scholarly journals Antibacterial and Antifungal Activity of Novel Synthesized Neodymium-Substituted Cobalt Ferrite Nanoparticles for Biomedical Application

Processes ◽  
2019 ◽  
Vol 7 (10) ◽  
pp. 714 ◽  
Author(s):  
Rehman ◽  
Ansari ◽  
Alzohairy ◽  
Alomary ◽  
Jermy ◽  
...  

Neodymium (Nd)-substituted cobalt ferrite nanoparticles (NPs), i.e., CoNdxFe2−xO4 (0.0 ≤ x ≤ 0.2) NPs, were synthesized by the sonochemical method. The compositional characterization was done by scanning electron microscopy (SEM) equipped with energy-dispersive X-ray spectroscopy (EDX) and transmission electron microscopy (TEM). Antistaphylococcal activity was found to be enhanced, i.e., survival rate was 50%, 45%, 40%, and 30% with the increase in the ratio of Nd (0.0 ≤ x ≤ 0.2), whereas anticandidal activity was found efficient, i.e., 9%, 20%, 22%, and 40% survival rate at all the four ratios. The morphogenesis studies indicated that the synthesized metal–ligand, improves the antimicrobial capacity by binding them strongly to the microbial walls. To the best of our knowledge, this is the first report which demonstrates the series of CoNdxFe2−xO4 (0.0 ≤ x ≤ 0.2) NPs being active towards Staphylococcus aureus and Candida albicans and encourages its potential candidature for pharmaceutical and biomedical purposes.

Molecules ◽  
2020 ◽  
Vol 25 (19) ◽  
pp. 4428
Author(s):  
Mauricio A. Medina ◽  
Goldie Oza ◽  
A. Ángeles-Pascual ◽  
Marlene González M. ◽  
R. Antaño-López ◽  
...  

Magnetic nanoparticles such as cobalt ferrite are investigated under clinical hyperthermia conditions for the treatment of cancer. Cobalt ferrite nanoparticles (CFNPs) synthesized by the thermal decomposition method, using nonionic surfactant Triton-X100, possess hydrophilic polyethylene oxide chains acting as reducing agents for the cobalt and iron precursors. The monodispersed nanoparticles were of 10 nm size, as confirmed by high-resolution transmission electron microscopy (HR-TEM). The X-ray diffraction patterns of CFNPs prove the existence of cubic spinel cobalt ferrites. Cs-corrected scanning transmission electron microscopy–high-angle annular dark-field imaging (STEM–HAADF) of CFNPs confirmed their multi-twinned crystallinity due to the presence of atomic columns and defects in the nanostructure. Magnetic measurements proved that the CFNPs possess reduced remnant magnetization (MR/MS) (0.86), which justifies cubic anisotropy in the system. Microwave-based hyperthermia studies performed at 2.45 GHz under clinical conditions in physiological saline increased the temperature of the CFNP samples due to the transformation of radiation energy to heat. The specific absorption rate of CFNPs in physiological saline was 68.28 W/g. Furthermore, when triple-negative breast cancer cells (TNBC) in the presence of increasing CFNP concentration (5 mg/mL to 40 mg/mL) were exposed to microwaves, the cell cytotoxicity was enhanced compared to CFNPs alone.


Author(s):  
Dominique Piché ◽  
Juan G Lozano ◽  
Aakash Varambhia ◽  
Frank Dillon ◽  
Lewys Jones ◽  
...  

2019 ◽  
Vol 69 (12) ◽  
pp. 3345-3348
Author(s):  
Maria Colie ◽  
Dan Eduard Mihaiescu ◽  
Daniela Istrati ◽  
Adrian Vasile Surdu ◽  
Bogdan Vasile ◽  
...  

