Yams.

Author(s):  
S. N. Moorthy ◽  
M. S. Sajeev ◽  
R. P. K. Ambrose ◽  
R. J. Anish

Abstract This chapter discusses the extraction of starch from different yam (Dioscorea) species. The physiochemical (biochemical property, amylose and amylopectin content), structural (granular morphology, X-ray diffraction pattern, starch crystallinity, and amylose and amylopectin structure), functional (swelling pattern, solubility, viscosity, rheological properties and retrogradation) and thermal properties of yam starches and their digestibility are described.

Author(s):  
S. N. Moorthy ◽  
M. S. Sajeev ◽  
R. P. K. Ambrose ◽  
R. J. Anish

Abstract This chapter discusses the extraction, physiochemical (chemical composition, amylose and amylopectin content), structural (granular morphology, X-ray diffraction pattern, starch crystallinity, and amylose and amylopectin structure), functional (swelling pattern, solubility, viscosity, rheological properties and retrogradation) and thermal properties, and digestibility of starches from minor tuber crops (e.g., arrowroot, Curcuma spp., Canna edulis [C. indica], Chinese water chestnut [Eleocharis dulcis], chayote [Sechium edule], Pachyrhizus ahipa, Oxalis tuberosa, Arracacia xanthorrhiza, Lilium spp.).


Author(s):  
S. N. Moorthy ◽  
M. S. Sajeev ◽  
R. P. K. Ambrose ◽  
R. J. Anish

Abstract This book chapter outlines the extraction and purification, physiochemical composition (i.e. biochemical content, amylose and amylopectin content), structural properties (i.e. granular morphology, XRD and starch crystallinity, amylose and amylopectin structure), functional properties (i.e. swelling and solubility, viscosity, rheological properties, retrogradation), thermal properties (i.e. DSC, digestibility) of aroids.


Author(s):  
J. M. Galbraith ◽  
L. E. Murr ◽  
A. L. Stevens

Uniaxial compression tests and hydrostatic tests at pressures up to 27 kbars have been performed to determine operating slip systems in single crystal and polycrystal1ine beryllium. A recent study has been made of wave propagation in single crystal beryllium by shock loading to selectively activate various slip systems, and this has been followed by a study of wave propagation and spallation in textured, polycrystal1ine beryllium. An alteration in the X-ray diffraction pattern has been noted after shock loading, but this alteration has not yet been correlated with any structural change occurring during shock loading of polycrystal1ine beryllium.This study is being conducted in an effort to characterize the effects of shock loading on textured, polycrystal1ine beryllium. Samples were fabricated from a billet of Kawecki-Berylco hot pressed HP-10 beryllium.


Author(s):  
Daniel C. Pease

A previous study demonstrated that tissue could be successfully infiltrated with 50% glutaraldehyde, and then subsequently polymerized with urea to create an embedment which retained cytomembrane lipids in sectioned material. As a result, the 180-190 Å periodicity characteristic of fresh, mammalian myelin was preserved in sections, as was a brilliant birefringence, and the capacity to bind OsO4 vapor in the hydrophobic bilayers. An associated (unpublished) study, carried out in co-operation with Drs. C.K. Akers and D.F. Parsons, demonstrated that the high concentration of glutaraldehyde (and urea) did not significantly alter the X-ray diffraction pattern of aldehyde-fixed, myelin. Thus, by itself, 50% glutaraldehyde has little effect upon cytomembrane systems and can be used with confidence for the first stages of dehydration.


2019 ◽  
Vol 15 ◽  
pp. 102605
Author(s):  
Ian Gregory Shuttleworth

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
M. K. Eseev ◽  
A. A. Goshev ◽  
K. A. Makarova ◽  
D. N. Makarov

AbstractIt is well known that the scattering of ultrashort pulses (USPs) of an electromagnetic field in the X-ray frequency range can be used in diffraction analysis. When such USPs are scattered by various polyatomic objects, a diffraction pattern appears from which the structure of the object can be determined. Today, there is a technical possibility of creating powerful USP sources and the analysis of the scattering spectra of such pulses is a high-precision instrument for studying the structure of matter. As a rule, such scattering occurs at a frequency close to the carrier frequency of the incident USP. In this work, it is shown that for high-power USPs, where the magnetic component of USPs cannot be neglected, scattering at the second harmonic appears. The scattering of USPs by the second harmonic has a characteristic diffraction pattern which can be used to judge the structure of the scattering object; combining the scattering spectra at the first and second harmonics therefore greatly enhances the diffraction analysis of matter. Scattering spectra at the first and second harmonics are shown for various polyatomic objects: examples considered are 2D and 3D materials such as graphene, carbon nanotubes, and hybrid structures consisting of nanotubes. The theory developed in this work can be applied to various multivolume objects and is quite simple for X-ray structural analysis, because it is based on analytical expressions.


Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 729
Author(s):  
Junhyub Jeon ◽  
Namhyuk Seo ◽  
Hwi-Jun Kim ◽  
Min-Ha Lee ◽  
Hyun-Kyu Lim ◽  
...  

Fe-based bulk metallic glasses (BMGs) are a unique class of materials that are attracting attention in a wide variety of applications owing to their physical properties. Several studies have investigated and designed the relationships between alloy composition and thermal properties of BMGs using an artificial neural network (ANN). The limitation of the wide-scale use of these models is that the required composition is yet to be found despite numerous case studies. To address this issue, we trained an ANN to design Fe-based BMGs that predict the thermal properties. Models were trained using only the composition of the alloy as input and were created from a database of more than 150 experimental data of Fe-based BMGs from relevant literature. We adopted these ANN models to design BMGs with thermal properties to satisfy the intended purpose using particle swarm optimization. A melt spinner was employed to fabricate the designed alloys. X-ray diffraction and differential thermal analysis tests were used to evaluate the specimens.


2020 ◽  
Vol 7 (21) ◽  
pp. 4197-4221 ◽  
Author(s):  
Francisco Colmenero ◽  
Jakub Plášil ◽  
Jiří Sejkora

The structure, hydrogen bonding, X-ray diffraction pattern and mechanical properties of six important uranyl carbonate minerals, roubaultite, fontanite, sharpite, widenmannite, grimselite and čejkaite, are determined using first principles methods.


1995 ◽  
Vol 80 (7-8) ◽  
pp. 869-872 ◽  
Author(s):  
George D. Guthrie ◽  
David L. Bish ◽  
Robert C. Reynolds

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