scholarly journals The effects of milling time on structure, magnetic properties and microwave absorption capability of strontium lanthanum ferrite compounds

2020 ◽  
Vol 1494 ◽  
pp. 012042
Author(s):  
Mukhtar Effendi ◽  
Endra Nugraha ◽  
Wahyu Tri Cahyanto ◽  
Wahyu Widanarto
2020 ◽  
Vol 855 ◽  
pp. 255-260
Author(s):  
Mukhtar Effendi ◽  
Efi Solihah ◽  
Candra Kurniawan ◽  
Wahyu Tri Cahyanto ◽  
Wahyu Widanarto

The synthesize of Nd3+-strontium hexaferrite magnetic material by the solid-state reaction method has been successfully carried out. This study aims to determine the effect of Nd3+ on the structure, magnetic properties, and microwave absorption capability of the material. Preparation of (1-x)SrO:xNd2O3:6Fe2O3 where x = 0, 10, 20, and 30 mol% using basic material in the form of SrCO3 powder, Nd2O3 powder and Fe3O4 from natural iron sand. The characterization includes the X-Ray Diffraction (XRD) examination to determine the crystal structure, the Scanning Electron Microscope (SEM) for exploring the surface morphology, Vibrating Sample Magnetometer (VSM) for the magnetic properties investigation of material, and Vector Network Analyzer (VNA) for microwave absorption capability analysis. The XRD results show that the addition of Nd3+ doping increases the number of SrNdFeO4 phases. The phase has a tetragonal crystal system that has cell parameters a = b = 3.846 Å, and c = 12.594 Å. The magnetic properties of the material showed that the addition of Nd3+ decreased the saturation and remanence magnetization values, whereas the value of the coercivity field increased. Meanwhile, the best microwave absorption occurs in samples with the addition of Nd3+ as much as 0.3 mol, which results in a reflection loss value of -18.9 dB with a frequency bandwidth of 3.9 GHz.


Author(s):  
Jinxiang Guo ◽  
Zhaofei Tong ◽  
Qihua Liang ◽  
Fangyu Gan ◽  
Lepeng Wei ◽  
...  

2009 ◽  
Vol 23 (06n07) ◽  
pp. 1383-1388 ◽  
Author(s):  
MASLEEYATI YUSOP ◽  
DELIANG ZHANG ◽  
MARCUS WILSON ◽  
NICK STRICKLAND

Al 2 O 3-20 vol % Fe 70 Co 30 composite powders have been prepared by high energy ball milling a mixture of Al 2 O 3 powder and Fe 70 Co 30 alloy powder. The Fe 70 Co 30 alloy powder was also prepared by mechanical alloying of Fe and Co powders using the same process. The effects of milling duration from 8 to 48 hours on microstructure and magnetic properties of the nanostructured composite powders have been studied by means of X-ray Diffractometry (XRD), scanning electron microscopy (SEM) and vibrating sample magnetometry (VSM). It was found that the nanostructured composite powder particles with irregular shapes and Fe 70 Co 30 alloy particles being embedded in them formed after 8 hours of milling. The average grain size of the Al 2 O 3 matrix reduced drastically to less than 18nm after 16 hours of milling. On the other hand, the embedded alloy particles demonstrated almost unchanged average grain size in the range of 14-15nm. Magnetic properties of the powder compacts at room temperature were measured from hysteresis curves, and show strong dependence of the milling time, with the coercivity increasing from 67.1 up to 127.9kOe with increasing the milling time from 8 to 48 hours. The possible microstructural reasons for this dependence are discussed.


2019 ◽  
Vol 13 ◽  
pp. 100393 ◽  
Author(s):  
Martha Rianna ◽  
Timbangen Sembiring ◽  
Marhaposan Situmorang ◽  
Candra Kurniawan ◽  
Anggito P. Tetuko ◽  
...  

2009 ◽  
Vol 423 ◽  
pp. 119-124 ◽  
Author(s):  
Marta López ◽  
M. Elena Gómez ◽  
David Reyes ◽  
K. Ramam ◽  
Ramalinga V. Mangalaraja ◽  
...  

The structure, mechanical and magnetic properties of Cu90Co5Ni5 alloys produced by mechanical alloying and subsequent cold consolidation and sintering behavior, have been investigated. A system of small Co and Ni magnetic particles embedded in the non-magnetic copper matrix were prepared through a mechanical milling process by using a planetary ball mill under argon atmosphere for 20 to 60 h. The morphology and particles size, phase formation and chemical composition of the alloyed powder samples for each milling time were characterized by scanning electron microscope and powder X-ray diffraction techniques, respectively. After milling for 60 h, a supersaturated solid solution with coercive field Hc with maximum value of 235Oe was obtained. The continuous decreasing trend of saturation magnetization (Ms) with increasing of milling time can be explained by the reduction of copper oxide by (CoNi) oxide formation, confirmed by powder XRD patterns. The XRD analyses of the as-milled samples revealed that the Bragg peaks of FCC-Co changed partially to HCP-Co on increasing the milling time. Cu90Co5Ni5 powders cold consolidated and sintered at 650°C for 1h segregated mainly into two-phases of mixed (fcc,hc)-Co and fcc-CuNi. After sintering, the mechanical properties for 60h milling reached its optimum, 26HV in hardness corresponding to 250MPa as compressive strength. TEM microanalysis of sintered alloys revealed Co cluster of 2 to 5 nm in size separated each one by 10 to 20 nm in size. The variation of magnetic properties and its dependence on structural-precipitation change with milling time are discussed.


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