GRAIN REFINEMENT AND MICROSTRUCTURE EVOLUTION IN ALUMINUM A2618 ALLOY BY HIGH-PRESSURE TORSION

2016 ◽  
Vol 78 (6-9) ◽  
Author(s):  
Intan Fadhlina Mohamed ◽  
Seungwon Lee ◽  
Kaveh Edalati ◽  
Zenji Horita ◽  
Shahrum Abdullah ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Saturation Level ◽  
Microstructural Refinement ◽  
Average Grain Size

This work presents a study related to the grain refinement of an aluminum A2618 alloy achieved by High-Pressure Torsion (HPT) known as a process of Severe Plastic Deformation (SPD). The HPT is conducted on disks of the alloy under an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm at room temperature. The HPT processing leads to microstructural refinement with an average grain size of ~250 nm at a saturation level after 5 turns. Gradual increases in hardness are observed from the beginning of straining up to a saturation level. This study thus suggests that hardening due to grain refinement is attained by the HPT processing of the A2618 alloy at room temperature.

Microstructural Evolution in an Al-6061 Alloy Processed by High-Pressure Torsion and Rapid Annealing

2010 ◽  
Vol 667-669 ◽  
pp. 223-228 ◽  
Author(s):  
Aicha Loucif ◽  
Roberto B. Figueiredo ◽  
Thierry Baudin ◽  
François Brisset ◽  
Terence G. Langdon
Keyword(s):  
Grain Size ◽  
High Pressure ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Al 6061 ◽  
Fine Grain ◽  
Grain Structures ◽  
Average Grain Size ◽  
Continuous Recrystallization

The processing of bulk metals through the application of severe plastic deformation provides the opportunity for introducing significant grain refinement into bulk solids. In the present investigation, an aluminum alloy (Al-6061) was processed by high-pressure torsion (HPT) at room temperature under an applied pressure of 6.0 GPa up to a total of 5 turns. Detailed measurements after processing revealed the occurrence of continuous grain refinement and material strengthening with increasing imposed strain. The average grain size of the alloy was reduced from ~150 m to a grain size in the range of ~500 nm through processing by HPT. Although there was a difference in the average grain size of samples processed to different levels of imposed strain, careful inspection showed that the structures became similar after annealing at 250°C for 5 min. This suggests that the additional grain refinement introduced at large amounts of deformations is less stable at high temperatures. The results of this investigation, including the distributions of the grain sizes after annealing, are consistent with the predictions of a model based on the occurrence of continuous recrystallization in aluminum alloys having fine grain structures, large fractions of high-angle grain boundaries and where there is a large amount of deformation.

Developing the Technique of Severe Plastic Deformation Processing through High-Pressure Torsion

2010 ◽  
Vol 667-669 ◽  
pp. 397-402 ◽  
Author(s):  
Megumi Kawasaki ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Severe Plastic Deformation Processing ◽  
Average Grain Size ◽  
High Purity Aluminum ◽  
Sample Characteristics ◽  
Nanoscale Range

The processing of metals through the application of severe plastic deformation provides the potential for achieving exceptional grain refinement in bulk solids. Several SPD methods are now available but processing by high-pressure torsion (HPT) has attracted much attention over the last five years. Numerous reports are now available describing the application of HPT to a range of pure metals and simple alloys and excellent grain refinement were achieved using this process with the average grain size often reduced to the nanoscale range. However, in order to make this technique more practical, the nature of the sample characteristics immediately after conventional HPT must be considered in order to understand the fundamental principles of HPT processing. This report examines the procedure with special emphasis on the evolution in hardness homogeneity in both high-purity aluminum and a Zn-22% Al eutectoid alloy processed by HPT.

Strengthening of Al 6061 Alloy by High-Pressure Torsion through Grain Refinement and Aging

2013 ◽  
Vol 765 ◽  
pp. 408-412
Author(s):  
Mohamed Intan Fadhlina ◽  
Seung Won Lee ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Precipitation Hardening ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Aging Treatment ◽  
Microstructural Refinement ◽  
Al 6061 ◽  
Average Grain Size ◽  
Maximum Period ◽  
Processed Sample

The concurrent strengthening process by high-pressure torsion (HPT) and fine precipitation hardening of an Al 6061 alloy has been studied. The HPT was conducted on disks of the alloys at room temperature with an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm. It is shown that the HPT processing leads to microstructural refinement with an average grain size of ~200 nm and to an increase in hardness up to a saturation after 5 turns. Aging treatment was performed at temperatures of 373 and 423 K for a maximum period up to 256 hours. The hardness at the saturation level remains the same during aging at 373 K. When aged at 423 K, the hardness decreases from the beginning of the aging. This study thus suggests that aging of the HPT-processed sample may not be effective to strengthen the alloy if it is carried out at higher temperatures. It is suggested that simultaneous strengthening may be achieved through reduced straining and aging at reduced temperatures.

