Effect of pickling and mechanical surface treatment methods on adhesion strength of Ti oxide layer formed on Titanium alloy substrate

Author(s):  
S. Izman ◽  
Mohammed Rafiq Abdul-Kadir ◽  
Mahmood Anwar ◽  
E. M. Nazim ◽  
E. K. Khor ◽  
...  
2010 ◽  
Vol 146-147 ◽  
pp. 1621-1630 ◽  
Author(s):  
Sudin Izman ◽  
Mohammed Rafiq Abdul Kadir ◽  
Mahmood Anwar ◽  
Engku Mohammad Nazim ◽  
Low Yik Kuan ◽  
...  

Titanium alloys are commonly used in biomedical application in hard tissues replacement especially for knee and hip implants. Surface modifications are required prior to diamond coating process for improving the tribological and wear properties of the titanium alloy. In this study, experiments were carried out to investigate the effects of different pickling times as well as temperature on the adhesion strength of oxide layer formed on the Titanium alloy after oxidation process. The aqueous acid solution of HF and HNO3 was used as a pickling solution. The chemical pretreatment was carried out at 4 levels by varying the pickling time as well as temperature. All treated samples were thermally oxidized in a fixed parameters at 900 °C for 25 hours. Surface morphology, oxide layer thickness and adhesion strength were measured after each step using FESEM and Blast Wear Tester (BWT). It was revealed that the thickness of oxide layer increases with pickling time but the adhesion strengths become weaker. It was also found that the adhesion strength of oxide layer formed on Ti substrate surface increases with the increase of temperature while the thickness of the oxide layer decreased within 40oC pickling temperature.


2020 ◽  
Vol 990 ◽  
pp. 44-49
Author(s):  
Xing Sheng Lao ◽  
Xu Feng Zhao ◽  
Yong Liu ◽  
Chun Hui Dai ◽  
Wei Jian Lv

In order to study the effect of microarc oxidation modification treatment on the friction properties of titanium alloy surface, the surface treatment layer of Ti-6Al-4V ELI specimen modified by Microarc oxidation surface was sampled, the surface layer hardness, roughness and treatment layer thickness were tested, the microscopic morphology was analyzed, The friction tests of TC4 substrate and micro-arc oxidation treatment surface disc with 25% glass fiber, 15% fiberglass +5% graphite and 60% tin bronze reinforced PTFE pin were carried out, and the results showed that the thickness increased slightly and the surface layer hardness increased by about 75% after the micro-arc oxidation surface modification treatment. Compared with the substrate, the surface roughness is obviously improved, and the friction coefficient of the surface treatment specimen is similar to that of the TC4 titanium alloy substrate, but the wear amount is higher than that of the TC4 titanium alloy substrate.


Author(s):  
Patiphan Juijerm ◽  
Berthold Scholtes

Today, aluminum alloys are being considered as substitutes for many automotive parts made from steels because of the growing interest in producing lightweight vehicles. Consequently, it is crucial to understand the fatigue lifetime—the property itself and its behavior—of aluminum alloys, and to clarify its capacities at both room temperature and 1001 elevated temperatures. In particular, the aluminum alloys in the AA5xxx (non-precipitation-hardenable) and AA6xxx (precipitation-hardenable) series are very similar to those found in automotive industries, and are both frequently mentioned and the focus of studies. The satisfactory fatigue lifetime and the improved strength of aluminum alloys make them a strong candidate for automotive industries. This article focuses upon the fatigue property and behavior of aluminum alloys at room temperature and elevated temperatures. Then, the focus will shift to the concept of mechanical surface treatment, the so-called deep-rolling process, which can be used to improve the fatigue lifetime of aluminum alloys. The effects of a mechanical surface treatment on the fatigue properties and behavior of the aluminum alloys AA5083 and AA6110, and the residual stress stability at room temperature and elevated temperatures has been discussed. Moreover, modified deep-rolling processes, i.e., deep-rolling followed by an appropriate annealing process and high-temperature deep-rolling, have been elaborated upon in this article.


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