scholarly journals Experimental Study of Hydraulic Sealability and Shear Bond Strength of Cementitious Barrier Materials

2021 ◽  
pp. 1-33
Author(s):  
Mohammadreza Kamali ◽  
Mahmoud Khalifeh ◽  
Elsayed Eid ◽  
Arild Saasen

Abstract In this experimental study, two different cementitious materials including (i) a class of expansive cement currently used for plug and abandonment (P&A) operations, and (ii) a non-cement-based naturally occurring rock, known as geopolymer are selected to examine the hydraulic bond strength and shear bond strength. Clean machined steel and rusty corroded steel were selected to represent the casing. The test samples were cured at 90 °C considered as bottom-hole static temperature (BHST) and under elevated pressure of 17.2 MPa for one week. The hydraulic sealability of the barrier materials tested up to 3.4 MPa of differential pressure. The results indicated that additives used in slurry preparation impact the hydraulic sealability of the material. Additionally, the rusty corroded streel provided a better hydraulic sealability comparing to the clean machined steel for the same cementitious material. The shear bond strength test was performed by running the push-out test. According to the present test observations, no correlation was found between the shear bond and hydraulic bond strength of different barrier materials. The geopolymer showed the lowest shear bond strength, while it provided the highest hydraulic sealability.

2021 ◽  
Author(s):  
Mohammadreza Kamali ◽  
Mahmoud Khalifeh ◽  
Elsayed Eid ◽  
Arild Saasen

Abstract In this experimental study, two different cementitious materials including (i) a class of expansive cement that is currently used for P&A operations, and (ii) a non-cement-based naturally occurring rock, known as geopolymer are selected to examine the hydraulic bond strength and shear bond strength. Clean machined steel and rusty corroded steel were selected to represent the casing. The test samples were cured at 90 °C, which is considered as bottom-hole static temperature (BHST), and under elevated pressure of 17.2 MPa for one week. The hydraulic sealability of the barrier materials tested up to 3.4 MPa of differential pressure. The results indicated that additives used in slurry preparation have an impact on the hydraulic sealability of the material. Additionally, the rusty corroded streel provided a better hydraulic sealability comparing to the clean machined steel for the same cementitious material. The shear bond strength test was performed by running the push-out test. According to the present test observations, no correlation was found between the shear bond and hydraulic bond strength of different barrier materials. The geopolymer showed the lowest shear bond strength, while it provided the highest hydraulic sealability.


2020 ◽  
Vol 10 (7) ◽  
pp. 2535
Author(s):  
Hyoung-Sik Kim ◽  
Song-Yi Yang ◽  
Eun Ha Choi ◽  
Kwang-Mahn Kim ◽  
Jae-Sung Kwon

The purpose of the study was to evaluate the adhesion between dental core resin and epoxy resin-based fiber post after treatment with non-thermal atmospheric pressure plasma (NTAPP) and compare with conventional methods of epoxy resin-based fiber post treatments. Contact angle was measured on the surface of epoxy resin before and after NTAPP treatment and X-ray photoelectron spectroscopy was used to analyze the surface chemistry. Finally, two shear bond strength tests were carried out; shear bond strength between core resin and epoxy resin for comparison between NTAPP treated and untreated sample, and push-out shear bond strength between core resin and NTAPP treated commercially available epoxy resin-based fiber post for comparison between NTAPP treated samples with conventionally treated samples. Contact angle on the surface of epoxy resin generally decreased with increasing NTAPP treatment time with presence of surface chemical changes. Also, there was significantly higher shear bond strength and push-out shear bond strength between epoxy resin and core resin for NTAPP treated epoxy resin, even to the conventionally treated epoxy resin-based fiber post with hydrofluoric acid or silane. In conclusion, new technology of NTAPP has potential for application on the epoxy resin-based fiber post to improve endodontic restoration success rate.


2011 ◽  
Vol 366 ◽  
pp. 494-497
Author(s):  
Wei Jun Yang ◽  
Huan Zeng

This article analyzes about four aspects of insulation mortar of various performance indicators, including anti-cracking, flexural strength and compressive strength, shear bond strength and shrinkage rate, it is concluded that the insulation mortar meets to various performance indicators requirement of masonry mortar or plastering mortar.


