Water Content Measurement of Gas Diffusion Media and Membranes by Neutron Radiography

2019 ◽  
Vol 33 (1) ◽  
pp. 1385-1395 ◽  
Author(s):  
Daniel S. Hussey ◽  
Elias Baltic ◽  
David Jacobson
2014 ◽  
Vol 64 (3) ◽  
pp. 839-851 ◽  
Author(s):  
T. Kotaka ◽  
Y. Tabuchi ◽  
U. Pasaogullari ◽  
C.-Y. Wang

2021 ◽  
Vol 42 (3) ◽  
Author(s):  
Rudolf Aro ◽  
Mohamed Wajdi Ben Ayoub ◽  
Ivo Leito ◽  
Éric Georgin ◽  
Benoit Savanier

AbstractIn the field of water content measurement, the calibration of coulometric methods (e.g., coulometric Karl Fischer titration or evolved water vapor analysis) is often overlooked. However, as coulometric water content measurement methods are used to calibrate secondary methods, their results must be obtained with the highest degree of confidence. The utility of calibrating such instruments has been recently demonstrated. Both single and multiple point calibration methods have been suggested. This work compares these calibration methods for the evolved water vapor analysis technique. Two uncertainty estimation approaches (Kragten’s spreadsheet and M-CARE software tool) were compared as well, both based on the ISO GUM method.


Author(s):  
Pradyumna Challa ◽  
James Hinebaugh ◽  
A. Bazylak

In this paper, through-plane liquid water distribution is analyzed for two polymer electrolyte membrane fuel cell (PEMFC) gas diffusion layers (GDLs). The experiments were conducted in an ex situ flow field apparatus with 1 mm square channels at two distinct flow rates to mimic water production rates of 0.2 and 1.5 A/cm2 in a PEMFC. Synchrotron radiography, which involves high intensity monochromatic X-ray beams, was used to obtain images with a spatial and temporal resolution of 20–25 μm and 0.9 s, respectively. Freudenberg H2315 I6 exhibited significantly higher amounts of water than Toray TGP-H-090 at the instance of breakthrough, where breakthrough describes the event in which liquid water reaches the flow fields. While Freudenberg H2315 I6 exhibited a significant overall decrease in liquid water content throughout the GDL shortly after breakthrough, Toray TGP-H-090 appeared to retain breakthrough water-levels post-breakthrough. It was also observed that the amount of liquid water content in Toray TGP-H-090 (10%.wt PTFE) decreased significantly when the liquid water injection rate increased from 1 μL/min to 8 μL/min.


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