Strengthening of Al 6061 Alloy by High-Pressure Torsion through Grain Refinement and Aging

2013 ◽  
Vol 765 ◽  
pp. 408-412
Author(s):  
Mohamed Intan Fadhlina ◽  
Seung Won Lee ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Precipitation Hardening ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Aging Treatment ◽  
Microstructural Refinement ◽  
Al 6061 ◽  
Average Grain Size ◽  
Maximum Period ◽  
Processed Sample

The concurrent strengthening process by high-pressure torsion (HPT) and fine precipitation hardening of an Al 6061 alloy has been studied. The HPT was conducted on disks of the alloys at room temperature with an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm. It is shown that the HPT processing leads to microstructural refinement with an average grain size of ~200 nm and to an increase in hardness up to a saturation after 5 turns. Aging treatment was performed at temperatures of 373 and 423 K for a maximum period up to 256 hours. The hardness at the saturation level remains the same during aging at 373 K. When aged at 423 K, the hardness decreases from the beginning of the aging. This study thus suggests that aging of the HPT-processed sample may not be effective to strengthen the alloy if it is carried out at higher temperatures. It is suggested that simultaneous strengthening may be achieved through reduced straining and aging at reduced temperatures.

GRAIN REFINEMENT AND MICROSTRUCTURE EVOLUTION IN ALUMINUM A2618 ALLOY BY HIGH-PRESSURE TORSION

2016 ◽  
Vol 78 (6-9) ◽  
Author(s):  
Intan Fadhlina Mohamed ◽  
Seungwon Lee ◽  
Kaveh Edalati ◽  
Zenji Horita ◽  
Shahrum Abdullah ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Saturation Level ◽  
Microstructural Refinement ◽  
Average Grain Size

This work presents a study related to the grain refinement of an aluminum A2618 alloy achieved by High-Pressure Torsion (HPT) known as a process of Severe Plastic Deformation (SPD). The HPT is conducted on disks of the alloy under an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm at room temperature. The HPT processing leads to microstructural refinement with an average grain size of ~250 nm at a saturation level after 5 turns. Gradual increases in hardness are observed from the beginning of straining up to a saturation level. This study thus suggests that hardening due to grain refinement is attained by the HPT processing of the A2618 alloy at room temperature.

Microstructural Evolution in an Al-6061 Alloy Processed by High-Pressure Torsion and Rapid Annealing

2010 ◽  
Vol 667-669 ◽  
pp. 223-228 ◽  
Author(s):  
Aicha Loucif ◽  
Roberto B. Figueiredo ◽  
Thierry Baudin ◽  
François Brisset ◽  
Terence G. Langdon
Keyword(s):  
Grain Size ◽  
High Pressure ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Al 6061 ◽  
Fine Grain ◽  
Grain Structures ◽  
Average Grain Size ◽  
Continuous Recrystallization

The processing of bulk metals through the application of severe plastic deformation provides the opportunity for introducing significant grain refinement into bulk solids. In the present investigation, an aluminum alloy (Al-6061) was processed by high-pressure torsion (HPT) at room temperature under an applied pressure of 6.0 GPa up to a total of 5 turns. Detailed measurements after processing revealed the occurrence of continuous grain refinement and material strengthening with increasing imposed strain. The average grain size of the alloy was reduced from ~150 m to a grain size in the range of ~500 nm through processing by HPT. Although there was a difference in the average grain size of samples processed to different levels of imposed strain, careful inspection showed that the structures became similar after annealing at 250°C for 5 min. This suggests that the additional grain refinement introduced at large amounts of deformations is less stable at high temperatures. The results of this investigation, including the distributions of the grain sizes after annealing, are consistent with the predictions of a model based on the occurrence of continuous recrystallization in aluminum alloys having fine grain structures, large fractions of high-angle grain boundaries and where there is a large amount of deformation.

