A program for refinement of lattice parameters and strain determination using Kossel diffraction patterns

2016 ◽  
Vol 49 (1) ◽  
pp. 322-329 ◽  
Author(s):  
A. Morawiec

The Kossel diffraction technique is well suited for investigating crystal lattices. Progress in digital recording of images opens the opportunity for simplification and improvement of the examination of Kossel patterns. Such patterns can be processed immediately after recording if appropriate computer programs are available. To provide such a tool, a new Windows-based software for computer-assisted analysis of Kossel patterns has been developed. With its easy-to-operate user interface, the program is intended to facilitate refinement of lattice parameters and determination of elastic strains. The refinement is based on matching experimental and geometrically simulated patterns, whereas the strain is obtained by matching Kossel line profiles in similar experimental patterns. The software is capable of simultaneous handling of multiple patterns.

2014 ◽  
Vol 70 (a1) ◽  
pp. C1454-C1454
Author(s):  
Hejing Wang ◽  
Ting Li ◽  
Ling Wang ◽  
Zhao Zhou ◽  
Lei Yuan

Lattice and diffraction are two relating aspects of a crystal. The former reflects the nature of a crystal and the latter describes the basic feature of a crystal. A lattice possesses points and rows two basic characteristics. Great attention has been paid to the points and their distances and directions (angles) they form since the early time of crystallography. Starting from lattice points people have already revealed and found so many regulations in crystals and made great progresses in crystallography. What about the lattice rows? Starting from the geometric relations of reciprocal lattice, we propose six general formulae [1] to describe the relationships between the lattice row distance, the Miller indices h, k, l and the lattice parameters for all crystal systems along any direction. This, like the lattice points, establishes the foundation of the row-indexing, row-refinement of lattice parameters and row-determination of incidence direction theoretically. It is a new method from the lattice row distance to the Miller indices, to the lattice parameters or to the incidence direction. Five steps are optimized for the procedure of "Row-indexing" or "Row-refinement". For example, the procedure of row-indexing is described as 1) measurement of row distance; 2) calculation of row distance; 3) comparison of the measured with the calculated row distances; 4) indexing, and 5) check according to the crystallographic regulations. In respect to diffraction patterns, a series of diffraction spots (points) comprise row(s) and arrange into a series of parallel "lines". When diffraction is strong, diffraction spots are isolated and sharp. However, when diffraction is weak, those spots are obscure or gloomy and often distorted into elongation, asymmetry, deformation, etc. This leads to the outstanding of the rowing "lines" relatively and hence, the row-distance formulae are able to be utilized to structure analysis for those "linear diffraction patterns".


Author(s):  
Donald L. Gibbon ◽  
Beverly J. Komlosi

Incomplete powder electron diffraction patterns are traditionally difficult to interpret and are usually simply overlooked as being a sort of not-veryuseful background noise in the flow of data gathered in sample analysis. However, if techniques can be developed to systematize the information contained in those patterns, it can be a major contribution to the unravelling of complex materials problems. The following simple techniques are applied in our laboratories:1. Patterns are recorded on Technical Pan 35mm film, using a double-exposure to obtain a well-exposed record of the rings and spots; a very small central spot is exposed at much lower intensity with the beam stop removed. The film is developed at high contrast in HC-110, dilution F (1:9).


2007 ◽  
Vol 40 (3) ◽  
pp. 618-622 ◽  
Author(s):  
A. Morawiec

A package of computer programs for refinement of lattice parameters based on convergent-beam electron diffraction (CBED) patterns has been developed. The package is intended to facilitate the measurement of local elastic strains. The strain or lattice parameters are determined by matching experimental and simulated central disks of CBED patterns. The kinematical simulation is used in the primary fitting. In some cases, further refinement by means of dynamical simulation can be applied. User-specified strain components, camera lengths and voltage can be fitted. The software is not limited to any particular material or structure. It is capable of simultaneous matching of multiple patterns originating from the same sample location. The use of a number of different strategies allows for the verification of results and for checking their reliability. Operation of the software is controlledviaa Windows user interface.


1975 ◽  
Vol 43 (2) ◽  
pp. 136-141 ◽  
Author(s):  
Jerzy Szewczykowski ◽  
Stanislaw Sliwka ◽  
Adam Kunicki ◽  
Jolanta Korsak-Sliwka ◽  
Jacek Dziduszko ◽  
...  

✓The effect of prolonged mannitol infusion upon intraventricular pressure was investigated with the aid of a specially-designed automatic digital recording system; the data recorded were processed off-line by a minicomputer. The character of the pressure curves is thought to result from interaction between the mannitol effect and the observed system's shifting equilibrium position, which is caused by other factors. The character of the pressure curves prior to mannitol infusion must be taken into consideration in estimating the actual effect of the drug; the authors suggest that in certain cases it might be possible to decrease further the rate of mannitol administration. The advantages of statistical approach to the evaluation of intracranial pressure variations are discussed.


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