Accurate full-chip estimation of power map, current densities and temperature for EM assessment

Author(s):  
Marko Chew ◽  
Ara Aslyan ◽  
Jun-ho Choy ◽  
Xin Huang
Keyword(s):  
Author(s):  
W.R. Bottoms ◽  
G.B. Haydon

There is great interest in improving the brightness of electron sources and therefore the ability of electron optical instrumentation to probe the properties of materials. Extensive work by Dr. Crew and others has provided extremely high brightness sources for certain kinds of analytical problems but which pose serious difficulties in other problems. These sources cannot survive in conventional system vacuums. If one wishes to gather information from the other signal channels activated by electron beam bombardment it is necessary to provide sufficient current to allow an acceptable signal-to-noise ratio. It is possible through careful design to provide a high brightness field emission source which has the capability of providing high currents as well as high current densities to a specimen. In this paper we describe an electrode to provide long-lived stable current in field emission sources.The source geometry was based upon the results of extensive computer modeling. The design attempted to maximize the total current available at a specimen.


Author(s):  
R. Sharma ◽  
B.L. Ramakrishna ◽  
N.N. Thadhani ◽  
D. Hianes ◽  
Z. Iqbal

After materials with superconducting temperatures higher than liquid nitrogen have been prepared, more emphasis has been on increasing the current densities (Jc) of high Tc superconductors than finding new materials with higher transition temperatures. Different processing techniques i.e thin films, shock wave processing, neutron radiation etc. have been applied in order to increase Jc. Microstructural studies of compounds thus prepared have shown either a decrease in gram boundaries that act as weak-links or increase in defect structure that act as flux-pinning centers. We have studied shock wave synthesized Tl-Ba-Cu-O and shock wave processed Y-123 superconductors with somewhat different properties compared to those prepared by solid-state reaction. Here we report the defect structures observed in the shock-processed Y-124 superconductors.


Author(s):  
T. F. Kelly ◽  
P. J. Lee ◽  
E. E. Hellstrom ◽  
D. C. Larbalestier

Recently there has been much excitement over a new class of high Tc (>30 K) ceramic superconductors of the form A1-xBxCuO4-x, where A is a rare earth and B is from Group II. Unfortunately these materials have only been able to support small transport current densities 1-10 A/cm2. It is very desirable to increase these values by 2 to 3 orders of magnitude for useful high field applications. The reason for these small transport currents is as yet unknown. Evidence has, however, been presented for superconducting clusters on a 50-100 nm scale and on a 1-3 μm scale. We therefore planned a detailed TEM and STEM microanalysis study in order to see whether any evidence for the clusters could be seen.A La1.8Sr0.2Cu04 pellet was cut into 1 mm thick slices from which 3 mm discs were cut. The discs were subsequently mechanically ground to 100 μm total thickness and dimpled to 20 μm thickness at the center.


Author(s):  
I-Fei Tsu ◽  
D.L. Kaiser ◽  
S.E. Babcock

A current theme in the study of the critical current density behavior of YBa2Cu3O7-δ (YBCO) grain boundaries is that their electromagnetic properties are heterogeneous on various length scales ranging from 10s of microns to ˜ 1 Å. Recently, combined electromagnetic and TEM studies on four flux-grown bicrystals have demonstrated a direct correlation between the length scale of the boundaries’ saw-tooth facet configurations and the apparent length scale of the electrical heterogeneity. In that work, enhanced critical current densities are observed at applied fields where the facet period is commensurate with the spacing of the Abrikosov flux vortices which must be pinned if higher critical current density values are recorded. To understand the microstructural origin of the flux pinning, the grain boundary topography and grain boundary dislocation (GBD) network structure of [001] tilt YBCO bicrystals were studied by TEM and HRTEM.


