Synthesis and characterization of some S,S-Dimethyl-N-pyrimidinylsulfimides

1983 ◽  
Vol 36 (10) ◽  
pp. 2119 ◽  
Author(s):  
DT Hurst
Keyword(s):  
Synthesis And Characterization ◽  
Mass Spectral ◽  
Convenient Synthesis ◽  
Elemental Analyses

A convenient synthesis of several S,S-dimethyl-N-pyrimidin-2 4-ylsulfimides is described. The compounds were characterized by n.m.r., mass spectral and elemental analyses.

Synthesis and characterization of N-glucosylated dithiadiazepine derivatives through carbon-sulfur bond formation

2015 ◽  
Vol 21 (5) ◽  
pp. 269-272 ◽  
Author(s):  
Snehal A. Chavan ◽  
Avinash G. Ulhe ◽  
Baliram N. Berad
Keyword(s):  
Bond Formation ◽  
Synthesis And Characterization ◽  
Mass Spectral ◽  
H Nmr ◽  
Chemical Structures ◽  
Elemental Analyses ◽  
New Compounds ◽  
Sulfur Bond ◽  
C Nmr

AbstractNew 4,7-bis(arylamino)-2-tetra-O-acetyl-β-d-glucopyranosylimino-1,3,5,6-dithiadiazepines were synthesized via reaction of N-tetra-O-acetyl-β-d-glucopyranosyl isocyanodichloride with 1,6-diaryl-2,5-dithio-bis-ureas without using any catalyst. Thus, the synthesis of 7-membered heterocycles containing two sulfur and two nitrogen atoms through carbon-sulfur bond formation was explored. The chemical structures of these new compounds were elucidated by IR, 1H NMR, 13C NMR, mass spectral, and elemental analyses.

Synthesis and Characterization of Palladium(II) Complexes with Substituted Dihydrobenzoimidazo Quinazoline Derivatives

2017 ◽  
Vol 13 (2) ◽  
pp. 1-15
Author(s):  
Rita Bhattacharjee Virupaiah Gayathri
Keyword(s):  
Metal Ion ◽  
Synthesis And Characterization ◽  
Planar Geometry ◽  
Conductivity Measurements ◽  
Spectral Techniques ◽  
Mass Spectral ◽  
Square Planar ◽  
Elemental Analyses ◽  
Quinazoline Derivatives

A series of palladium(II) halo complexes of the types [PdX 2 L 2 ].nH 2 O {n = 0, X = Cl, L = L 2 , L 4 and L 5 ; X = Br, L = L 2 ; n = 1, X = Cl, L = L 1 and L 3 } and Pd 2 X 4 L 3 [X = Br, L = L 1 , L 3 , L 4   and L 5 ] were prepared where L is 6-R-5,6- dihydrobenzoimidazo quinazoline (R-Diq; where R = ethyl: L 1 / n or i-propyl: L 2 , L 3 / n or i-butyl: L 4 , L 5 ) and characterized by elemental analyses, conductivity measurements, TGA, infrared, electronic, NMR and mass spectral techniques. Based    on these studies monomeric/dimeric structure with a square planar geometry around the metal ion was proposed for all the complexes. Some of the complexes were investigated for anti-microbial activity.

The Template Synthesis and Characterization of New Mono- and Dinuclear Podand Schiff Base Complexesof Scandium Group Elements

1998 ◽  
Vol 63 (3) ◽  
pp. 371-377 ◽  
Author(s):  
Emilia Luks ◽  
Wanda Radecka-Paryzek
Keyword(s):  
Schiff Base ◽  
Template Synthesis ◽  
Molar Ratio ◽  
Synthesis And Characterization ◽  
Mass Spectral Data ◽  
Mass Spectral ◽  
H Nmr ◽  
Elemental Analyses ◽  
Materials Used

The partial Schiff base condensation reactions between 2,6-diacetylpyridine and 1,3-phenylenediamine in the presence of scandium(III), yttrium(III) and lanthanum(III) ions as template agents afford new mono- and dinuclear hexadentate complexes of podate type, depending on the molar ratio of starting materials used in the synthesis. They were characterized by IR, UV-VIS, 1H NMR, and mass spectral data as well as by thermogravimetric and elemental analyses.

scholarly journals Synthesis and characterization of barbitones as antimicrobial agents

2006 ◽  
Vol 71 (6) ◽  
pp. 587-591 ◽  
Author(s):  
H.G. Sangani ◽  
K.B. Bhimani ◽  
R.C. Khunt ◽  
A.R. Parikh
Keyword(s):  
Antimicrobial Activity ◽  
Barbituric Acid ◽  
Antimicrobial Agents ◽  
Spectral Studies ◽  
Synthesis And Characterization ◽  
Mass Spectral ◽  
Elemental Analyses ◽  
Bacteria And Fungi