Nanostructure and Fatigue Behavior of β-Type Titanium Alloy Subjected to High-Pressure Torsion after Aging Treatment

2014 ◽  
Vol 891-892 ◽  
pp. 9-14
Author(s):  
Hakan Yilmazer ◽  
Mitsuo Niinomi ◽  
Ken Cho ◽  
Masaaki Nakai ◽  
Junko Hieda ◽  
...  
Keyword(s):  
High Pressure ◽  
Fatigue Strength ◽  
Biomedical Applications ◽  
High Pressure Torsion ◽  
Fatigue Behavior ◽  
Large Fraction ◽  
Aging Treatment ◽  
Fatigue Behaviour ◽  
Microstructural Refinement ◽  
High Mechanical Strength

A novel β-type, Ti-29Nb-13Ta-4.6Zr, referred to as TNTZ has been developed for biomedical applications. Its fatigue strength is one of the most important mechanical biocompatibilities of TNTZ because, in surgical applications, it will be used under cyclic loading conditions. The effect of the microstructural refinement by high-pressure torsion (HPT) on the fatigue behaviour of TNTZ is systematically investigated in this study. TNTZ subjected to HPT processing where the rotation number (N) is 20 (TNTZAHPT) after aging treatment (AT) shows a unique microstructure having ultrafine elongated grains (285 nm in length and 36 nm in width) with high-density dislocations, a large fraction of blurred and wavy boundaries consisting of non-uniform subgrains with high misorientation and nanostructured precipitated α phase. Remarkably, a good combination of high mechanical strength (1375 MPa) and low Young’s modulus (87 GPa), compared to that of Ti-6Al-4V (Ti64) ELI, is achieved for TNTZAHPT at N = 20. TNTZAHPT a great fatigue strength, which is comparable to those of (Ti64) ELI.

Deformation Induced Percolating Porosity In High Pressure Torsioned (HPT) Copper

2011 ◽  
Vol 702-703 ◽  
pp. 105-108 ◽  
Author(s):  
Matthias Wegner ◽  
Jörn Leuthold ◽  
Sergiy V. Divinski ◽  
Daria Setman ◽  
Michael Zehetbauer ◽  
...  
Keyword(s):  
High Pressure ◽  
Impurity Concentration ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Processing Parameters ◽  
Tracer Method ◽  
Radiotracer Technique ◽  
Degree Of Deformation ◽  
Radio Tracer ◽  
Structural Aspects

Copper of different purity levels (4N, 5N) produced by High Pressure Torsion (HPT) with varying processing parameters is investigated utilizing the radiotracer technique. While the degree of deformation is constant, the effect of the applied quasi-hydrostatic pressure and of the impurity concentration on the as deformed samples is analysed. By applying the radio tracer method micro structural aspects are revealed that are not easily accessible by conventional methods. The measurements indicate the formation of a percolating porosity during the HPT process as a function of the applied pressure and (although less pronounced) of the impurity concentration.

Variation of Microstructure and Mechanical Properties of ZW61 Magnesium Alloy Solidified under Different Pressures

2022 ◽  
Vol 327 ◽  
pp. 3-10
Author(s):  
Shu Sen Wu ◽  
Xiao Gang Fang ◽  
Shu Lin Lü ◽  
Long Fei Liu ◽  
Wei Guo
Keyword(s):  
Mechanical Properties ◽  
High Pressure ◽  
Volume Fraction ◽  
Applied Pressure ◽  
Second Phase ◽  
Cast State ◽  
Microstructure And Properties ◽  
Microstructure Refinement ◽  
Porosity Reduction ◽  
Average Grain Size

There is little datum related to microstructure and properties of Mg alloys squeeze-casted with pressure over 200 MPa. In this study, the microstructure and properties of Mg-6Zn-1.4Y (ZW61) alloy solidified under 100MPa to 800MPa were investigated. The results show that a remarkable microstructure refinement and porosity reduction can be reached through solidification under high pressure. The average grain size and the volume fraction of second phase, i.e. quasicrystal I-phase, decrease continuously with the increase of applied pressure. The tensile properties, especially elongation, are obvious enhanced because of the microstructure refinement and castings densification under high pressure. The ultimate tensile strength and elongation of ZW61 alloy in as-cast state are 243 MPa and 18.7% when the applied pressure is 800 MPa, which are increased by 35% and 118% respectively, compared with that of the gravity castings.

