Deformation of Polymers During Hydrostatic Extrusion

1978 ◽  
Vol 100 (4) ◽  
pp. 400-405 ◽  
Author(s):  
N. Inoue ◽  
T. Nakayama ◽  
M. Shimono

Crystalline as well as amorphous polymers and a thermosetting resin were hydrostatically extruded with pressures up to 4 kilobars. A linear relation was obtained between the extrusion pressure and extrusion ratio. Temperature of the billets during the extrusion process was determined, along with the flow pattern of the deformation. Tension tests at the temperature, to which the billet was exposed during the extrusion, was carried out at atmospheric pressure on the high-density polyethylene specimen to supply a theoretical basis to the experimental formula. Effects of temperature and strain rate on the extrusion process are discussed in the light of the temperature-time superposition principle.

1975 ◽  
Vol 40 (1) ◽  
pp. 129-132 ◽  
Author(s):  
C. E. LYON ◽  
B. G. LYON ◽  
A. A. KLOSE ◽  
J. P. HUDSPETH

2012 ◽  
Vol 2012 (HITEC) ◽  
pp. 000129-000134 ◽  
Author(s):  
Kewei Xiao ◽  
Jesus N. Calata ◽  
Hanguang Zheng ◽  
Khai D.T. Ngo ◽  
Guo-Quan Lu

Sintered nanoscale silver joint is an emerging lead-free die-attach solution for high-temperature packaging because of silver's high melting temperature. For bonding small chips, the nanosilver solution can be achieved with a simple heating profile under atmospheric pressure. However, for bonding large-area chips, e.g. > 1 cm2 IGBT chips, uniaxial pressure of a few MPa has been found necessary during the sintering stage of the bonding process, which is carried out at temperatures below 275°C. Hot-pressing at high temperatures can cause significant wear and tear on the processing equipment, resulting in high maintenance cost. In this study, we ran a series of experiments aimed at lowering the hot-pressing temperature. Specifically, we examined a process involving hot-press drying, followed by sintering without any applied pressure. A fractional factorial design of experiments was used to identify the importance and interaction of various processing parameters, such as hot-pressing pressure/temperature/time and sintering temperature/time, on the final bond quality of sintered nanosilver joints. Based on the results, a simpler process, consisting of hot-press drying at 180°C under 3 MPa, followed by sintering at 275°C under atmospheric pressure was found to produce attachments with die-shear strength in excess of 30 MPa.


2017 ◽  
Vol 12 (1) ◽  
pp. 88-96 ◽  
Author(s):  
Tong Xu ◽  
Veronica Rodriguez-Martinez ◽  
Shreya N. Sahasrabudhe ◽  
Brian E. Farkas ◽  
Stephanie R. Dungan

2021 ◽  
Vol 93 ◽  
pp. 106932
Author(s):  
Lei Xu ◽  
Zhengliang Huang ◽  
Yao Yang ◽  
Binbo Jiang ◽  
Jingyuan Sun ◽  
...  

2014 ◽  
Vol 8 (7) ◽  
pp. 491-504 ◽  
Author(s):  
A. Aguilar-Rios ◽  
P. J. Herrera-Franco ◽  
A. de J. Martinez-Gomez ◽  
A. Valadez-Gonzalez

2012 ◽  
Vol 538-541 ◽  
pp. 1187-1191
Author(s):  
Min Cong Zhang ◽  
Chen Yi Liu ◽  
Shu Yun Wang

The non-metallic inclusions in FGH96 superalloy during different plastic processes were studied. The results show that SiO2 react with aluminum and titanium in FGH96 superalloy and the reaction zone is formed in the interface between SiO2 and alloy, whereas Al2O3 react with no elements in FGH96 superalloy and the transition zone between them is mechanical combination during the plastic processes. In addition the sizes of non-metallic inclusions increase in the direction perpendicular to deformation during isothermal forging process. The non-metallic inclusions are pulled into a discontinuous line in extrusion direction and areas of non-metallic inclusions in each direction are constricted during extrusion process. The non-metallic inclusions of FGH96 superalloy is conditioned by the state of the as-extrusion inclusions during extrusion+isothermal forging process. In summary, extrusion process with large extrusion ratio can break the non-metallic inclusions in FGH96 alloy effectively and improve forging quality.


2004 ◽  
Vol 449-452 ◽  
pp. 317-320 ◽  
Author(s):  
Hyouk Chon Kwon ◽  
Taek Kyun Jung ◽  
Sung Chul Lim ◽  
Mok Soon Kim

The optimized extrusion conditions from the present research were the extrusion temperature of 573~623K and the extrusion ratio(A0/A) of 21.39. Above the extrusion temperature of 623K, the fracture of sheath material was observed. It is due to the difference of flow stress between the sheath material and the core material during extrusion process. The bonding strength increased with increasing the extrusion temperature and the extrusion ratio. The bonding strength increased with increasing the annealing temperature. However, over 573K, it decreased abruptly since the thick and brittle intermetallic compounds of larger than 3µm were formed. The electricalconductivity of copper clad aluminum wire was about 70%IACS without annealing.


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