Effect of SPD Processing Technique on Grain Refinement and Properties of an Austenitic Stainless Steel

2016 ◽  
Vol 879 ◽  
pp. 1957-1962 ◽  
Author(s):  
Marina Tikhonova ◽  
Iaroslava Shakhova ◽  
Rustam Kaibyshev ◽  
Andrey Belyakov
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Stainless Steel ◽  
Severe Plastic Deformation ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Processing Technique ◽  
Multidirectional Forging ◽  
Average Grain Size ◽  
Nanocrystalline Structures

The formation of nanocrystalline structures and mechanical properties were studied in a nitrogen-bearing 304-type stainless steel subjected to severe plastic deformation (SPD). The steel samples were processed at ambient temperature using three different methods, i.e., caliber rolling, multidirectional forging and high pressure torsion. All these techniques resulted in pronounced grain refinement. The microstructures consisting of austenite/ferrite crystallites with transverse dimensions of 50 and 30 nm evolved in the rolled and forged samples, respectively. The austenite fractions comprised approximately 0.4. In contrast, the microstructure consisted mainly of austenite with an average grain size of about 25 nm evolved after high pressure torsion. All samples of the stainless steel subjected to severe plastic deformation demonstrated significant strengthening. The ultimate tensile strengths of 2065 MPa and 1950 MPa, were obtained after rolling and high pressure torsion, respectively. The ultimate tensile strength of samples subjected to multidirectional forging was 1540 MPa.

Microstructural Evolution in the Processing of Bulk Samples Using High-Pressure Torsion

2007 ◽  
Vol 539-543 ◽  
pp. 80-85
Author(s):  
Z. Horita ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Severe Plastic Deformation ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Central Zone ◽  
Thin Disk ◽  
Metallic Materials ◽  
Microstructural Refinement ◽  
Established Technique

Although high-pressure torsion (HPT) is now a well-established technique for imposing severe plastic deformation on metallic materials, the technique is generally restricted to use with thin disk samples. This paper describes experiments which were conducted to evaluate the potential for making use of HPT with bulk samples in the form of small cylinders. The experiments were performed using an Al-Mg-Sc alloy and the samples were strained under a pressure of 1 GPa at room temperature. The results demonstrate excellent microstructural refinement in the vicinity of the central zone around the periphery of the cylinders.

Processing Different Magnesium Alloys through HPT

2014 ◽  
Vol 783-786 ◽  
pp. 2617-2622 ◽  
Author(s):  
Livia Raquel C. Malheiros ◽  
Roberto B. Figueiredo ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Magnesium Alloys ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Structure Refinement ◽  
Hardness Distribution ◽  
Metallic Materials ◽  
Processing Conditions ◽  
Significant Structure

High-Pressure Torsion (HPT) is widely used to refine the structure of metallic materials through the use of severe plastic deformation. This technique is used in this report to process different magnesium alloys using various processing conditions. The high hydrostatic pressure allows processing of these materials at room temperature without cracking. The structure was characterized and hardness distribution was determined at different areas of the processed samples. The results show significant structure refinement and increased hardness. The evolution of the structure and hardness depends on the alloying and HPT processing conditions.

Microstructure and Texture Evolution in Metals and Alloys during Intense Plastic Deformation

2012 ◽  
Vol 715-716 ◽  
pp. 51-60 ◽  
Author(s):  
Alexandre P. Zhilyaev ◽  
Terry R. McNelley ◽  
Oscar A. Ruano
Keyword(s):  
Plastic Deformation ◽  
Grain Refinement ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Texture Evolution ◽  
Pure Aluminum ◽  
Liquid Nitrogen Temperature ◽  
Metals And Alloys ◽  
Work Piece ◽  
Friction Stir

