scholarly journals Magnetization and Specific Absorption Rate Studies of Ball-Milled Iron Oxide Nanoparticles for Biomedicine

2013 ◽  
Vol 2013 ◽  
pp. 1-13 ◽  
Author(s):  
P. Burnham ◽  
N. Dollahon ◽  
C. H. Li ◽  
A. J. Viescas ◽  
G. C. Papaefthymiou

Comparative studies are presented of iron oxide nanoparticles in the 7–15 nm average diameter range ball milled in hexane in the presence of oleic acid. Transmission electron microscopy identified spherical particles of decreasing size as milling time and/or surfactant concentration increased. Micromagnetic characterization via Mössbauer spectroscopy at room temperature yielded broadened magnetic spectroscopic signatures, while macromagnetic characterization via vibrating sample magnetometry of 7-8 nm diameter particles showed largely superparamagnetic behavior at room temperature and hysteretic at 2 K. Zero-field and field-cooled magnetization curves exhibited a broad maximum at ~215 K indicating the presence of strong interparticle magnetic interactions. The specific absorption rates of ferrofluids based on these nanoparticle preparations were measured in order to test their efficacies as hyperthermia agents.

2015 ◽  
Vol 230 ◽  
pp. 108-113 ◽  
Author(s):  
O.V. Yelenich ◽  
S.O. Solopan ◽  
T.V. Kolodiazhnyi ◽  
Jean Marc Greneche ◽  
Anatolii G. Belous

In this work, iron oxide nanoparticles have been synthesized by precipitation in diethylene glycol, by cryochemical synthesis, in microemulsions using surfactants Triton X-100, Brij-35 and CTAB. Comparative spectroscopic, thermal, X-ray diffraction, 57Fe zero-field Mössbauer and magnetic studies of the synthesized nanoparticles have been carried out. Magnetic fluids prepared from synthesized nanopowders have been characterized by calorimetric measurements of specific loss power (SLP).


2021 ◽  
Author(s):  
Lukasz Kilanski ◽  
Roman Jedrzejewski ◽  
Daniel Sibera ◽  
I Kuryliszyn-Kudelska ◽  
Sandeep M. Gorantla ◽  
...  

Author(s):  
Nicholas J. Hobson ◽  
Xian Weng ◽  
Marianne Ashford ◽  
Nguyen T.K. Thanh ◽  
Andreas G. Schätzlein ◽  
...  

2009 ◽  
Vol 152-153 ◽  
pp. 205-208 ◽  
Author(s):  
H. Arabi ◽  
S. Nateghi ◽  
S. Sadeghi

Iron oxide nanoparticles were synthesis by reverse micelle method. X-ray diffraction technique and vibration sample magnetometer were applied to characterize the produced samples at different conditions and parameters for synthesis route. There is no significant difference between samples prepared at 5°C and room temperature except a better crystalline at room temperature. The molar ratio of water to surfactant (w parameter) and concentration of the salt solution on size and magnetic properties of nanoparticles have been investigated. Increasing w leads to producing particles with larger size i.e. for w=16.83, 11.22, and 5.6, particles size are 15.22, 11.66 and 10.5 nm, respectively. The size of nanoparticles are in the range of 9 to 20 nanometers


RSC Advances ◽  
2016 ◽  
Vol 6 (112) ◽  
pp. 111099-111108 ◽  
Author(s):  
Nikesh Gupta ◽  
Chetna Gupta ◽  
Sandeep Sharma ◽  
Brijesh Rathi ◽  
Rakesh Kumar Sharma ◽  
...  

We report synthesis of iron oxide nanoparticles encapsulating HRP. The average diameter of the particles was around 20 nm. HRP has been used to convert IAA to a toxic oxidized product and its toxic effect has been seen on cancerous cell lines.


2004 ◽  
Vol 43 (45) ◽  
pp. 6135-6139 ◽  
Author(s):  
Rie Mikami ◽  
Minori Taguchi ◽  
Koji Yamada ◽  
Koji Suzuki ◽  
Osamu Sato ◽  
...  

2015 ◽  
Vol 15 (5) ◽  
pp. 3870-3878 ◽  
Author(s):  
S. Vikram ◽  
M. Dhakshnamoorthy ◽  
R. Vasanthakumari ◽  
A. R. Rajamani ◽  
Murali Rangarajan ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-7 ◽  
Author(s):  
Alina Mihaela Prodan ◽  
Simona Liliana Iconaru ◽  
Carmen Mariana Chifiriuc ◽  
Coralia Bleotu ◽  
Carmen Steluta Ciobanu ◽  
...  

The aim of this study was to provide information about the biological properties of iron oxide nanoparticles (IO-NPs) obtained in an aqueous suspension. The IO-NPs were characterized by transmission electron microscopy (TEM). Analysis of hysteresis loops data at room temperature for magnetic IO-NPs sample indicated that the IO-NPs were superparamagnetic at room temperature. The calculated saturation magnetization for magnetic iron oxide wasMs= 18.1 emu/g. The antimicrobial activity of the obtained PMC-NPs was tested against Gram-negative (Pseudomonas aeruginosa1397,Escherichia coliATCC 25922), Gram-positive (Enterococcus faecalisATCC 29212,Bacillus subtilisIC 12488) bacterial as well as fungal (Candida krusei963) strains. The obtained results suggested that the antimicrobial activity of IO-NPs is dependent on the metallic ions concentrations and on the microbial growth state, either planktonic or adherent. The obtained IO-NPs exhibited no cytotoxic effect on HeLa cells at the active antimicrobial concentrations.


Sign in / Sign up

Export Citation Format

Share Document