scholarly journals The Preparation and Performances of Self-Dispersed Nanomicron Emulsified Wax Solid Lubricant Ewax for Drilling Fluids

2014 ◽  
Vol 2014 ◽  
pp. 1-7
Author(s):  
Feng-shan Zhou ◽  
Ting-ting Wang ◽  
Zheng-qiang Xiong ◽  
Wen-yue Guo ◽  
Xi Xiang ◽  
...  

An oil-in-water nanomicron wax emulsion with oil phase content 45 wt% was prepared by using the emulsifying method of surfactant-in-oil. The optimum prepared condition is 85°C, 20 min, and 5 wt% complex emulsifiers. Then the abovementioned nanomicron emulsifying wax was immersed into a special water-soluble polymer in a certain percentage by the semidry technology. At last, a solidified self-dispersed nanomicron emulsified wax named as Ewax, a kind of solid lubricant for water based drilling fluid, was obtained after dried in the special soluble polymer containing emulsifying wax in low temperature. It is shown that the adhesion coefficient reduced rate(ΔKf)is 73.5% and the extreme pressure (E-P) friction coefficient reduced rate(Δf)is 77.6% when the produced Ewax sample was added to fresh water based drilling fluid at dosage 1.0 wt%. In comparison with other normal similar liquid products, Ewax not only has better performances of lubrication, filtration loss control property, heat resistance, and tolerance to salt and is environmentally friendly, but also can solve the problems of freezing in the winter and poor storage stability of liquid wax emulsion in oilfield applications.

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Jinliang Liu ◽  
Fengshan Zhou ◽  
Fengyi Deng ◽  
Hongxing Zhao ◽  
Zhongjin Wei ◽  
...  

Abstract Most of bentonite used in modern drilling engineering is physically and chemically modified calcium bentonite. However, with the increase of drilling depth, the bottom hole temperature may reach 180 °C, thus a large amount of calcium bentonite used in the drilling fluid will be unstable. This paper covers three kinds of calcium bentonite with poor rheological properties at high temperature, such as apparent viscosity is greater than 45 mPa·s or less than 10 mPa·s, API filtration loss is greater than 25 mL/30 min, which are diluted type, shear thickening type and low-shear type, these defects will make the rheological properties of drilling fluid worse. The difference is attributed to bentonite mineral composition, such as montmorillonite with good hydration expansion performance. By adding three kinds of heat-resistant water-soluble copolymers Na-HPAN (hydrolyzed polyacrylonitrile sodium), PAS (polycarboxylate salt) and SMP (sulfomethyl phenolic resin), the rheological properties of calcium bentonite drilling fluids can be significantly improved. For example, the addition of 0.1 wt% Na-HPAN and 0.1 wt% PAS increased the apparent viscosity of the XZJ calcium bentonite suspension from 4.5 to 19.5 mPa·s at 180 °C, and the filtration loss also decreased from 20.2 to 17.8 mL.


1999 ◽  
Author(s):  
Danuta Bielewicz ◽  
Lucja Kraj ◽  
Edgar Bortel ◽  
Ewa Witek

2013 ◽  
Vol 829 ◽  
pp. 818-824
Author(s):  
Sahar Kafashi ◽  
Ramin Taghdimi ◽  
Gholamreza Karimi

This study was aimed to investigate the rheological properties and the possibility of nano(Na, Ca )- bentonites nanoproducts to meet the required drilling mud properties. Sepiolite (Sp) and the mixture of 2% nanoNaB with 1% Sp were collected and prepared from Irans oil Company (NIOC). The nanoclay performance evaluation involved the experimental tests of the rheological properties, filtration and gel strength. According to the results obtained from flow properties tests for the mixture, it was indicated that the mixture was not adequate to be a suitable drilling fluid. The main objective was to make stable dispersions with nanobentonite and sepiolite by using a water soluble polymer as stabilizer. The changes in the rheological properties of bentonite were investigated at various concentrations of polyvinyl alcohol (PVA) to discover the stability of the dispersions. The standard API tests were applied for drilling fluid to determine the properties of dispersions.


