Dependence of Shear Strength of Adhesive Conductive Joints on Adhesive Modification with the Silver Nanoparticles and Climatic Aging

Author(s):  
Pavel Mach
Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 5941
Author(s):  
Steve Lien-Chung Hsu ◽  
Yen-Ting Chen ◽  
Meng-Liang Chen ◽  
In-Gann Chen

A silver precursor (silver 2-ethylhexanoate) and silver nanoparticles were synthesized and used to prepare a low sintering temperature nano-silver paste (PM03). We optimized the amount of silver 2-ethylhexanoate added and the sintering temperature to obtain the best performance of the nano-silver paste. The relationship between the microstructures and properties of the paste was studied. The addition of silver 2-ethylhexanoate resulted in less porosity, leading to lower resistivity and higher shear strength. Thermal compression of the paste PM03 at 250 °C with 10 MPa pressure for 30 min was found to be the proper condition for copper-to-copper bonding. The resistivity was (3.50 ± 0.02) × 10−7 Ω∙m, and the shear strength was 57.48 MPa.


2006 ◽  
Vol 942 ◽  
Author(s):  
A. J. Murray ◽  
P. Jaroenapibal ◽  
B. Koene ◽  
S. Evoy

ABSTRACTWe report the development of a metallic colloid sintering process enabling the creation of bonding layers at moderate temperatures ranging from 150°C to 300°C, and pressures lower than 5MPa. This colloidal n-propyl acetate dispersion of Ag nanoparticles, having an average size distribution of 103nm, was used in sintered interconnect fabrication. Open air sintering of a 10um thick film resulted in an average resistivity of 0.20·10−6 −0.30·10−6 Ωm. Film resistances were found to be as low as 0.18·10−6 Ωm. Independent test varying either pressure or temperature were correlated to ultimate shear strength and modulus. The analysis of a 1cm2 bond area resulted in a peak shear strength of 5.83 MPa and shear modulus of 346 MPa which occurred following bonding at 300°C with a pressure of 4.219 MPa.


2014 ◽  
Vol 10 (1) ◽  
pp. 293-298 ◽  
Author(s):  
Zbyněk Pešina ◽  
Vít Vykoukal ◽  
Marián Palcut ◽  
Jiří Sopoušek

2019 ◽  
Vol 107 (3) ◽  
pp. 305
Author(s):  
Mengmei Geng ◽  
Yuting Long ◽  
Tongqing Liu ◽  
Zijuan Du ◽  
Hong Li ◽  
...  

Surface-enhanced Raman Scattering (SERS) fiber probe provides abundant interaction area between light and materials, permits detection within limited space and is especially useful for remote or in situ detection. A silver decorated SERS fiber optic probe was prepared by hydrothermal method. This method manages to accomplish the growth of silver nanoparticles and its adherence on fiber optic tip within one step, simplifying the synthetic procedure. The effects of reaction time on phase composition, surface plasmon resonance property and morphology were investigated by X-ray diffraction analysis (XRD), ultraviolet-visible absorption spectrum (UV-VIS absorption spectrum) and scanning electron microscope (SEM). The results showed that when reaction time is prolonged from 4–8 hours at 180 °C, crystals size and size distribution of silver nanoparticles increase. Furthermore, the morphology, crystal size and distribution density of silver nanoparticles evolve along with reaction time. A growth mechanism based on two factors, equilibrium between nucleation and growth, and the existence of PVP, is hypothesized. The SERS fiber probe can detect rhodamin 6G (R6G) at the concentration of 10−6 M. This SERS fiber probe exhibits promising potential in organic dye and pesticide residue detection.


1992 ◽  
Vol 05 (03) ◽  
pp. 100-103 ◽  
Author(s):  
G. Jean ◽  
J. K. Roush ◽  
R. M. DeBowes ◽  
E. M. Gaughan ◽  
J. Kirpensteijn

SummaryThe holding power and holding power per mm bone width of 4.5 mm and 5.5 mm cortical and 6.5 mm cancellous orthopaedic screws were obtained by tensile load-to-failure studies in excised metacarpal and metatarsal bones of young female Holstein calves. Holding power and holding power per mm bone width of 6.5 mm orthopaedic screws were significantly greater than those of 4.5 and 5.5 mm orthopaedic screws in the diaphysis and metaphysis. Significant differences were not detected between holding power and holding power per mm bone width of 4.5 and 5.5 mm orthopaedic screws. The holding power was not different between metacarpi and metatarsi. The limiting factor in all tests of holding power was the shear strength of the bone. We found that 6.5 mm orthopaedic screws have the greatest holding power in the metacarpal and metatarsal bones of young calves.This study compares the holding power of 4.5 mm and 5.5 mm cortical and 6.5 mm cancellous orthopaedic screws in excised metacarpal and metatarsal bones from young female Holstein calves. We found that 6.5 mm orthopaedic screws have the greatest holding power.


2020 ◽  
Author(s):  
Iván A. Contreras ◽  
Jed D. Greenwood ◽  
Aaron T. Grosser

2020 ◽  
Vol 9 (4) ◽  
pp. e31942727
Author(s):  
João Gabriel Missia da Silva ◽  
Pedro Nicó de Medeiros ◽  
Denise Ransolin Soranso ◽  
Vinicius Peixoto Tinti ◽  
José Tarcísio da Silva Oliveira ◽  
...  

The aim of this study was to evaluate the influence of anatomical characteristics on the adhesion performance of Vatairea sp., Paulownia sp., Aspidosperma populifolium and Tectona grandis wood. Specimens for anatomical, physical and mechanical analyzes were produced from tangentially oriented boards. The treatments were joint glued from pieces of the same anatomical orientation (radial and tangential), evaluated for shear strength and glue line failure. The Vatairea sp wood had the highest specific gravity (0.74 g cm-3) and the Paulownia sp (0.34 g cm-3) wood was smaller. Aspidosperma populifolium species showed the highest shear strength in the glue line in the tangential and radial faces. The anatomical variables with higher influence on the wood adhesion process were pith ray cells and especially fibers that exhibit the greatest correlation with the shear strength of the glue line.


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