Synthesis of Silver Nanostructures by the Polyol Method and their Statistical Analysis Using Design of Experiments

2012 ◽  
Vol 1371 ◽  
Author(s):  
Jaime E. Pérez ◽  
Adriana B. Arauz ◽  
Luis A. García ◽  
José L. Rodríguez
Keyword(s):  
Statistical Analysis ◽  
Design Of Experiments ◽  
Polyol Process ◽  
Polyol Method ◽  
Synthesis Process ◽  
Silver Nanostructures ◽  
Significant Information ◽  
Injection Speed ◽  
Concentration Time ◽  
Time Of Reaction

ABSTRACTIn this work we present the bases to perform investigation on the effects on the morphology and size of nanostructures of silver, owed to the modification of synthesis factors in a polyol process such as temperature, concentration, time of reaction, injection speed and time of injection. It is claimed that control over Ag nanostructures shape could be improved and significant information about the synthesis process can be obtained. The design of experiments was done aimed to obtain useful information about how to yield as much as possible specific structures of interest.

Using Design of Experiments to Analyze Open Source Software Metrics for Change Impact Estimation

2019 ◽  
Vol 10 (1) ◽  
pp. 16-33
Author(s):  
Miloud Dahane ◽  
Mustapha Kamel Abdi ◽  
Mourad Bouneffa ◽  
Adeel Ahmad ◽  
Henri Basson
Keyword(s):  
Statistical Analysis ◽  
Design Of Experiments ◽  
Open Source Software ◽  
Software Maintenance ◽  
Software Metrics ◽  
Software Evolution ◽  
Measurement Tool ◽  
Software Artifacts ◽  
Change Impact ◽  
Evolution Control

Software evolution control mostly relies on the better structure of the inherent software artifacts and the evaluation of different qualitative factors like maintainability. The attributes of changeability are commonly used to measure the capability of the software to change with minimal side effects. This article describes the use of the design of experiments method to evaluate the influence of variations of software metrics on the change impact in developed software. The coupling metrics are considered to analyze their degree of contribution to cause a change impact. The data from participant software metrics are expressed in the form of mathematical models. These models are then validated on different versions of software to estimate the correlation of coupling metrics with the change impact. The proposed approach is evaluated with the help of a set of experiences which are conducted using statistical analysis tools. It may serve as a measurement tool to qualify the significant indicators that can be included in a Software Maintenance dashboard.

scholarly journals Selection criteria for a radiography programme in South Africa: Predictors for academic success in the first year of study

2016 ◽  
Vol 21 ◽  
pp. 206-213 ◽  
Author(s):  
Carol A. Kridiotis ◽  
Johan Bezuidenhout ◽  
Jacques Raubenheimer
Keyword(s):  
Academic Success ◽  
Statistical Analysis ◽  
Selection Criteria ◽  
Life Sciences ◽  
Study Data ◽  
First Year ◽  
Directed Search ◽  
Physical Sciences ◽  
Significant Information ◽  
Predictive Values

Background: Selection criteria used to admit students to a radiography programme at the Central University of Technology (CUT) included academic criteria, as well as the General Scholastic Aptitude Test (GSAT) and Self-directed Search (SDS) Questionnaire.Aims and objectives: The aim of the study was to identify which selection criteria were predictors of academic success in the first year of study. As a four year Bachelor's degree in Radiography (480 credits) was to replace the three year National Diploma (NDip) in Radiography (360 credits), selection criteria would come under review.Design and method: Data from 130 students were gathered in a retrospective quantitative study. Data were edited, categorised and summarised. A statistical analysis was undertaken to identify which selection criteria predicted academic success in the first year of study.Results: Statistics showed that the matriculation Admission Points Score (National Senior Certificate/NCS APS) and core matriculation subject results in Mathematics, Physical Sciences and English were adequate predictors for first-year academic success, and the subjects Life Sciences for the NSC and Biology for the Senior Certificate (SC), showed strong predictive values for first-year academic success. According to the statistical analysis, the GSAT and SDS Questionnaire did not contribute any significant information which could predict academic success.Conclusion: Matriculation marks and NSC APS were adequate predictors for academic success, with a focus on Life Sciences or Biology marks as the strongest predictor. The usefulness of the GSAT and SDS Questionnaire could be questioned, and a recommendation was made to replace these tests with alternative student selection methods.

scholarly journals The analysis of friction properties after laser texturizing of the silicon carbide surface layer

2018 ◽  
Vol 183 ◽  
pp. 02010
Author(s):  
Norbert Radek ◽  
Agnieszka Szczotok ◽  
Renata Dwornicka
Keyword(s):  
Silicon Carbide ◽  
Surface Layer ◽  
Statistical Analysis ◽  
Design Of Experiments ◽  
Laser Beam ◽  
High Reliability ◽  
Laser Beam Machining ◽  
Before And After ◽  
High Roughness ◽  
Modification Of The Surface

The modification of the surface properties is a desired technological procedure. One of the possible method is the electro-spark deposition (ESD). Unfortunately, ESD process produces a surface with high roughness. The laser beam machining (LBM) has been involved to lower roughness of the coating made by ESD. The elements coated by ESD have been tested to determine tribological properties and they were compared before and after LBM. To achieve high reliability of the results, the test has been conducted in accordance with design of experiments methodology and the results which were obtained have been processed by a statistical analysis. The description of such an experiment performed for a silicon carbide SiC coating, the obtained results and the conclusions are included in this paper.

