Silane Modified Multiwall Carbon Nanotubes/Polyimide Composites Prepared Using In-Situ Polymerization

2014 ◽  
Vol 6 (3) ◽  
pp. 190-196 ◽  
Author(s):  
Hung-Han Ko ◽  
Yao-Yi Cheng ◽  
Chi-An Dai
2012 ◽  
Vol 531-532 ◽  
pp. 258-261 ◽  
Author(s):  
Gunawan ◽  
Iis Sopyan ◽  
S. Nurfaezah ◽  
M. ‘Ammar

Triphasic calcium phosphate, composed of a more stable phase hydroxyapatite (HA) and highly soluble tricalcium phosphates (α- and β-TCP) has been synthesized through hydrothermal method. In the present work, an in-situ method to disperse 1wt% multiwall carbon nanotubes (MWCNTs) within HA/TCP powder has been used in order to develop HA/TCP-CNTs composite. XRD results confirmed the formation of HA, α-TCP and β-TCP in both as-prepared powder and composite samples. The graphite peaks appeared in the composite samples as well. FTIR analysis of sintered compacted powder showed the formation of weak bands of PO43- as the temperature was increased. The sintered compacts were mechanically tested by Vickers microhardness indentation method. HA/TCP-CNTs composite was found to have a significant of Vickers Hardness of 1.98 GPa after 1100°C sintering. The morphology analysis showed that in-situ deposition technique provides homogeneous dispersion of CNTs in the calcium phosphate matrix.


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