High-resolution x-ray diffraction study of single crystals of lead zirconate titanate

2011 ◽  
Vol 84 (2) ◽  
Author(s):  
S. Gorfman ◽  
D. S. Keeble ◽  
A. M. Glazer ◽  
X. Long ◽  
Y. Xie ◽  
...  
1995 ◽  
Vol 10 (7) ◽  
pp. 1582-1584 ◽  
Author(s):  
Fei Fang ◽  
Xiaowen Zhang

The ordering behavior of La-modified lead zirconate titanate relaxor (PLZT 9/65/35) was investigated by use of an x-ray diffractometer (XRD) and high-resolution transmission electron microscopy (HRTEM). It was shown that a {h + 1/2, k + 1/2, 0}-type superlattice exists both in the x-ray diffraction pattern and selected area electron diffraction (SAED) image. High-resolution electron micrographs further demonstrated the existence of the superlattice and exposed the ordered and disordered regions in the lattice level. A model referring to an A-site body-centered pseudo-cubic superstructure was proposed.


2001 ◽  
Vol 84 (12) ◽  
pp. 2921-2929 ◽  
Author(s):  
Alexandre E. Glazounov ◽  
Hans Kungl ◽  
Jan-Thorsten Reszat ◽  
Michael J. Hoffmann ◽  
Arnd Kolleck ◽  
...  

2007 ◽  
Vol 90 (26) ◽  
pp. 262905 ◽  
Author(s):  
Satoko Osone ◽  
Yoshiro Shimojo ◽  
Kyle Brinkman ◽  
Takashi Iijima ◽  
Keisuke Saito

2005 ◽  
Vol 902 ◽  
Author(s):  
Lingjuan Che ◽  
Yongping Ding ◽  
Jinrong Cheng ◽  
Chao Chen ◽  
Zhongyan Meng

AbstractLead Zirconate Titanate (PZT) powders have been synthesized by a hydrothermal method at the processing temperatures of 120-220 °C for 1.5-50 hours, based on the reaction of Pb(CH3COOH)2·3H2O, ZrOCl2·8H2O, Ti(C4H9O)4 and KOH. Hydrothermally treated PZT powders were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transformation infrared (FTIR) techniques respectively. The influences of hydrothermal synthesize conditions on the crystalline structure and the morphology of PZT particles were investigated. Crystallized PZT powders could be synthesized at the KOH concentration of >2.5 mol/l.


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