2012 ◽  
Vol 525-526 ◽  
pp. 205-208 ◽  
Author(s):  
Peter Helincks ◽  
Wouter de Corte ◽  
Jan Klusák ◽  
Veerle Boel ◽  
Geert de Schutter

Steel-concrete joints are often provided with welded shear studs. However, stress concentrations are induced in the structure due to the welding. Moreover, a reduction in toughness and ductility of the steel and a decreased fatigue endurance of the construction is observed. In this paper the shear bond strength between steel and ultra-high performance concrete (UHPC) without mechanical shear connectors is evaluated through push-out tests. The test samples consist of two sandblasted steel plates with a thickness of 10 mm and a concrete core. The connection between steel and concrete is obtained by a 2-component epoxy resin. Test samples with a smooth adhesive layer are compared with those with an epoxy layer, which is applied with a toothed paddle and/or gritted with small aggregates. In this research, specimens prepared with river gravel, crushed stone, and steel grit are compared and also two different epoxy resins are used. During the tests, the ultimate shear force is recorded as well as the slip between steel and concrete. All test specimens exhibited a concrete-adhesive or concrete failure. Furthermore, test results show that the use of a more fluid epoxy resin improves the anchorage of the gritted aggregates in the adhesive layer, resulting in higher shear bond stresses. No significant difference is found between specimens, gritted with river gravel or crushed stone. Applying the adhesive layer with the toothed paddle in horizontal direction slightly improves the bond behaviour. Finally, the experimental results of the test members with a smooth epoxy layer without gritted aggregates, provide test data for a fracture mechanics approach, which uses a 2D numerical model of the test specimen, composed of steel, epoxy resin, and concrete.


2016 ◽  
Vol 2016 ◽  
pp. 1-7 ◽  
Author(s):  
Natália Araújo Silva Prado ◽  
Reinaldo de Souza Ferreira ◽  
Marcos Henrique de Pinho Maurício ◽  
Sidnei Paciornik ◽  
Mauro Sayão de Miranda

The present study evaluated the influence of the cement film thickness on the push-out bond strength of glass fiber posts in the cervical, medium, and apical thirds of root canal spaces. Thirty roots were randomly divided into three groups, according to the fiber post system’s drills: (G1) #2; (G2) #3; (G3) #4. The posts were cemented using a self-adhesive cement, and a small amount of powdered Rhodamine B was used as a stain. Images of both sides of each slice were obtained before and after the push-out test. To determine the cement thickness, a macro routine was developed using the software KS 400. The data were analyzed statistically using Kruskal-Wallis and Dunn’s test. G2 (14.62±5.15 MPa) showed statistically higher bond strength values than G1 (10.04±5.13 MPa) and G3 (7.68±6.14 MPa). All groups presented higher bond strength values in the apical third. The bur diameter significantly influenced the results of the shear bond strength for the push-out test. The slight increase in the cement thickness allowed an increase in the values of shear bond strength when compared to very thin or very thick cement films.


2016 ◽  
Vol 45 (4) ◽  
pp. 227-233
Author(s):  
Adriana Rosado Valente ANDRIOLI ◽  
Margareth COUTINHO ◽  
Andréa Araújo de VASCONCELLOS ◽  
Milton Edson MIRANDA

Abstract Introduction The correct use of glass fiber posts in endodontically treated teeth is essential for the clinical success of restorative treatment. Objective This study evaluated the push-out shear bond strength of relined (R) or non-relined (NR) glass fiber posts, cemented with self-adhesive resin cement [RelyXTM U100 (U100)] and conventional resin cement [RelyXTM ARC (ARC)]. Material and method Sixty human single-rooted teeth were endodontically treated and divided into ARC-NR; U100-NR; ARC-R; U100-R groups. The teeth were sectioned into cervical, middle and apical thirds, and subjected to the push-out test. Bond strength was analyzed by the Friedman test; cement and post types were compared by the Mann Whitney test. The pattern of failures was evaluated with digital camera through images at 200x magnification, and was classified as adhesive (at the cement/dentin or cement/post interface), cohesive (cement or post), and mixed failures. Result In ARC-NR, bond strength values were higher in the cervical third; in U100-NR and ARC-R they were similar between the thirds. In U100-R, in the cervical and middle thirds the bond strength values were similar, and there was lower value in the apical third. For non-relined glass fiber posts, the highest mean bond strength values were observed with self-adhesive resin cement. Whereas, relined posts cemented with conventional resin cement had stronger cement layer in comparison with non-relined fiber posts. Conclusion The post relining technique was efficient in ARC-R. ARC-NR and U100-R showed improved bond strength in the cervical region of canal walls. The main failures were adhesive at the cement-post interface.


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