Design of Experimental Loop With Supercritical Carbon Dioxide

2014 ◽  
Author(s):  
Ladislav Vesely ◽  
Vaclav Dostal ◽  
Petr Hajek
Keyword(s):  
Heat Transfer ◽  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Experimental Research ◽  
Research Program ◽  
Operating Conditions ◽  
Research Centre ◽  
Experimental Measurements ◽  
The World ◽  
Supercritical Carbon

Supercritical carbon dioxide (S-CO2) cycles are recently very perspective and are researched all around the world. For successful deployment of these cycles experimental research is necessary. This paper describes the design and research program of S-CO2 experimental loop that was performed in collaboration of the Czech Technical University in Prague (CTU) and the Research Centre Rez i.n.c.. The loop will be constructed at the premises of the Research Centre Rez i.n.c a part of the project SUSEN. This paper particularly focuses on the design of components, their thermotechnical calculations, construction and arrangement of the experimental loop. It also deals with the preparation of experimental measurements to be implemented. The loop is envisioned for the research of the heat transfer for various operating conditions, testing of the material in the environment of S-CO2 and sampling of gas from the loop.

Comparison of Existing Supercritical Carbon Dioxide Heat Transfer Correlations for Horizontal and Vertical Bare Tubes

2012 ◽  
Author(s):  
Prabu Surendran ◽  
Sahil Gupta ◽  
Tiberiu Preda ◽  
Igor Pioro
Keyword(s):  
Heat Transfer ◽  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Wall Temperature ◽  
Statistical Error ◽  
Heat Fluxes ◽  
Transfer Coefficients ◽  
Bulk Fluid ◽  
Heat Transfer Correlations ◽  
Supercritical Carbon

This paper presents a thorough analysis of ability of various heat transfer correlations to predict wall temperatures and Heat Transfer Coefficients (HTCs) against experiments on internal forced-convective heat transfer to supercritical carbon dioxide conducted by Koppel [1], He [2], Kim [3] and Bae [4]. It should be noted the Koppel dataset was taken from a paper which used the Koppel data but was not written by Koppel. All experiments were completed in bare tubes with diameters from 0.948 mm to 9 mm for horizontal and vertical configurations. The datasets contain a total of 1573 wall temperature points with pressures ranging from 7.58 to 9.59 MPa, mass fluxes of 400 to 1641 kg/m2s and heat fluxes from 20 to 225 kW/m2. The main objective of the study was to compare several correlations and select the best of them in predicting HTC and wall temperature values for supercritical carbon dioxide. This study will be beneficial for analyzing heat exchangers involving supercritical carbon dioxide, and for verifying scaling parameters between CO2 and other fluids. In addition, supercritical carbon dioxide’s use as a modeling fluid is necessary as the costs of experiments are lower than supercritical water. The datasets were compiled and calculations were performed to find HTCs and wall and bulk-fluid temperatures using existing correlations. Calculated results were compared with the experimental ones. The correlations used were Mokry et al. [5], Swenson et al. [6] and a set of new correlations presented in Gutpa et al. [7]. Statistical error calculations were performed are presented in the paper.

Extraction and Identification of Vitamin E from Pithecellobium Jiringan Seeds Using Supercritical Carbon Dioxide

2015 ◽  
Vol 74 (7) ◽  
Author(s):  
Mohd Azizi Che Yunus ◽  
Salman Zhari ◽  
Saharudin Haron ◽  
Nur Husnina Arsad ◽  
Zuhaili Idham ◽  
...  
Keyword(s):  
Carbon Dioxide ◽  
Vitamin E ◽  
Supercritical Carbon Dioxide ◽  
Potential Method ◽  
Operating Conditions ◽  
Oil Yield ◽  
Flight Mass Spectrometry ◽  
Carbon Dioxide Extraction ◽  
Natural Herb ◽  
Supercritical Carbon

