scholarly journals Synthesis of Foam Glass-Ceramic from CRT Panel Glass using One-step Powder Sintering

Author(s):  
Hao Yuan ◽  
Hongcheng Wu ◽  
Jie Guan
2013 ◽  
Vol 45 (3) ◽  
pp. 331-339
Author(s):  
A. Faeghi-Nia

An Apatite-Wollastonite-Phlogopite glass-ceramic composite, was developed by sintering and crystallization of the powdered glass. The non-isothermal and isothermal sintering kinetics were studied for this glass-ceramic. Hot-stage microscopy (HSM) measurements demonstrated that it is possible to sinter and crystallize this glass-ceramic with 80% relative density. The activation energy of sintering was analyzed using previously reported model of sintering and it was obtained Q=193.83 KjmolK-1. Also it was shown that the microstructure of sample is a function of particle size distribution.


2008 ◽  
Vol 65 (3-4) ◽  
pp. 74-76 ◽  
Author(s):  
A. S. Apkar’yan ◽  
V. G. Khristyukov ◽  
G. V. Smirnov

2011 ◽  
Vol 3 (1) ◽  
pp. 69-74 ◽  
Author(s):  
Federico Smeacetto ◽  
Milena Salvo ◽  
Andrea Ventrella ◽  
Stefano Rizzo ◽  
Monica Ferraris

2008 ◽  
Vol 22 (5) ◽  
pp. 999-1003 ◽  
Author(s):  
Vladimir I. Vereshagin ◽  
Svetlana N. Sokolova

Author(s):  
Xinxing Li ◽  
Zirun Yang ◽  
Hongxia Wang ◽  
Lin Li ◽  
Naifei Ren

Abstract ZrO2/Ni3Al-Ni3Al double-layer coating on stainless steel was prepared by powder sintering one-step forming process. The surface-interface morphologies, chemical element distribution and phase compositions of the coatings before and after thermal oxidation or hot corrosion were analyzed using scanning electron microscope (SEM), energy dispersive spectrometer (EDS) and X-ray diffractometer (XRD). The microstructure of the coating was Ni3Al matrix with dispersed ZrO2 particles, which was pure and compacted. The Ni3Al intermediate layer compactly formed between stainless steel substrate and ZrO2/Ni3Al composite coating, with good metallurgical bonding interfaces. The ZrO2/Ni3Al-Ni3Al double-layer coating exhibited a relatively high outmost microhardness of about 500 HV, and then gradually decreased from the coating to the substrate. When thermal oxidized or hot corroded at 1050 ℃, a mixed oxide layer of NiO, Al2O3 and NiAl2O4 formed on the coating surface, which effectively acted as a diffusion barrier for oxygen and corrosive substances, and thus demonstrated the good protective effect of ZrO2/Ni3Al coating.


2018 ◽  
Vol 280 ◽  
pp. 83-89 ◽  
Author(s):  
Siti Rohani Zainudin ◽  
S.A. Syed Nuzul Fadzli ◽  
Dewi Suriyani Che Halin ◽  
Mohd Reusmaazran Yusof ◽  
Johar Banjuraizah ◽  
...  

Bioactive glass and glass-ceramics have a huge interest in biomedical application due to their high biocompatibility and bioactive property. In this study, macro porous glass-ceramic based on 51.26% SiO2 - 36.56% CaO - 11.83% P2O5 and 42.11% SiO2 - 18.42% CaO - 29.82% Na2O - 9.65% P2O5 (in mol%) were prepared via sol-gel synthesis and powder sintering method. Sodium nitrate was used as the precursor for sodium oxide (Na2O) composition in the sol-gel glass. Effect of sodium nitrate addition on the sintered glass (glass-ceramic) properties were studied. The stabilized gel-glasses obtained were compacted into pellets and sintered at 1000 °C for 3 hours. It was found that, Na-contained glass-ceramic (Na-GC) crystallized at 71.5% due to increase in sodium-related crystalline phases. Na-GC showed 72.98% of apparent porosity and densified at 27.02% with macro porous structure with pore sizes in the range of 22.4 μm to 302 μm. The macro porous structure of Na-GC was obtained due to the foaming effect occurred during sintering. Flux effect occurred during sintering also resulted in relatively high compressive strength of Na-GC at 21.53 MPa. The macro porous Na-GC also proved to be bioactive as apatite-like structures were deposited on its surface after immersed into SBF solution for 14 days. The prepared macro porous Na-GC has high potential to be used as a scaffold material in biomedical application due to combination of suitable macro-pore size range, bioactive and has sufficient mechanical strength.


2015 ◽  
Vol 71 (11-12) ◽  
pp. 413-417 ◽  
Author(s):  
A. S. Apkar’yan ◽  
T. A. Gubaidulina ◽  
O. V. Kaminskaya

2019 ◽  
Vol 44 (19) ◽  
pp. 4857 ◽  
Author(s):  
Longfei Zhang ◽  
Yiguang Jiang ◽  
Zaiyang Wang ◽  
Chengfeng Yuan ◽  
Meisong Liao ◽  
...  
Keyword(s):  

2010 ◽  
Vol 105-106 ◽  
pp. 765-768 ◽  
Author(s):  
Dong Sheng Lv ◽  
Xiu Hua Li ◽  
Lei Wang ◽  
Juan Juan Du ◽  
Jie Zhang

Insulation effect and mechanical performance of foam glass depend, to a large extent, on foam structure. Hence understanding foam formation is not only a problem of significant fundamental interest but also of tremendous practical impact. In this paper, foam growth was modeled comparing to grain growth theory in sintering. TG-DTG analysis of carbon black indicated that pre-oxidation took place prior to foaming temperature. Furthermore effects of heating rate and particle size of carbon black on foam structure have been taken into account. Several borosilicate foam glasses were fabricated by powder sintering process at different heating rates using carbon black of different particle sizes as foaming agent, respectively. It was found that increasing the heating rate tended to decrease the pre-oxidation of carbon black resulting in inhomogeneous foam distribution. Foam structure of sample heated at a rate of 8°C/min using carbon black with particle size of 0.15mm was optimal.


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