ntense plastic deformation is generally effective in producing grain refinement. IPD methods include equal channel angular pressing/extrusion (ECAP/ECAE), high-pressure torsion (HPT), accumulative roll bonding (ARB), and friction stir processing (FSP), among others. In this work, we summarize the main results on grain refinement by these processing methods and present our own data on microstructure and texture evolution in metals and alloys during ECAP, HPT and FSP. Whereas ECAP and HPT are usually performed with the work piece material initially at room temperature or even at liquid nitrogen temperature to enhance refinement, FSP involves a brief but complex thermomechanical cycle with peak temperatures up to 0.7 0.9 TMelt. Apparently, materials undergo dynamic recrystallization (DRX) during FSP. DRX also occurs also in metals and alloys of low TMeltdue to adiabatic heating during HPT performed at room temperature. The paper is devoted to revisiting of previous as well as new results and a comparative analysis of microstructure and texture evolution in commercially pure aluminum and selected pure metals and alloys during ECAP, HPT and FSP in order to illustrate the limits of grain refinement.

Superplasticity of Ultra-Fine Grained 7075 Alloy Processed by High-Pressure Torsion

2014 ◽  
Vol 794-796 ◽  
pp. 807-810 ◽  
Author(s):  
Seungwon Lee ◽  
Zen Ji Horita
Keyword(s):  
High Pressure ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Tensile Tests ◽  
Initial Strain ◽  
Strain Rates ◽  
Fine Grained ◽  
Al 7075 ◽  
7075 Alloy

An Al 7075 alloy (5.63mass%Zn-2.56mass%Mg-1.68mass%Cu-0.21mass%Fe-0.19mass%Cr-0.14mass%Si-0.02mass%Ti with balance of Al) was processed by high-pressure torsion (HPT) under an applied pressure of 6 GPa for 1, 3 and 5 revolutions with a rotation speed of 1 rpm at room temperature. Vickers microhardness saturated to a level of 220 Hv after the HPT processing and the grain size was refined to 120 nm at the state of the hardness saturation. Tensile tests were conducted with initial strain rates from 2.0 × 10-4 to 2.0 × 10-2 s-1 at temperatures as 200 °C and 250 °C (equivalent to 0.52Tm and 0.57Tm, respectively, where Tm is the melting point of the alloy). The HPT-processed samples for 3 revolutions exhibited superplastic elongations of 640% and 510% at 250 °C with initial strain rates of 2.0 × 10-3 s-1 and 2.0 × 10-2 s-1, respectively.

Application of High-Pressure Sliding for Grain Refinement of Al and Mg Alloys

2010 ◽  
Vol 667-669 ◽  
pp. 91-96 ◽  
Author(s):  
Kiyonari Tazoe ◽  
Shuji Honda ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Strain Rate ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Initial Strain Rate ◽  
Mg Alloys ◽  
Initial Strain ◽  
Mg Alloy ◽  
Al Alloy ◽  
Average Grain Size

An earlier study showed that high-pressure sliding (HPS) is effective for grain refinement of pure Al in a rectangular sheet form using the principle of high-pressure torsion. In this study, the HPS is applied for grain refinement of an Al-3%Mg-0.2%Sc alloy and an AZ61 Mg alloy. HPS was conducted under a pressure of 1 GPa with sliding distances of 10 to 30 mm at room temperature for the Al alloy and at 473 K for the Mg alloy The average grain size is ~300 nm for both the Al and Mg alloys, respectively. Tensile tests showed that a superplastic elongation of ~1500% is achieved in the Al-3%Mg-0.2%Sc alloy at 573 K with an initial strain rate of 3.3x10-3 s-1 and of ~600% in the AZ61 alloy at 573 K with an initial strain rate of 1x10-3 s-1.

Mechanical Properties and Microstructural Behavior of a Metal Matrix Composite Processed by Severe Plastic Deformation Techniques

MRS Advances ◽  
2015 ◽  
Vol 1 (58) ◽  
pp. 3865-3870 ◽  
Author(s):  
Shima Sabbaghianrad ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Metal Matrix Composite ◽  
Matrix Composite ◽  
Metal Matrix ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Average Grain Size ◽  
Al 7075 ◽  
7075 Alloy

ABSTRACTA severe plastic deformation (SPD) technique was applied to an Al-7075 alloy reinforced with 10 vol.% Al2O3. This processing method of high-pressure torsion (HPT) was performed at room temperature under a pressure of 6.0 GPa through a total number of up to 20 turns. The metal matrix composite (MMC) showed a significant grain refinement from an initial average grain size of ∼8 μm to ∼300 nm after processing by HPT through 20 turns which led to an increase in the average values of Vickers microhardness at room temperature.

Sign in / Sign up

Export Citation Format

Share Document