A Methodology for Quantifying the Perceived Environmental Friendliness of Vehicle Silhouettes in Engineering Design

2009 ◽  
Author(s):  
Tahira Reid ◽  
Richard Gonzalez ◽  
Panos Papalambros
Keyword(s):  
Statistical Analysis ◽  
Design Of Experiments ◽  
Design Optimization ◽  
Engineering Design ◽  
Survey Design ◽  
Modeling Method ◽  
Modeling Framework ◽  
Environmental Friendliness ◽  
Design Attributes

Methods from psychology and engineering are used to quantify subjective, or perceptual, design attributes of artifacts. A modeling framework of perceptual attributes suitable for inclusion in design optimization is presented. The framework includes stimuli development based on design of experiments, survey design, and statistical analysis of data. The proposed modeling method is demonstrated on a subjective attribute we call ‘perceived environmental friendliness’ using vehicle silhouettes as a case study.

Study on Hydrothermal Process Variables Correlation to WO3 Nanostructure through Design of Experiments (DOE) Approach

2014 ◽  
Vol 607 ◽  
pp. 47-50
Author(s):  
Amirul Abd Rashid ◽  
Nor Hayati Saad ◽  
Daniel Bien Chia Sheng ◽  
Kah Yaw Lee ◽  
Wai Yee Lee ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Design Of Experiments ◽  
Tungsten Trioxide ◽  
Ph Value ◽  
Hydrothermal Process ◽  
Synthesis Temperature ◽  
Synthesis Process ◽  
Process Variables ◽  
Material Source ◽  
Experimental Procedure

There are few known parameters which govern tungsten trioxide (WO3) hydrothermal synthesis process which includes material source concentration, synthesis temperature, duration, pH value and additive level. Using design of experiments (DOE) approach, a systematic experimental procedure was conducted to investigate the effect of each parameter to the final morphology of the synthesized nanostructure. Despite the response obtained from this study is in qulitative form, the analysis still can be done to identify the combination of variables that most likely can produce either 1-D, 2-D or 3-D nanostructure. This insight is essential before further optimization of the process can be done in order to predict the behavior of the WO3 hydrothermal synthesis process.

Design of Experiments for Statistical Analysis of Geological Data

1953 ◽  
Vol 61 (6) ◽  
pp. 510-532 ◽  
Author(s):  
W. C. Krumbein ◽  
Robert L. Miller
Keyword(s):  
Statistical Analysis ◽  
Design Of Experiments ◽  
Geological Data

scholarly journals Polyol Silver Nanowire Synthesis and the Outlook for a Green Process

2020 ◽  
Vol 2020 ◽  
pp. 1-25 ◽  
Author(s):  
Shohreh Hemmati ◽  
Michael T. Harris ◽  
Dale P. Barkey
Keyword(s):  
Silver Nanowires ◽  
Synthesis Method ◽  
Polyol Process ◽  
Silver Nanowire ◽  
Polyol Synthesis ◽  
High Yield ◽  
Silver Nanostructures ◽  
Wearable Electronics ◽  
Aspect Ratios ◽  
Size And Morphology

Silver nanowires (AgNWs) have a broad range of applications including nanoelectronics, energy conversion, health care, solar cells, touch screens, sensors and biosensors, wearable electronics, and drug delivery systems. As their characteristics depend strongly on their size and morphology, it is essential to find the optimal and most cost-effective synthesis method with precise control over the size and morphology of the wires. Various methods for AgNW synthesis have been reported along with process optimization and novel techniques to increase the yield and aspect ratios of synthesized AgNWs. The most promising processes for synthesis of AgNWs are wet chemical techniques, in which the polyol process is low cost and simple and provides high yield compared to other chemical methods. Reaction mechanism is one of the most important factors in strategies to control the process. Our purpose here is to provide an overview on the main findings regarding synthesis, preparation, and characterization of AgNWs. Recent efforts in the polyol synthesis of AgNWs are summarized with respect to product morphology and size, reaction conditions, and characterization techniques. The effect of essential factors such as reagent concentration and preparation, temperature, and reaction atmosphere that control the size, morphology, and yield of synthesized AgNWs is reviewed. Moreover, a review on the novel modified polyol process and reactor design such as continuous millifluidic and flow reactors to increase the yield of synthesized AgNWs on large scales is provided. The most recent proposed growth mechanisms and kinetics behind the polyol process are addressed. Finally, comparatively few available studies in green and sustainable development of 1D silver nanostructures through the application of natural products with inherent growth termination, stabilization, and capping characteristics are reviewed to provide an avenue to natural synthesis pathways to AgNWs. Future directions in both chemical and green synthesis approaches of AgNWs are addressed.

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