Barbitones (3) were synthesised by the condensation of chalcones (2) with barbituric acid. The structure of the synthesized compounds were assigned on the basis of elemental analyses, IR, NMR and mass spectral studies. All the products were evaluated for their in vitro antimicrobial activity against various strains of bacteria and fungi.

scholarly journals Tetrastyryl-Bodipy Dyes: Convenient Synthesis and Characterization of Elusive Near IR Fluorophores

2009 ◽  
Vol 11 (20) ◽  
pp. 4644-4647 ◽  
Author(s):  
Onur Buyukcakir ◽  
O. Altan Bozdemir ◽  
Safacan Kolemen ◽  
Sundus Erbas ◽  
Engin U. Akkaya
Keyword(s):  
Synthesis And Characterization ◽  
Near Ir ◽  
Convenient Synthesis

Chemistry of Alkoxo Complexes, Part III *Synthesis and Characterization of Some Mono(carboxylato)mono (alkoxo)nickel(II) Complexes

1979 ◽  
Vol 34 (3) ◽  
pp. 459-463 ◽  
Author(s):  
B. P. Baranwal ◽  
G. K. Parashar ◽  
R. C. Mehrotra
Keyword(s):  
Molecular Weight ◽  
Magnetic Susceptibility ◽  
General Formula ◽  
Synthesis And Characterization ◽  
Probable Structure ◽  
Equimolar Ratio ◽  
Elemental Analyses ◽  
Infra Red ◽  
Interchange Reactions

AbstractA number of mono(carboxylato)mono(alkoxo)nickel(II) complexes of the general formula, Ni(OR)(OOCR′), (with R′ = C13H27, C15H35 and C17H35) have been synthesized (where R = Me and Pri) by the reactions of nickel methoxide and isopropoxide with the respective carboxylic acids in equimolar ratio and (where R = Et and But) by alcohol interchange reactions. A study of the molecular weight, infra-red and electronic reflectance spectra and magnetic susceptibility in addition to elemental analyses has been carried out to throw some light on the probable structure of these derivatives.

New Poly(4-Dichloro)Maleimides: III. Synthesis and Characterization of Poly[Ether-Ester-Azomethine-(4-Chloro) Maleimides] and Poly(Azomethin Ester-Aspartimides)

2001 ◽  
Vol 13 (4) ◽  
pp. 269-280 ◽  
Author(s):  
C Gaina ◽  
V Gaina ◽  
M Sava
Keyword(s):  
Weight Loss ◽  
Synthesis And Characterization ◽  
Model Compounds ◽  
Elemental Analyses ◽  
Ether Ester

New poly[(N-ester-azo)-3-ether-4-chloro)maleimides] and poly(azomethin-ester-aspartimides) were synthesized by the reaction of N-[4-(formylphenoxy carboxylphenyl)]-3-(4-formylphenoxy)-4-chloromaleimide (3 a) or N-[4-formylphenoxycarbonylphenyl)maleimide (3 b) with various diamines. IR and elemental analyses confirmed the structures of the resulting polymers. A series of model compounds were synthesized to facilitate confirmation of the polymer structures. The polymers possess inherent viscosities in the range 0.17–0.42 dl g−1, solubility in aprotic dipolar solvents and 5% weight loss at temperatures above 300 °C.

scholarly journals Synthesis and characterization of cis-dioxomolybdenum(VI) complexes having furil as precursor molecule

2012 ◽  
Vol 77 (9) ◽  
pp. 1205-1210
Author(s):  
Devendra Rao ◽  
Hardeo Yadav ◽  
Ashok Yadava ◽  
Sanjay Singh ◽  
Uma Yadav
Keyword(s):  
Oxygen Transfer ◽  
Chelating Agent ◽  
Molar Conductance ◽  
Octahedral Geometry ◽  
Transfer Reactions ◽  
Synthesis And Characterization ◽  
Precursor Molecule ◽  
Elemental Analyses ◽  
Tetraazamacrocyclic Ligands

Synthesis of some new dioxomolybdenum(VI) complexes having general formula [MoO2(mac)](acac)2, (where mac = tetraazamacrocyclic ligands derived from condensation of furil with 1,2-diaminobenzene or 2,3-diaminopyridine and their reaction with ?-diketones) using dioxometal ion as kinetic template are reported. The prepared complexes have been characterized by molar conductance, elemental analyses, infrared and electronic data. The spectral data indicate that ligands act as tetradentate chelating agent. Due to their biological relevance, molybdenum catalyzed oxygen transfer reactions have great interest. All the dioxomolybdenum(VI) complexes have octahedral geometry with six coordination.

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