scholarly journals Simple Synthesis and Characterization of Cobalt Ferrite Nanoparticles by a Thermal Treatment Method

2010 ◽  
Vol 2010 ◽  
pp. 1-8 ◽  
Author(s):  
Mahmoud Goodarz Naseri ◽  
Elias B. Saion ◽  
Hossein Abbastabar Ahangar ◽  
Abdul Halim Shaari ◽  
Mansor Hashim
Keyword(s):  
Thermal Treatment ◽  
Cobalt Ferrite ◽  
Structural Characteristics ◽  
Treatment Method ◽  
Ferrite Nanoparticles ◽  
Absorption Bands ◽  
Cobalt Ferrite Nanoparticles ◽  
Metal Nitrates ◽  
Transmission Electron ◽  
Ft Ir

Crystalline, magnetic, cobalt ferrite nanoparticles were synthesized from an aqueous solution containing metal nitrates and polyvinyl pyrrolidone (PVP) as a capping agent by a thermal treatment followed by calcination at various temperatures from 673 to 923 K. The structural characteristics of the calcined samples were determined by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and transmission electron microscopy (TEM). A completed crystallization occurred at 823 and 923 K, as shown by the absence of organic absorption bands in the FT-IR spectrum. Magnetization measurements were obtained at room temperature by using a vibrating sample magnetometer (VSM), which showed that the calcined samples exhibited typical magnetic behaviors.

scholarly journals An Overview on Nanocrystalline ZnFe2O4, MnFe2O4, and CoFe2O4 Synthesized by a Thermal Treatment Method

2012 ◽  
Vol 2012 ◽  
pp. 1-11 ◽  
Author(s):  
Mahmoud Goodarz Naseri ◽  
Elias B. Saion ◽  
Ahmad Kamali
Keyword(s):  
Thermal Treatment ◽  
Treatment Method ◽  
Vinyl Pyrrolidone ◽  
Average Particle ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
Ft Ir ◽  
Poly Vinyl Pyrrolidone ◽  
Co Nanoparticles ◽  
Oxide Bands

This study reports the simple synthesis of MFe2O4 (where M=Zn, Mn, and Co) nanoparticles by a thermal treatment method, followed by calcination at various temperatures from 723 to 873 K. Poly(vinyl pyrrolidone) (PVP) was used as a capping agent to stabilize the particles and prevent them from agglomeration. The characterization studies were conducted by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The average particle sizes were obtained by TEM images, which were in good agreement with the XRD results. Fourier transform infrared spectroscopy (FT-IR) confirmed the presence of metal oxide bands for all the calcined samples. Magnetic properties were demonstrated by a vibrating sample magnetometer (VSM), which displayed that the calcined samples exhibited superparamagnetic and ferromagnetic behaviors.

scholarly journals Synthesis and Characterization of a Core-shell Material Using YBa2Cu3O7-d and Cobalt Ferrite Nanoparticles

2019 ◽  
Vol 69 (12) ◽  
pp. 3345-3348
Author(s):  
Maria Colie ◽  
Dan Eduard Mihaiescu ◽  
Daniela Istrati ◽  
Adrian Vasile Surdu ◽  
Bogdan Vasile ◽  
...  
Keyword(s):  
Cobalt Ferrite ◽  
Nanostructured Material ◽  
Ferrite Nanoparticles ◽  
Precipitation Method ◽  
Core Shell ◽  
Shell Material ◽  
X Ray ◽  
Cobalt Ferrite Nanoparticles ◽  
Transmission Electron ◽  
Co Precipitation

In this paper we describe the synthesis of a core-shell material using yttrium superconducting ceramic material (YBCO) and cobalt ferrite nanoparticles in order to obtain a nanostructured material with magnetic properties. The advantages of such material aim the selective deposition of nanofilms oriented in magnetic fields. To obtain this core-shell material, the solutions of the nitrates were first obtained by dissolving the salts in demineralised water. The suspension with cobalt ferrite nanoparticles was obtained by co-precipitation method. To obtain YBa2Cu3O7-�- coated magnetic nanoparticles by autocombustion reaction the solutions of nitrates and citric acid were used. The ratio of the metal ions: Y:Ba:Cu was 1:2:3, and between the oxidant and the reducing agent was used a citrate / nitrate mass ratio equal with 0.7. The final material was analyzed by X-ray diffraction (XRD), electronic scanning microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), high resolution transmission electron microscopy (HRTEM) and vibrating sample magnetometer (VSM).

scholarly journals Antibacterial and Antifungal Activity of Novel Synthesized Neodymium-Substituted Cobalt Ferrite Nanoparticles for Biomedical Application

