Electron microscopy of barium strontium titanate nanostructures in the aluminum oxide matrix

2009 ◽  
Vol 51 (7) ◽  
pp. 1485-1488 ◽  
Author(s):  
O. M. Zhigalina ◽  
K. A. Vorotilov ◽  
A. N. Kuskova ◽  
A. S. Sigov
2019 ◽  
Vol 16 (1) ◽  
pp. 65
Author(s):  
Rahmi Dewi ◽  
Tiara Pertiwi ◽  
Krisman Krisman

The thin film of Barium Strontium Titanate (BST) has been studied withcomposition ofby using sol-gel method that annealed in temperature of 600oC and 650oC. The thin film of BST is characterized by using Field Emission Scanning Electron Microscopy (FESEM) and an impedance spectroscopy. The results of  FESEM characterization for samples in temperature of 600oC and 650oC are 55.83 nm and 84.88 nm in thickness respectively. The result of impedance spectroscopy characterization given frequency values obtained by the impedance value of real and imaginary.The capacitance value at a frequency of 20 Hz from a thin film of BST in temperature of 600oC and 650oC are 69.36Fand138.70F. The dielectric constant of the thin film of BST in temperature of 600oC and 650oC are 22.17 dan 131.56 respectively.


2010 ◽  
Vol 152-153 ◽  
pp. 1013-1016
Author(s):  
Hong Wang ◽  
Jing Yang

Nanometer barium-strontium titanate based coated aluminum oxide (ABST) was prepared by the sol–gel method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrophotometry (FTIR). Its application in speciation of Cr(III) and Cr(VI) from water were studied. The results showed that the nanometer barium-strontium titanate was immobilized on aluminum oxide firmly, becoming a new adsorbent. Two forms of chromium showed different exchange capacities at different pH values, viz. Cr (III) selectively retained at pH 10–13, whereas Cr (VI) retained at pH 1. Hence complete separation of the two forms of chromium is possible. Retained species were eluted with 5mL of 1 mol•L−1 HCl and 1 mol•L−1 NaOH. The Cr(III) and Cr(VI) concentration was measured by atomic absorption spectroscopy. The adsorbent had a promising prospect in the separation of Cr(III) and Cr(VI) in environment water.


2015 ◽  
Vol 18 (53) ◽  
Author(s):  
Rahmi Dewi ◽  
Krisman ◽  
Khaironiati ◽  
Fauziana

Sampel Barium Strontium Titanate, Ba0.8Sr0.2TiO3 (BST) telah disediakan dengan menggunakan reaksi kimia padatan. Mikrostruktur sampel telah dikarakterisasi dengan menggunakan teknik difraksi sinar-X (XRD) dan Scanning  Electron Microscopy (SEM). Sampel disediakan dengan variasi suhu yang berbeda yaitu pada suhu 600oC, 700 oC dan 800oC selama 60 menit di udara. Karakterisasi XRD menunjukkan dengan meningkatnya suhu annealing maka kristaline sampel semakin meningkat dengan struktur tetragonal. Karakterisasi SEM menunjukkan sampel adalah homogen dengan ukuran butiran  seragam. Ukuran butiran sampel akan bertambah dengan bertambahnya suhu annealing. Seluruh sampel mempunyai ukuran butiran dalam nanometer.


2010 ◽  
Vol 26-28 ◽  
pp. 682-685 ◽  
Author(s):  
Dong Zhang ◽  
Chun Li Zhang

Nanometer barium-stroutium titanate immobilized on aluminum oxide (ABST) was prepared by the citric acid sol–gel method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrophotometry (FTIR). Its Pb2+ and Cd2+ adsorption properties from water were studied. Adsorption and elution were investigated under different conditions. The results showed that the nanometer barium-strontium titanate was immobilized on aluminum oxide firmly, becoming a composite adsorbent. The lead and cadmium ions were quantitatively retained at pH 5-8; their adsorption capacities of ABST were 70.28 mg•g-1 and 8.12 mg•g-1, respectively. The adsorbent of adsorped lead and cadmium ions were regenerated completely by elution with 1 mol•L-1 HNO3. The adsorbent had a promising prospect in analyticl chemistry and water treatment.


2018 ◽  
Vol 649 ◽  
pp. 187-191 ◽  
Author(s):  
Hong Yan ◽  
Junyuan Wang ◽  
Bing Yang ◽  
Shuanhu Wang ◽  
Hui Xing ◽  
...  

Author(s):  
Rahmi Dewi ◽  
Krisman Krisman ◽  
Tiara Pertiwi ◽  
Tengku Luqman

Lapisan tipis Barium Strontium Titanate (BST) telah ditelaah dengan komposisi  Ba0.75 Sr0.25 TiO3 menggunakan metode sol-gel yang digabungkan pada suhu 600 dan 650oC. Lapisan tipis BST dikarakterisasi menggunakan Field Emission Scanning Electron Microscopy (FESEM) dan spektroskopi impedansi. Hasil dari karakterisasi FESEM untuk sampel pada suhu 600 dan 650oC ialah 55.83 nm dan 84.88 nm dari segi ketebalan secara berurutan. Hasil dari karakterisasi spektroskopi impedansi berdasarkan nilai frekuensi menunjukkan nilai impedansi yang nyata dan imajiner. Nilai kapasitsa pada frekuensi 20 Hz dari lapisan tipis BST pada suhu 600 dan 650oC ialah 69.36 dan 138.70 F. Konstanta dielektrik dari lapisan tipis BST pada suhu 600 dan 650oC ialah 22.17 dan 131.56 secara berurutan.   The thin film of Barium Strontium Titanate (BST) has been studied with composition of Ba0.75 Sr0.25 TiO3 by using sol-gel method that annealed in temperature of 600oC and 650oC. The thin film of BST is characterized by using Field Emission Scanning Electron Microscopy (FESEM) and an impedance spectroscopy. The results of FESEM characterization for samples in temperature of 600 dan 650oC are 55.83 nm and 84.88 nm in thickness respectively. The result of impedance spectroscopy characterization given frequency values obtained by the impedance value of real and imaginary.The capacitance value at a frequency of 20 Hz from a thin film of BST in temperature of 600 dan 650oC are 69.36 F and 138.7oF. The dielectric constant of the thin film of BST in temperature of 600 dan 650oC are 22.17 and 131.56 respectively.


2021 ◽  
Vol 1 (1) ◽  
pp. 71-82
Author(s):  
V. Kavitha ◽  
V. Ragavendran ◽  
N. Sethupathi ◽  
Suresh Sagadevan ◽  
V. Sasirekha ◽  
...  

Gadolinium (Gd) doped barium strontium titanate (BST) was prepared using the microwave-assisted solid-state reaction method for dye sensitized solar cell (DSSC) applications. The optical properties and the structural analysis of the prepared samples reveal the optical band gap and the morphology. The XRD pattern of the annealed samples confirms the polycrystalline nature with the cubic crystal structure. When the dopant is added, the bandgap increases slightly from 3.11 to 3.27 eV. The J-V characteristics of DSSCs prepared with pure and doped BST were investigated. The efficiency of the DSSCs remained constant and there is a slight increase in the Jsc for highly doped samples under 1-sun illumination. Gadolinium doped barium strontium titanate shows variation in the J-V characteristics and could be a potential candidate for the solar photovoltaic applications.


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