Effect of Vacuum Heat Treatment on Electron-Beam-Irradiation-Cured Polycarbosilane Fibers

2001 ◽  
Vol 84 (1) ◽  
pp. 111-116 ◽  
Author(s):  
Toshio Shimoo ◽  
Masahiro Ito ◽  
Kiyohito Okamura ◽  
Michio Takeda
2007 ◽  
Vol 87 (2) ◽  
pp. 327-331 ◽  
Author(s):  
H. Ou ◽  
T.P. Rørdam ◽  
K. Rottwitt ◽  
F. Grumsen ◽  
A. Horsewell ◽  
...  

2016 ◽  
Vol 68 (1) ◽  
pp. 83-92 ◽  
Author(s):  
Apichate Maneewong ◽  
Baek Seok Seong ◽  
Eun Joo Shin ◽  
Jeong Seog Kim ◽  
Varavuth Kajornrith

2017 ◽  
Vol 381 ◽  
pp. 64-68
Author(s):  
Dae Kyun Hwang ◽  
Jeong Ho Kim ◽  
Oh Hyeong Kwon ◽  
Won Ho Park ◽  
Dong Hwan Cho

In the present work, lignin extracted from black liquor, which is industrial waste of pulp manufacturing. The extracted lignin was irradiated at various electron beam intensities from 100 to 1000 kGy. Also, the extracted lignin was thermally stabilized by heat treatment process. The characteristics of the stabilized and irradiated lignin materials were examined by means of TGA, ATR-FTIR, EA, and SEM. The ATR-FTIR result shows that both stabilized and irradiated lignin samples exhibit the decrease of characteristic absorption peaks, indicating the presence of guaiacyl and syringyl groups in the lignin structure. It reveals that the irradiation done to the ‘as-extracted’ lignin with appropriate electron beam intensity provides an efficiency as thermal stabilization of the lignin, suggesting that electron beam irradiation may apply directly to the extracted lignin, prior to carbonization the lignin without thermal stabilization process.


2017 ◽  
Vol 23 (S1) ◽  
pp. 2046-2047 ◽  
Author(s):  
T. Kimura ◽  
M. Ishimaru ◽  
M. Okugawa ◽  
R. Nakamura ◽  
H. Yasuda

Author(s):  
B. L. Armbruster ◽  
B. Kraus ◽  
M. Pan

One goal in electron microscopy of biological specimens is to improve the quality of data to equal the resolution capabilities of modem transmission electron microscopes. Radiation damage and beam- induced movement caused by charging of the sample, low image contrast at high resolution, and sensitivity to external vibration and drift in side entry specimen holders limit the effective resolution one can achieve. Several methods have been developed to address these limitations: cryomethods are widely employed to preserve and stabilize specimens against some of the adverse effects of the vacuum and electron beam irradiation, spot-scan imaging reduces charging and associated beam-induced movement, and energy-filtered imaging removes the “fog” caused by inelastic scattering of electrons which is particularly pronounced in thick specimens.Although most cryoholders can easily achieve a 3.4Å resolution specification, information perpendicular to the goniometer axis may be degraded due to vibration. Absolute drift after mechanical and thermal equilibration as well as drift after movement of a holder may cause loss of resolution in any direction.


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