Thermal Stability of Ultrafine-Grained Pure Titanium Processed by High-Pressure Torsion

2021 ◽  
Vol 1016 ◽  
pp. 338-344
Author(s):  
Wan Ji Chen ◽  
Jie Xu ◽  
De Tong Liu ◽  
De Bin Shan ◽  
Bin Guo ◽  
...  
Keyword(s):  
Activation Energy ◽  
Thermal Stability ◽  
Grain Size ◽  
High Pressure ◽  
Annealing Temperature ◽  
High Pressure Torsion ◽  
Stored Energy ◽  
Ultrafine Grained ◽  
Average Grain Size ◽  
Thermal Stability Of

High-pressure torsion (HPT) was conducted under 6.0 GPa on commercial purity titanium up to 10 turns. An ultrafine-grained (UFG) pure Ti with an average grain size of ~96 nm was obtained. The thermal properties of these samples were studied by using differential scanning calorimeter (DSC) which allowed the quantitative determination of the evolution of stored energy, the recrystallization temperatures, the activation energy involved in the recrystallization of the material and the evolution of the recrystallized fraction with temperature. The results show that the stored energy increases, beyond which the stored energy seems to level off to a saturated value with increase of HPT up to 5 turns. An average activation energy of about 101 kJ/mol for the recrystallization of 5 turns samples was determined. Also, the thermal stability of the grains of the 5 turns samples with subsequent heat treatments were investigated by microstructural analysis and Vickers microhardness measurements. It is shown that the average grain size remains below 246 nm when the annealing temperature is below 500 °C, and the size of the grains increases significantly for samples at the annealing temperature of 600 °C.

Aging and Precipitation Behavior in Supersaturated Al-2%Fe Alloy Produced by High-Pressure Torsion

2014 ◽  
Vol 794-796 ◽  
pp. 766-771 ◽  
Author(s):  
Jorge M. Cubero-Sesin ◽  
Masashi Watanabe ◽  
Makoto Arita ◽  
Zen Ji Horita
Keyword(s):  
High Pressure ◽  
High Pressure Torsion ◽  
Xrd Analysis ◽  
Aged Condition ◽  
Subsequent Aging ◽  
Transmission Electron ◽  
Fe Content ◽  
Average Grain Size ◽  
The Matrix ◽  
Peak Aged

The aging behavior of a cast Al-2 wt.% Fe alloy processed by High-Pressure Torsion (HPT) at room temperature was studied by subsequent aging treatments at 200 °C. Observations by Transmission Electron Microscopy (TEM) revealed that the microstructure after HPT processing reached an ultrafine-grained level with an average grain size in the Al matrix of ~120 nm. The initial eutectic structures were fragmented into particles with sizes of less than 400 nm and partially dissolved in the matrix up to a supersaturated Fe content of ~1% as confirmed by X-Ray Diffraction (XRD) analysis. The peak-age condition was achieved within 0.25 h of aging, which provides the maximum hardness of ~200 HV. Analyses by high-resolution S/TEM show that round particles of Al6Fe with sizes of ~5-10 nm and semi-coherent with the matrix are the dominant precipitates in the peak-aged condition. The hardness increases by aging for 12 h above the as-HPT-processed level of 185 HV. The dominant precipitate phase transforms to Al3Fe in the over-aged condition with a loss of coherency during growth. Enhanced precipitation kinetics was observed because of high density of lattice defects induced by the HPT processing, which were also confirmed by significant recovery in the electrical conductivity of the samples after aging.

Superplasticity of Ultra-Fine Grained 7075 Alloy Processed by High-Pressure Torsion

2014 ◽  
Vol 794-796 ◽  
pp. 807-810 ◽  
Author(s):  
Seungwon Lee ◽  
Zen Ji Horita
Keyword(s):  
High Pressure ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Tensile Tests ◽  
Initial Strain ◽  
Strain Rates ◽  
Fine Grained ◽  
Al 7075 ◽  
7075 Alloy

An Al 7075 alloy (5.63mass%Zn-2.56mass%Mg-1.68mass%Cu-0.21mass%Fe-0.19mass%Cr-0.14mass%Si-0.02mass%Ti with balance of Al) was processed by high-pressure torsion (HPT) under an applied pressure of 6 GPa for 1, 3 and 5 revolutions with a rotation speed of 1 rpm at room temperature. Vickers microhardness saturated to a level of 220 Hv after the HPT processing and the grain size was refined to 120 nm at the state of the hardness saturation. Tensile tests were conducted with initial strain rates from 2.0 × 10-4 to 2.0 × 10-2 s-1 at temperatures as 200 °C and 250 °C (equivalent to 0.52Tm and 0.57Tm, respectively, where Tm is the melting point of the alloy). The HPT-processed samples for 3 revolutions exhibited superplastic elongations of 640% and 510% at 250 °C with initial strain rates of 2.0 × 10-3 s-1 and 2.0 × 10-2 s-1, respectively.

Application of High-Pressure Sliding for Grain Refinement of Al and Mg Alloys

2010 ◽  
Vol 667-669 ◽  
pp. 91-96 ◽  
Author(s):  
Kiyonari Tazoe ◽  
Shuji Honda ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Strain Rate ◽  
Grain Refinement ◽  
High Pressure Torsion ◽  
Initial Strain Rate ◽  
Mg Alloys ◽  
Initial Strain ◽  
Mg Alloy ◽  
Al Alloy ◽  
Average Grain Size

An earlier study showed that high-pressure sliding (HPS) is effective for grain refinement of pure Al in a rectangular sheet form using the principle of high-pressure torsion. In this study, the HPS is applied for grain refinement of an Al-3%Mg-0.2%Sc alloy and an AZ61 Mg alloy. HPS was conducted under a pressure of 1 GPa with sliding distances of 10 to 30 mm at room temperature for the Al alloy and at 473 K for the Mg alloy The average grain size is ~300 nm for both the Al and Mg alloys, respectively. Tensile tests showed that a superplastic elongation of ~1500% is achieved in the Al-3%Mg-0.2%Sc alloy at 573 K with an initial strain rate of 3.3x10-3 s-1 and of ~600% in the AZ61 alloy at 573 K with an initial strain rate of 1x10-3 s-1.

X-Ray Analysis of High Pressure Torsion Induced Nanostructures in Ti and Ni

2006 ◽  
Vol 114 ◽  
pp. 329-336 ◽  
Author(s):  
A.R. Kilmametov ◽  
Ruslan Valiev ◽  
Igor V. Alexandrov
Keyword(s):  
High Pressure ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Orientation Distribution ◽  
Nanocrystalline State ◽  
Cubic Symmetry ◽  
X Ray ◽  
Ω Phase ◽  
Commercially Pure ◽  
Pressure Phase

X-ray investigations revealed that the increase in the applied pressure during high pressure torsion (HPT) of commercially pure Ti leads not only to substructure refinement with an increase of the dislocation density and microstrain level but also to an α→ ω phase transition at room temperature. The coexistence of both α and ω phases, the latter known as a high pressure phase, in the ratio approximately of 1:3 has been obtained after removal of thehigh pressure. Texture analysis of electodeposited Ni after HPT discovered a new form of crystallite orientation distribution in the nanocrystalline state. A nearly random orientation crystallite distribution has been observed unlike the “traditional” case of a shear texture forming in cubic symmetry metals. The crystallographic texture data obtained were considered as experimental evidence of the changed plastic deformation mechanisms in nanocrystalline Ni produced by HPT.

Sign in / Sign up

Export Citation Format

Share Document