Author(s):  
M. R. McCartney ◽  
J. K. Weiss ◽  
David J. Smith

It is well-known that electron-beam irradiation within the electron microscope can induce a variety of surface reactions. In the particular case of maximally-valent transition-metal oxides (TMO), which are susceptible to electron-stimulated desorption (ESD) of oxygen, it is apparent that the final reduced product depends, amongst other things, upon the ionicity of the original oxide, the energy and current density of the incident electrons, and the residual microscope vacuum. For example, when TMO are irradiated in a high-resolution electron microscope (HREM) at current densities of 5-50 A/cm2, epitaxial layers of the monoxide phase are found. In contrast, when these oxides are exposed to the extreme current density probe of an EM equipped with a field emission gun (FEG), the irradiated area has been reported to develop either holes or regions almost completely depleted of oxygen. ’ In this paper, we describe the responses of three TMO (WO3, V2O5 and TiO2) when irradiated by the focussed probe of a Philips 400ST FEG TEM, also equipped with a Gatan 666 Parallel Electron Energy Loss Spectrometer (P-EELS). The multi-channel analyzer of the spectrometer was modified to take advantage of the extremely rapid acquisition capabilities of the P-EELS to obtain time-resolved spectra of the oxides during the irradiation period. After irradiation, the specimens were immediately removed to a JEM-4000EX HREM for imaging of the damaged regions.


The Analyst ◽  
2020 ◽  
Vol 145 (1) ◽  
pp. 122-131 ◽  
Author(s):  
Wanda V. Fernandez ◽  
Rocío T. Tosello ◽  
José L. Fernández

Gas diffusion electrodes based on nanoporous alumina membranes electrocatalyze hydrogen oxidation at high diffusion-limiting current densities with fast response times.


2015 ◽  
Vol 3 (1) ◽  
pp. 9-18
Author(s):  
Ali J. Jaeel

Chicken manure wastewaters are increasingly being considered a valuable resource of organic compounds. Screened chicken manure was evaluated as a representative solid organic waste. In this study, electricity generation from livestock wastewater (chicken manure) was investigated in a continuous mediator-less horizontal flow microbial fuel cell with graphite electrodes and a selective type of membrane separating the anodic and cathodic compartments of MFC from each other. The performance of MFC was evaluated to livestock wastewater using aged anaerobic sludge. Results revealed that COD and BOD removal efficiencies were up to 88% and 82%, respectively. At an external resistance value of 150 Ω, a maximum power and current densities of 278 m.W/m2 and 683 mA/m2, respectively were obtained, hence MFC utilizing livestock wastewater would be a sustainable and reliable source of bio-energy generation .


1993 ◽  
Vol 28 (11-12) ◽  
pp. 473-480
Author(s):  
A. Heduit ◽  
B. Martin ◽  
I. Duchamp ◽  
D. R. Thevenot

Gold and platinum were compared to ascertain how they expressed a stabilized potential in activated sludge. The comparison was based on electrochemical determination of the electron transfer rate (i.e. equilibrium exchange current density) and recording of potentials against time. When both metals are treated in the same way, platinum gives equilibrium exchange current densities approx. 10 times higher than gold, both in aerated activated sludge and in treated water. For platinum, the equilibrium exchange current densities range from 0.1 to 0.25 µA/cm2 immediately after polishing and decrease during prolonged contact with activated sludge subjected to alternating aeration/anoxia sequences. The lower kinetics of electron transfer on gold go together with significant differences in response:- In an aerobic medium a gold electrode potential is lower than that of a platinum electrode. In a strongly anaerobic medium, the reverse is true. Consequently, the amplitude of the potential variation between aerobic and anaerobic media is smaller for gold than for platinum. Under our experimental conditions this amplitude was approx 350 mV for gold and 850 mV for platinum.- The slopes of the linear relationships between potential and pH or potential and the logarithm of the dissolved oxygen concentration are two or three times greater for platinum than for gold. Although the values obtained with platinum electrodes cannot represent a veritable equilibrium state, the platinum electrode zero-current potential would seem to be far more sensitive to variations in the medium than that of the gold electrode; it is, therefore, more suitable for use in activated sludge.


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