In this paper we describe the synthesis of a core-shell material using yttrium superconducting ceramic material (YBCO) and cobalt ferrite nanoparticles in order to obtain a nanostructured material with magnetic properties. The advantages of such material aim the selective deposition of nanofilms oriented in magnetic fields. To obtain this core-shell material, the solutions of the nitrates were first obtained by dissolving the salts in demineralised water. The suspension with cobalt ferrite nanoparticles was obtained by co-precipitation method. To obtain YBa2Cu3O7-�- coated magnetic nanoparticles by autocombustion reaction the solutions of nitrates and citric acid were used. The ratio of the metal ions: Y:Ba:Cu was 1:2:3, and between the oxidant and the reducing agent was used a citrate / nitrate mass ratio equal with 0.7. The final material was analyzed by X-ray diffraction (XRD), electronic scanning microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), high resolution transmission electron microscopy (HRTEM) and vibrating sample magnetometer (VSM).


2012 ◽  
Vol 2 (1) ◽  
pp. 9 ◽  
Author(s):  
Anal K. Jha ◽  
Kamal Prasad

A low-cost green and reproducible yeast (<em>Saccharomyces cerevisiae</em>) mediated biosynthesis of cobalt ferrite nanoparticles is reported. The synthesis is performed at close to room temperature in the laboratory. X-ray, Fourier transform infrared spectroscopy and high resolution transmission electron microscopy analyses are performed to ascertain the formation of cobalt ferrite nanoparticles. Individual nanoparticles, as well as a very few aggregate having the size of 3-15 nm, were found. The vibrating sample magnetometer measurement showed superparamagnetic behavior in cobalt ferrite nanoparticles. The mechanism involved in the biosynthesis of cobalt ferrite nanoparticles has also been discussed.


2019 ◽  
Vol 10 (1) ◽  
pp. 4752-4763

Cadmium cobalt ferrite nanoparticles with a chemical formula of CdxCo1-xFe2O4 (x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 & 0.6) (CCF) were prepared via the citrate-gel auto combustion method followed by annealing at 773 Kelvin for 4 hrs in air. Further, the samples were characterized for structural, morphological, elemental, functional group, electrical and thermoelectric properties analysis. The X-ray diffraction patterns showed the single phase cubic structure. The crystalline size of the synthesized Co-Cd ferrites nanoparticle is found in the range of 11 to17 nm. In addition, with an increase of Cd content, we noticed that lattice constants (a) and x-ray density (dx) values were increasing from 0.8419 – 0.8496 nm and 5.222 – 5.777 g/c.c., respectively. Morphological properties were examined by scanning electron microscopy (SEM) & Transmission electron microscopy (TEM). The tetrahedral (υ1) and octahedral (υ2) frequencies were observed at around 400 - 600 cm-1. The electric and dielectric properties such as DC-electrical conductivity (σdc), dielectric constant (ε'), dielectric loss (ε") and thermoelectric power parameters were calculated. At a low temperature of 300 K, the samples express the p-type semiconducting nature due to having +ve value of ‘S’ while the same shows –ve value at high temperature suggesting the n-type semiconducting behavior. Moreover, the magnetic Curie-transition temperatures were determined as a function of composition and noted to be decreasing from 753 – 653 K respectively.


2010 ◽  
Vol 2010 ◽  
pp. 1-8 ◽  
Author(s):  
Mahmoud Goodarz Naseri ◽  
Elias B. Saion ◽  
Hossein Abbastabar Ahangar ◽  
Abdul Halim Shaari ◽  
Mansor Hashim

Crystalline, magnetic, cobalt ferrite nanoparticles were synthesized from an aqueous solution containing metal nitrates and polyvinyl pyrrolidone (PVP) as a capping agent by a thermal treatment followed by calcination at various temperatures from 673 to 923 K. The structural characteristics of the calcined samples were determined by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and transmission electron microscopy (TEM). A completed crystallization occurred at 823 and 923 K, as shown by the absence of organic absorption bands in the FT-IR spectrum. Magnetization measurements were obtained at room temperature by using a vibrating sample magnetometer (VSM), which showed that the calcined samples exhibited typical magnetic behaviors.


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