Polymers ◽  
2021 ◽  
Vol 13 (18) ◽  
pp. 3120
Author(s):  
Xianfeng Tan ◽  
Longchen Duan ◽  
Weichao Han ◽  
Ying Li ◽  
Mingyi Guo

To overcome the negative impact on the rheological and filtration loss properties of drilling fluids caused by elevated temperature and salts contamination, which are common in ultradeep or geothermal drilling operations, it is imperative to develop highly efficient additives used in the water-based drilling fluid. In this study, a zwitterionic copolymer P (AM/DMC/AMPS/DMAM, ADAD) was synthesized by using acrylamide (AM), cationic monomer methacrylatoethyl trimethyl ammonium chloride (DMC), anionic monomer 2-acrylamide-2-methyl propane sulfonic acid (AMPS), and N,N-dimethylacrylamide (DMAM) through free radical copolymerization. The copolymer was characterized by 1H Nuclear Magnetic Resonance (NMR), Fourier transform infrared spectroscopy (FTIR), elemental analysis, thermogravimetric analysis (TGA), and zeta potential. The rheological behavior, filtration properties, and the performance exposure to salt or calcium contamination in water-based drilling fluid were investigated. The bentonite/polymer suspension showed improved rheological and filtration properties even after aging at 160 °C or a high concentration of salt and calcium. The filtration loss can be greatly reduced by more than 50% (from 18 mL to 7 mL) by the inclusion of 2.0 wt% copolymer, while a slight increase in the filtrate loss was observed even when exposed to electrolyte contamination. Particle size distribution and zeta potential further validate the idea that zwitterionic copolymer can greatly improve the stability of base fluid suspension through positive group enhanced anchoring on the clay surface and repulsion force between negative particles. Moreover, this study can be directed towards the design and application of zwitterionic copolymer in a water-based drilling fluid.


Author(s):  
Ved Prakash ◽  
Neetu Sharma ◽  
Munmun Bhattacharya

AbstractRheological and filtration properties of drilling fluid contribute a vital role in successful drilling operations. Rheological parameters such as apparent viscosity (AV), plastic viscosity (PV), yield point (YP) and gel strength of drilling fluids are very essential for hydraulic calculations and lifting of drill cuttings during the drilling operation. Control of filtration loss volume is also very important for cost effective and successful drilling operations. Therefore, the main goal of this research is to improve the rheological and filtration properties of Grewia Optiva fibre powder (GOFP) by using 30–50 nm size of silica nano particles (SNP) in water-based drilling fluid. The experimental outcomes revealed that after hot rolling of mud samples at 100 °C for 16 h, the low pressure-low temperature (LPLT) and high pressure-high temperature (HPHT) filtration loss of GOFP additives was improved, after the addition of SNP on it. The mixture of 5% GOFP + 4% SNP has reduced the LPLT and HPHT filtration loss of drilling fluid by 74.03 and 78.12%, respectively, as compared to base mud. Thus, it was concluded that after the addition of 0.4% SNP, the LPLT and HPHT filtration control ability of GOFP additive in WBM were increased by 17.6 and 15%, respectively. The rheological parameters such as AV, PV, YP and gelation of drilling fluids were also improved by the addition of GOFP + SNP mixture in the base mud. Therefore, the implementation of GOFP + SNP mixture in water-based mud showed auspicious results which reaffirm the feasibility of using them in the successful drilling operations.


2021 ◽  
Author(s):  
Aranee Pleng Teepakakorn ◽  
Makoto Ogawa

Water-induced self-healing materials were prepared by the hybridization of a water-soluble polymer, poly(vinyl alcohol), with a smectite clay by mixing in an aqueous media and subsequent casting. Without using chemical...


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