Structural and Optical Properties of Group III-Nitride Quantum Wells Studied by (S)Tem and CL

1997 ◽  
Vol 482 ◽  
Author(s):  
H. Lakner ◽  
Q. Liu ◽  
G. Brockt ◽  
A. Radefeld ◽  
F. Schulze-Kraasch ◽  
...  
Keyword(s):  
Optical Properties ◽  
High Resolution ◽  
Quantum Wells ◽  
Structural Defects ◽  
Chemical Compositions ◽  
Contrast Imaging ◽  
X Ray ◽  
Group Iii ◽  
Scanning Transmission ◽  
Convergent Beam

AbstractWurtzite InGaN/GaN and AlGaN/GaN heterostructures grown on sapphire by metal organic vapor phase epitaxy were studied using scanning transmission electron microscopy (STEM), cathodoluminescence (CL) combined with secondary electron (SE) imaging, high resolution x-ray diffractometry (HRXRD), and atomic force microscopy (AFM).SE imaging and AFM were used to study the surface morphology. The results indicate the presence of the following structural defects on the surface of InGaN/GaN heterostructures: hexagonal mesa-like structures, hexagonal pyramids and micropipes, while the surface of the AlGaN/GaN heterostructures are mirror-like smooth. The local optical properties of defects and defect free regions were studied using spatially resolved CL at low temperature. In addition, the dependence of the optical properties of both sorts of heterostructures on the quantum well width or chemical composition of ternary materials was investigated. The structural properties of the heterostructures were studied by STEM and HRXRD. Convergent beam electron diffraction (CBED) and corresponding simulations, convergent beam imaging (CBIM), and high resolution x-ray diffraction (HRXRD) were used to study the strained layers. Dislocations and interface properties were characterized using bright-field imaging, while the chemical compositions fluctuations were analyzed by Z-contrast imaging and energy dispersive x-ray microanalysis (EDX).

High-resolution scanning transmission soft X-ray microscopy for rapid probing of nanoparticle distribution and sufferance features in exposed cells

2015 ◽  
Vol 44 (3) ◽  
pp. 163-168 ◽  
Author(s):  
G. Kourousias ◽  
L. Pascolo ◽  
P. Marmorato ◽  
J. Ponti ◽  
G. Ceccone ◽  
...  
Keyword(s):  
High Resolution ◽  
X Ray ◽  
Nanoparticle Distribution ◽  
Scanning Transmission

scholarly journals Thermal History of Matrix Forsterite Grains from Murchison Based on High-resolution Tomography

2021 ◽  
Vol 922 (2) ◽  
pp. 256
Author(s):  
Giulia Perotti ◽  
Henning O. Sørensen ◽  
Henning Haack ◽  
Anja C. Andersen ◽  
Dario Ferreira Sanchez ◽  
...  
Keyword(s):  
High Resolution ◽  
Electron Density ◽  
Chemical Compositions ◽  
X Ray Diffraction ◽  
X Ray ◽  
Density Maps ◽  
Thermally Processed ◽  
The Matrix ◽  
History Of ◽  
Chondrule Formation

Abstract Protoplanetary disks are dust- and gas-rich structures surrounding protostars. Depending on the distance from the protostar, this dust is thermally processed to different degrees and accreted to form bodies of varying chemical compositions. The primordial accretion processes occurring in the early protoplanetary disk such as chondrule formation and metal segregation are not well understood. One way to constrain them is to study the morphology and composition of forsteritic grains from the matrix of carbonaceous chondrites. Here, we present high-resolution ptychographic X-ray nanotomography and multimodal chemical microtomography (X-ray diffraction and X-ray fluorescence) to reveal the early history of forsteritic grains extracted from the matrix of the Murchison CM2.5 chondrite. The 3D electron density maps revealed, at unprecedented resolution (64 nm), spherical inclusions containing Fe–Ni, very little silica-rich glass and void caps (i.e., volumes where the electron density is consistent with conditions close to vacuum) trapped in forsterite. The presence of the voids along with the overall composition, petrological textures, and shrinkage calculations is consistent with the grains experiencing one or more heating events with peak temperatures close to the melting point of forsterite (∼2100 K), and subsequently cooled and contracted, in agreement with chondrule-forming conditions.

Spatially resolved optical emission of cubic GaN/AlN multi-quantum well structures

2014 ◽  
Vol 1736 ◽  
Author(s):  
D.J. As ◽  
R. Kemper ◽  
C. Mietze ◽  
T. Wecker ◽  
J.K.N. Lindner ◽  
...  
Keyword(s):  
Optical Properties ◽  
Low Temperature ◽  
Film Thickness ◽  
Quantum Wells ◽  
Emission Intensity ◽  
Optical Emission ◽  
Quantum Well Structures ◽  
Spatially Resolved ◽  
Scanning Transmission ◽  
Cubic Gan

ABSTRACTIn this contribution we report on the optical properties of cubic AlN/GaN asymmetric multi quantum wells (MQW) structures on 3C-SiC/Si (001) substrates grown by radio-frequency plasma-assisted molecular beam epitaxy (MBE). Scanning transmission electron microscopy (STEM) and spatially resolved cathodoluminescence (CL) at room temperature and at low temperature are used to characterize the optical properties of the cubic AlN/GaN MQW structures. An increasing CL emission intensity with increasing film thickness due to the improved crystal quality was observed. This correlation can be directly connected to the reduction of the linewidth of x-ray rocking curves with increasing film thickness of the c-GaN films. Defects like stacking faults (SFs) on the {111} planes, which also can be considered as hexagonal inclusions in the cubic crystal matrix, lead to a decrease of the CL emission intensity. With low temperature CL line scans also monolayer fluctuations of the QWs have been detected and the observed transition energies agree well with solutions calculated using a one-dimensional (1D) Schrödinger-Poisson simulator.

Incoherent High-Resolution Z-Contrast Imaging of Silicon and Gallium Arsenide Using HAADF-STEM

1999 ◽  
Vol 589 ◽  
Author(s):  
Y Kotaka ