Superplasticity of Ultra-Fine Grained 7075 Alloy Processed by High-Pressure Torsion

2014 ◽  
Vol 794-796 ◽  
pp. 807-810 ◽  
Author(s):  
Seungwon Lee ◽  
Zen Ji Horita
Keyword(s):  
High Pressure ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Tensile Tests ◽  
Initial Strain ◽  
Strain Rates ◽  
Fine Grained ◽  
Al 7075 ◽  
7075 Alloy

An Al 7075 alloy (5.63mass%Zn-2.56mass%Mg-1.68mass%Cu-0.21mass%Fe-0.19mass%Cr-0.14mass%Si-0.02mass%Ti with balance of Al) was processed by high-pressure torsion (HPT) under an applied pressure of 6 GPa for 1, 3 and 5 revolutions with a rotation speed of 1 rpm at room temperature. Vickers microhardness saturated to a level of 220 Hv after the HPT processing and the grain size was refined to 120 nm at the state of the hardness saturation. Tensile tests were conducted with initial strain rates from 2.0 × 10-4 to 2.0 × 10-2 s-1 at temperatures as 200 °C and 250 °C (equivalent to 0.52Tm and 0.57Tm, respectively, where Tm is the melting point of the alloy). The HPT-processed samples for 3 revolutions exhibited superplastic elongations of 640% and 510% at 250 °C with initial strain rates of 2.0 × 10-3 s-1 and 2.0 × 10-2 s-1, respectively.

scholarly journals Microstructure and Aging Behavior of Cu-Be Alloy Processed by High-Pressure Torsion

2014 ◽  
Vol 783-786 ◽  
pp. 2707-2712 ◽  
Author(s):  
Chihiro Watanabe ◽  
Ryoichi Monzen ◽  
Seiichiro Ii ◽  
Koichi Tsuchiya
Keyword(s):  
High Pressure ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Solution Treatment ◽  
Equivalent Strain ◽  
Aging Behavior ◽  
Fine Grained ◽  
Transmission Electron ◽  
Fine Grained Structure

The microstructure and aging behavior of Cu-1.8wt%Be-0.2wt%Co alloy specimens processed by high-pressure torsion (HPT) at room temperature (RT) and 150°C after solution treatment have been studied. Application of HPT processing at RT and 150°C under an applied pressure of 5 GPa for 10 revolutions at 1 rpm to alloy specimens (RT-and 150°C-specimen) produces an ultra-fine grained structure with a grain size of 70 nm. The hardnesses of the RT-and 150°C-specimens increase with equivalent strain up to 7 and then saturate at constant values of 400 and 430 Hv, respectively. Annealing the RT-specimen at 150°C for 10 min increases the hardness from 400 to 430 Hv. Transmission electron microscopy observations of the 150°C-specimen and the RT-specimen annealed at 150°C reveal that there are no intragranular and intergranular precipitates. It is suggested that the higher hardness of the 150°C-specimen than the RT-specimen is ascribed to the segregation of Be atoms on dislocations during HPT processing at 150°C. The RT-and 150°C-specimens harden rapidly and exhibit maximum values of hardness at 3 min during aging at 320°C. The increase in the hardness is attributed to the precipitation of finely dispersed G.P. zones.

Microtextural Changes and Superplasticity in an Al-7075 Alloy Processed by High-Pressure Torsion

2016 ◽  
Vol 838-839 ◽  
pp. 445-450 ◽  
Author(s):  
Aicha Loucif ◽  
Yi Huang ◽  
Anne Laure Helbert ◽  
Thierry Baudin ◽  
Shima Sabbaghianrad ◽  
...  
Keyword(s):  
High Pressure ◽  
Tensile Testing ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
X Ray Diffraction ◽  
X Ray ◽  
Pole Figures ◽  
Al 7075 ◽  
7075 Alloy ◽  
Superplastic Properties

The influence of High-Pressure Torsion (HPT) on texture and superplasticity in an Al-7075 was studied using X-ray diffraction and tensile testing. The alloy was processed by HPT at room temperature under a pressure of 6.0 GPA up to a maximum of 20 turns. The pole figures were measured at mid-radius of the disks after 1, 5, 10 and 20 turns. The results show the presence of a typical torsion texture during HPT, in particular, the C{001}<110> component was found to develop preferentially. With increasing deformation, the A {111}<110> and the C components are reinforced after 5 turns and the texture tends to be random with the presence of a fibre texture near the center. Moreover, the fraction of C components tends to gradually decrease and a fairly isotropic microtexture is apparent after 20 turns. Tensile testing showed the development of excellent superplastic properties in this alloy with elongations up to ~700% when testing at a temperature of 623 K.

GRAIN REFINEMENT AND MICROSTRUCTURE EVOLUTION IN ALUMINUM A2618 ALLOY BY HIGH-PRESSURE TORSION

2016 ◽  
Vol 78 (6-9) ◽  
Author(s):  
Intan Fadhlina Mohamed ◽  
Seungwon Lee ◽  
Kaveh Edalati ◽  
Zenji Horita ◽  
Shahrum Abdullah ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Saturation Level ◽  
Microstructural Refinement ◽  
Average Grain Size

This work presents a study related to the grain refinement of an aluminum A2618 alloy achieved by High-Pressure Torsion (HPT) known as a process of Severe Plastic Deformation (SPD). The HPT is conducted on disks of the alloy under an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm at room temperature. The HPT processing leads to microstructural refinement with an average grain size of ~250 nm at a saturation level after 5 turns. Gradual increases in hardness are observed from the beginning of straining up to a saturation level. This study thus suggests that hardening due to grain refinement is attained by the HPT processing of the A2618 alloy at room temperature.

Mechanical Properties and Microstructural Behavior of a Metal Matrix Composite Processed by Severe Plastic Deformation Techniques

MRS Advances ◽  
2015 ◽  
Vol 1 (58) ◽  
pp. 3865-3870 ◽  
Author(s):  
Shima Sabbaghianrad ◽  
Terence G. Langdon
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Metal Matrix Composite ◽  
Matrix Composite ◽  
Metal Matrix ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Average Grain Size ◽  
Al 7075 ◽  
7075 Alloy

ABSTRACTA severe plastic deformation (SPD) technique was applied to an Al-7075 alloy reinforced with 10 vol.% Al2O3. This processing method of high-pressure torsion (HPT) was performed at room temperature under a pressure of 6.0 GPa through a total number of up to 20 turns. The metal matrix composite (MMC) showed a significant grain refinement from an initial average grain size of ∼8 μm to ∼300 nm after processing by HPT through 20 turns which led to an increase in the average values of Vickers microhardness at room temperature.

scholarly journals Microstructure and Mechanical Properties of Al-3 Vol% CNT Nanocomposites Processed by High-Pressure Torsion

2017 ◽  
Vol 62 (2) ◽  
pp. 1109-1112 ◽  
Author(s):  
H. Asgharzadeh ◽  
H.S. Kim
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
High Pressure ◽  
Room Temperature ◽  
High Pressure Torsion ◽  
Tensile Ductility ◽  
Tensile Tests ◽  
Tensile Fracture ◽  
Tensile Fracture Surface ◽  
Transmission Electron

Abstract Al-3 vol% CNT nanocomposites were processed by high-pressure torsion (HPT) at room temperature under the pressure in the range of 2.5-10 GPa for up to 10 turns. Optical microscopy, scanning electron microscopy, and transmission electron microscopy (TEM) were used to investigate the microstructural evolutions upon HPT. Mechanical properties of the HPT-processed disks were studied using tensile tests and microhardness measurements. The results show gradual evolutions in the density, microstructure, and hardness with increasing the number of turns and applied presure. Nanostructured and elongated Al grains with an average grain thickness of ~40 nm perpendicular to the compression axis of HPT and an aspect ratio of ~3 are formed after 10 turns under 6 GPa. Evaluating the mechanical properties of the 10-turn processed Al/CNT nanocomposites indicates a tensile strength of 321 MPa and a hardness of 122 Hv. The tensile fracture surface of the Al/CNT nanocomposite mostly demonstrates a smooth fracture manner with fine dimples resulting in a low tensile ductility of ~1.5%.

Formability Characteristics of AA5083 Sheets under Hot Forming Conditions

2013 ◽  
Vol 549 ◽  
pp. 356-363
Author(s):  
Stefania Bruschi ◽  
Andrea Ghiotti ◽  
Francesco Michieletto
Keyword(s):  
Aluminum Alloy ◽  
Elevated Temperature ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Superplastic Forming ◽  
Tensile Tests ◽  
Processing Route ◽  
Strain Rates ◽  
Fine Grained ◽  
Axial Tensile

The production of aluminum alloy components through sheet forming processes conducted at elevated temperatures is gaining more and more interest as it gives raise to the possibility of a significant enhancement of the metal formability characteristics, compared to room temperature forming. Aluminum alloy AA5083 blanks, which present a limited formability at room temperature, are usually formed through superplastic forming at elevated temperature: however, this processing route is too slow to be applicable for large batch production, typical for instance of the automotive industry. The paper is aimed at exploring the formability characteristics of the AA5083 when deformed at elevated temperature, but in a range of strain rates higher than those usually applicable in superplastic forming. To this aim, uni-axial tensile tests were carried out, in order to record the material formability characteristics as a function of temperature and strain rate, and to correlate them with the developed microstructural features. It is shown that it is possible to work at higher strain rates, still preserving a significant formability, even without using a conventional fine-grained superplastic alloy.

Microstructure Development and Ductility of Ultra-Fine Grained Mg-Gd Alloy Prepared by High Pressure Torsion

2009 ◽  
Vol 633-634 ◽  
pp. 353-363 ◽  
Author(s):  
Jakub Čížek ◽  
Ivan Procházka ◽  
Bohumil Smola ◽  
Ivana Stulíková ◽  
Vladivoj Očenášek ◽  
...  
Keyword(s):  
Grain Size ◽  
High Pressure ◽  
Elevated Temperatures ◽  
High Pressure Torsion ◽  
High Sensitivity ◽  
Tensile Tests ◽  
Lattice Defects ◽  
Coarse Grained ◽  
Fine Grained ◽  
Mean Grain Size

Microstructure of ultra fine grained (UFG) Mg-Gd alloy prepared by high-pressure torsion (HPT) was investigated in the present work. Lattice defects introduced by HPT were characterized at first. Subsequently thermal stability of UFG structure and its development with annealing temperature were studied and correlated with changes of hardness and ductility. Precipitation effects in the alloy with UFG structure were compared with those in a conventional coarse-grained alloy. Defect studies were performed by positron annihilation spectroscopy (PAS), which represents well established non-destructive technique with a high sensitivity to open volume lattice defects like vacancies, dislocations, misfit defects etc. PAS investigations were combined with transmission electron microscopy (TEM) and X-ray diffraction (XRD). Changes of mechanical properties were monitored by Vicker’s microhardness (HV) and deformation tensile tests. It was found that HPT deformed Mg-Gd alloy exhibits UFG structure with mean grain size of 100 nm and a dense network of dislocations distributed uniformly throughout the whole sample. Although recovery of dislocations takes place at relatively low temperatures, it is not accompanied by grain growth and the mean grain size remains around 100 nm up to 300oC. Tensile tests performed at elevated temperatures to examine ductility showed that HPT-deformed alloy exhibits a superplastic behavior at 400oC. Moreover, it was found that the precipitation sequence in HPT-deformed alloy differs from that in conventional coarse-grained material.

Microstructure of Ultra Fine Grained Mg and Mg-10 wt.% Gd Prepared by High-Pressure Torsion

Magnesium ◽  
2005 ◽  
pp. 202-207
Author(s):  
J. Cizek ◽  
I. Prochazka ◽  
I. Stulikova ◽  
B. Smola ◽  
R. Kuzel ◽  
...  
Keyword(s):  
High Pressure ◽  
High Pressure Torsion ◽  
Fine Grained

Microstructure development of ultra fine grained Mg-22 wt%Gd alloy prepared by high pressure torsion

2017 ◽  
Vol 704 ◽  
pp. 181-191 ◽  
Author(s):  
J. Čížek ◽  
P. Hruška ◽  
T. Vlasák ◽  
M. Vlček ◽  
M. Janeček ◽  
...  
Keyword(s):  
High Pressure ◽  
High Pressure Torsion ◽  
Microstructure Development ◽  
Fine Grained

Deformation Induced Percolating Porosity In High Pressure Torsioned (HPT) Copper

2011 ◽  
Vol 702-703 ◽  
pp. 105-108 ◽  
Author(s):  
Matthias Wegner ◽  
Jörn Leuthold ◽  
Sergiy V. Divinski ◽  
Daria Setman ◽  
Michael Zehetbauer ◽  
...  
Keyword(s):  
High Pressure ◽  
Impurity Concentration ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Processing Parameters ◽  
Tracer Method ◽  
Radiotracer Technique ◽  
Degree Of Deformation ◽  
Radio Tracer ◽  
Structural Aspects

Copper of different purity levels (4N, 5N) produced by High Pressure Torsion (HPT) with varying processing parameters is investigated utilizing the radiotracer technique. While the degree of deformation is constant, the effect of the applied quasi-hydrostatic pressure and of the impurity concentration on the as deformed samples is analysed. By applying the radio tracer method micro structural aspects are revealed that are not easily accessible by conventional methods. The measurements indicate the formation of a percolating porosity during the HPT process as a function of the applied pressure and (although less pronounced) of the impurity concentration.

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