  
Author(s):  
Sunghwan Kim ◽  
H. J. Kim ◽  
H. Park ◽  
Heedong Kang ◽  
Sih-Hong Doh

2020 ◽  
Vol 18 (41) ◽  
pp. 8386-8394 ◽  
Author(s):  
Alexey V. Kletskov ◽  
Anastasya D. Zatykina ◽  
Mariya V. Grudova ◽  
Anna A. Sinelshchikova ◽  
Mikhail S. Grigoriev ◽  
...  

N-t-Bu-N′,N′′-Disulfonamide-1,3,5-triazinanes were synthesized and studied by X-ray single crystal structure analysis and dynamic low-temperature NMR.


2015 ◽  
Vol 135 (7) ◽  
pp. 733-738 ◽  
Author(s):  
Yasushi Kobayashi ◽  
Yoshihiro Nakata ◽  
Tomoji Nakamura ◽  
Mayumi B. Takeyama ◽  
Masaru Sato ◽  
...  
Keyword(s):  

2015 ◽  
Vol 2 (2) ◽  
pp. 70-73
Author(s):  
Kannan.P ◽  
Thambidurai.S ◽  
Suresh.N

Growth of optically transparent single crystals of thiourea succinic acid (TUSA) was grown successfully from aqueous solution by slow evaporation technique. The crystal structure was elucidated using the single crystal XRD. The various functional groups and the modes of vibrations were identified by FT-IR spectroscopic analysis. The optical absorption studies indicate that the optical transparency window is quite wide making its suitable for NLO applications. Thermal stability of the crown crystal carried out by TGA-DTA analysis.


1997 ◽  
Author(s):  
Anatoliy N. Ivakin ◽  
Darrell R. Jackson

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