Characterization of Zirconium Germanosilicide Formed by Solid State Reaction of ZR With Sil−xGex Alloys

1995 ◽  
Vol 402 ◽  
Author(s):  
Z. Wang ◽  
D. B. Aldrich ◽  
P. Goeller ◽  
R. J. Nemanich ◽  
D. E. Sayers
Keyword(s):  
Thin Films ◽  
Solid State ◽  
Sheet Resistance ◽  
Solid State Reaction ◽  
Solid Phase ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Final Phase ◽  
The Stability

AbstractWe have investigated the electrical and structural properties of zirconium germanosilicide (Zr-Si-Ge) films formed during the Zr-Sil−xGex solid state reaction. Thin films of C49 Zr(Si1−xGex)2 were formed from the solid phase reaction of Zr and Si1−xGex bilayer structures. It was observed that Zr reacts uniformly with the Sil−xGex alloy and that C49 Zr(Si1−x Gex)2 is the final phase of the Zr-Si1−xGex, solid phase reaction (such tht y = x) for all compositions examined (x = 0.20, 0.33, and 0.50). The sheet resistance of the Zr(Si1−xGex)2 thin films were higher than the sheet resistance measured for ZrSi2 films. The stability of Zr(Sil−x Gex)2 in contact with Si1−Gex was investigated and no germanium segregation was detected in the Zr(Si1−xGex)2/Si1−Gex structures.

Fabrication of Lithium Silicate Doped with Lithium Titanate by Solid-State Reaction and its XRD Study

2012 ◽  
Vol 624 ◽  
pp. 200-203
Author(s):  
Yu Tian Wang ◽  
You Dong Cao ◽  
Jin Hu ◽  
Wei Jun Zhang ◽  
Da Ping Wu ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Reaction ◽  
Solid Phase ◽  
Raw Materials ◽  
Xrd Analysis ◽  
Lithium Titanate ◽  
Lithium Silicate ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Scanning Calorimetry

Fabrication of lithium silicate powder containing lithium titanate by solid phase reaction method. LiFabrication of lithium silicate powder doped with lithium titanate by solid-state reaction. Take lithium carbonate, silicon dioxide and titania as raw materials and then these powders were mixed according to the different ratios and grinded in an agate mortar for 15 min. And then the mixture were dried at 80°C. Finally, the samples were sintered in vacuum tube furnace at 750, 800, 850 and 900°C for 2h. Thermogravimetric analysis, differential scanning calorimetry and XRD analysis were carried out systematically in this paper. The reaction process and mechanism at different temperatures and the effect of the different ratios and sintering temperature were discussed. Experimental results showed that lithium titanate component increased with increasing amount of titanium dioxide. While the mixture were sintered at 900°C for 2h, there would have lithium silicate and lithium titanate phase.

Study on the Synthesis and Characterization of PANi/Nano-CeO2 Composites

2007 ◽  
Vol 124-126 ◽  
pp. 287-290 ◽  
Author(s):  
Fei Liu ◽  
Yong Jun He ◽  
Jeung Soo Huh
Keyword(s):  
In Situ Polymerization ◽  
Solid Phase ◽  
Polymerization Reaction ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Vis Spectroscopy ◽  
Ft Ir ◽  
Average Size

The nano-CeO2 was synthesized by two-step solid-phase reaction. The image of TEM showed that nano-CeO2 with an average size of about 70 nm. The series of polyaniline/nano-CeO2 composites with different PANi: CeO2 ratios were prepared by in-situ polymerization in the presence of hydrochloric acid (HCl) as dopant by adding nano-CeO2 into the polymerization reaction mixture of aniline. The composites obtained were characterized by FT-IR and UV-vis spectroscopy analysis. The FT-IR spectra of nanocomposites indicate different blue-shifts, attributed to C–N stretching mode for benzenoid unit. The UV-vis spectra of nanocomposites display einstein-shifts compared with PANi at 620nm. The conductivity properties of the composites are also changed compare to the pure PANi. These results suggest that the interactions between the polymer matrix and nanoparticles take place in polyaniline/nano- CeO2 composites.

scholarly journals Структурные фазовые превращения при твердофазной реакции в тонких двухслойных пленках Al/Pt

2018 ◽  
Vol 60 (7) ◽  
pp. 1397
Author(s):  
Р.Р. Алтунин ◽  
Е.Т. Моисеенко ◽  
С.М. Жарков
Keyword(s):  
Thin Films ◽  
Electron Diffraction ◽  
Phase Transformations ◽  
Solid Phase ◽  
Structural Phase ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Formation Heat ◽  
Structural Phase Transformations

AbstractA sequence of phases forming during the solid-phase reaction in Al/Pt bilayer thin films has been investigated by in situ electron diffraction. It is shown that the amorphous PtAl_2 phase forms first during the solid-phase reaction initiated by heating. Upon further heating, PtAl_2, Pt_2Al_3, PtAl, and Pt_3Al crystalline phases sequentially form, which is qualitatively consistent with an effective formation heat model. The content of phases forming during the reaction has been quantitatively analyzed and the structural phase transformations have been examined.

Preparation of manganese silicide thin films by solid phase reaction

1997 ◽  
Vol 113-114 ◽  
pp. 53-56 ◽  
Author(s):  
Jinliang Wang ◽  
Masaaki Hirai ◽  
Masahiko Kusaka ◽  
Motohiro Iwami
Keyword(s):  
Thin Films ◽  
Solid Phase ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Manganese Silicide

Formation of Superconducting Y-Ba-Cu-O Thin Films by the Solid Phase Reaction between BaCo3/Cu/Y2O3Layers on Single Crystalline SrTiO3Substrate

1987 ◽  
Vol 26 (Part 2, No. 9) ◽  
pp. L1451-L1452 ◽  
Author(s):  
Yoshio Sorimachi ◽  
Akihito Kobayashi ◽  
Tsutomu Yamashita ◽  
Masasuke Takata ◽  
Shinnosuke Miyauchi ◽  
...  
Keyword(s):  
Thin Films ◽  
Solid Phase ◽  
Solid Phase Reaction ◽  
Phase Reaction ◽  
Single Crystalline

Characterization of Si/SiGe Heterostructures on Si Formed by Solid Phase Reaction

2002 ◽  
Vol 149 (3) ◽  
pp. G209 ◽  
Author(s):  
C. H. Huang ◽  
Albert Chin ◽  
W. J. Chen
Keyword(s):  
Solid Phase ◽  
Solid Phase Reaction ◽  
Phase Reaction
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