Processes ◽  
2019 ◽  
Vol 7 (10) ◽  
pp. 714 ◽  
Author(s):  
Rehman ◽  
Ansari ◽  
Alzohairy ◽  
Alomary ◽  
Jermy ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Survival Rate ◽  
Cobalt Ferrite ◽  
Biomedical Application ◽  
Ferrite Nanoparticles ◽  
Sonochemical Method ◽  
Cobalt Ferrite Nanoparticles ◽  
Transmission Electron ◽  
Antistaphylococcal Activity ◽  
Antibacterial And Antifungal

Neodymium (Nd)-substituted cobalt ferrite nanoparticles (NPs), i.e., CoNdxFe2−xO4 (0.0 ≤ x ≤ 0.2) NPs, were synthesized by the sonochemical method. The compositional characterization was done by scanning electron microscopy (SEM) equipped with energy-dispersive X-ray spectroscopy (EDX) and transmission electron microscopy (TEM). Antistaphylococcal activity was found to be enhanced, i.e., survival rate was 50%, 45%, 40%, and 30% with the increase in the ratio of Nd (0.0 ≤ x ≤ 0.2), whereas anticandidal activity was found efficient, i.e., 9%, 20%, 22%, and 40% survival rate at all the four ratios. The morphogenesis studies indicated that the synthesized metal–ligand, improves the antimicrobial capacity by binding them strongly to the microbial walls. To the best of our knowledge, this is the first report which demonstrates the series of CoNdxFe2−xO4 (0.0 ≤ x ≤ 0.2) NPs being active towards Staphylococcus aureus and Candida albicans and encourages its potential candidature for pharmaceutical and biomedical purposes.

scholarly journals Biological synthesis of cobalt ferrite nanoparticles

2012 ◽  
Vol 2 (1) ◽  
pp. 9 ◽  
Author(s):  
Anal K. Jha ◽  
Kamal Prasad
Keyword(s):  
Room Temperature ◽  
Cobalt Ferrite ◽  
Low Cost ◽  
Ferrite Nanoparticles ◽  
Biological Synthesis ◽  
Vibrating Sample Magnetometer ◽  
X Ray ◽  
Cobalt Ferrite Nanoparticles ◽  
Transmission Electron ◽  
Individual Nanoparticles

A low-cost green and reproducible yeast (<em>Saccharomyces cerevisiae</em>) mediated biosynthesis of cobalt ferrite nanoparticles is reported. The synthesis is performed at close to room temperature in the laboratory. X-ray, Fourier transform infrared spectroscopy and high resolution transmission electron microscopy analyses are performed to ascertain the formation of cobalt ferrite nanoparticles. Individual nanoparticles, as well as a very few aggregate having the size of 3-15 nm, were found. The vibrating sample magnetometer measurement showed superparamagnetic behavior in cobalt ferrite nanoparticles. The mechanism involved in the biosynthesis of cobalt ferrite nanoparticles has also been discussed.

scholarly journals Synthesis, Characterization and Magnetic Hyperthermia of Monodispersed Cobalt Ferrite Nanoparticles for Cancer Therapeutics

Molecules ◽  
2020 ◽  
Vol 25 (19) ◽  
pp. 4428
Author(s):  
Mauricio A. Medina ◽  
Goldie Oza ◽  
A. Ángeles-Pascual ◽  
Marlene González M. ◽  
R. Antaño-López ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Cobalt Ferrite ◽  
Magnetic Measurements ◽  
Cancer Therapeutics ◽  
Physiological Saline ◽  
Dark Field ◽  
Ferrite Nanoparticles ◽  
Cobalt Ferrite Nanoparticles ◽  
Transmission Electron

Magnetic nanoparticles such as cobalt ferrite are investigated under clinical hyperthermia conditions for the treatment of cancer. Cobalt ferrite nanoparticles (CFNPs) synthesized by the thermal decomposition method, using nonionic surfactant Triton-X100, possess hydrophilic polyethylene oxide chains acting as reducing agents for the cobalt and iron precursors. The monodispersed nanoparticles were of 10 nm size, as confirmed by high-resolution transmission electron microscopy (HR-TEM). The X-ray diffraction patterns of CFNPs prove the existence of cubic spinel cobalt ferrites. Cs-corrected scanning transmission electron microscopy–high-angle annular dark-field imaging (STEM–HAADF) of CFNPs confirmed their multi-twinned crystallinity due to the presence of atomic columns and defects in the nanostructure. Magnetic measurements proved that the CFNPs possess reduced remnant magnetization (MR/MS) (0.86), which justifies cubic anisotropy in the system. Microwave-based hyperthermia studies performed at 2.45 GHz under clinical conditions in physiological saline increased the temperature of the CFNP samples due to the transformation of radiation energy to heat. The specific absorption rate of CFNPs in physiological saline was 68.28 W/g. Furthermore, when triple-negative breast cancer cells (TNBC) in the presence of increasing CFNP concentration (5 mg/mL to 40 mg/mL) were exposed to microwaves, the cell cytotoxicity was enhanced compared to CFNPs alone.

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