Pithecellobium Jiringan (P. Jiringan) is traditionally known as natural herb consists of several medicinal compounds (vitamin E). Supercritical carbon dioxide extraction (SC-CO2) has been proven as potential method to extract interest compound from herbs. By altering pressure and temperature, the specific compound can be extracted. In this study, the SC-CO2 operating conditions are pressure (20.68 MPa to 55.16 MPa) and temperature (40°C to 80°C) in one hour extraction regime was used to extract vitamin E from P. jiringan. The quantification of vitamin E was analysed with Gas Chromatography Time of Flight Mass Spectrometry (GC-TOF-MS). The responses are overall oil yield and vitamin E yield. The overall oil yield was obtained at the highest condition of 55.16 MPa and 80°C with asymptotic yield of 8.06%. In contrast, the highest amount of vitamin E obtained is 0.0458mg/g sample (80.14 ppm) at the lowest extraction condition of 20.68 MPa and 40ᵒC.

Microcellular Polymeric Foams (MPFs) Generated Continuously in Supercritical Carbon Dioxide

2000 ◽  
Vol 629 ◽  
Author(s):  
Srinivas Siripurapu ◽  
Yvon J. Gay ◽  
Joseph R. Royer ◽  
Joseph M. DeSimone ◽  
Saad A. Khan ◽  
...  
Keyword(s):  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Vinylidene Fluoride ◽  
Amorphous Polymer ◽  
Extrusion Process ◽  
Operating Conditions ◽  
Polymeric Foams ◽  
Poly Vinylidene Fluoride ◽  
Cell Densities ◽  
Supercritical Carbon

ABSTRACTMicrocellular polymeric foams (MPFs) hold tremendous promise for engineering applications as substitutes to their solid analogs in light of reduced manufacturing/materials costs and improved properties. We present a two-part study addressing the generation of such materials in the presence of supercritical carbon dioxide (scCO2). The first part describes the production of polystyrene MPFs in a continuous extrusion process, as well as the effect of operating conditions such as temperature and CO2 concentration on foam morphology. The second part discusses microcellular foaming of poly (vinylidene fluoride) (PVDF), a semicrystalline polymer, via blending with the amorphous polymer poly (methyl methacrylate) PMMA. Foams of pure PVDF possess ill-defined morphologies, whereas those of PVDF-PMMA blends show an improvement with cell sizes on the order of 10 mm or less and cell densities in excess of 109 cells/cm3.

Supercritical Carbon Dioxide Heat Transfer in Horizontal Semicircular Channels

2012 ◽  
Vol 134 (8) ◽  
Author(s):  
Alan Kruizenga ◽  
Hongzhi Li ◽  
Mark Anderson ◽  
Michael Corradini
Keyword(s):  
Heat Transfer ◽  
Carbon Dioxide ◽  
Heat Exchanger ◽  
Supercritical Carbon Dioxide ◽  
Turbulent Heat Transfer ◽  
Turbulent Heat ◽  
Brayton Cycle ◽  
Heat Exchanger Design ◽  
Transfer Behavior ◽  
Supercritical Carbon

Competitive cycles must have a minimal initial cost and be inherently efficient. Currently, the supercritical carbon dioxide (S-CO2) Brayton cycle is under consideration for these very reasons. This paper examines one major challenge of the S-CO2 Brayton cycle: the complexity of heat exchanger design due to the vast change in thermophysical properties near a fluid’s critical point. Turbulent heat transfer experiments using carbon dioxide, with Reynolds numbers up to 100 K, were performed at pressures of 7.5–10.1 MPa, at temperatures spanning the pseudocritical temperature. The geometry employed nine semicircular, parallel channels to aide in the understanding of current printed circuit heat exchanger designs. Computational fluid dynamics was performed using FLUENT and compared to the experimental results. Existing correlations were compared, and predicted the data within 20% for pressures of 8.1 MPa and 10.2 MPa. However, near the critical pressure and temperature, heat transfer correlations tended to over predict the heat transfer behavior. It was found that FLUENT gave the best prediction of heat transfer results, provided meshing was at a y+ ∼ 1.

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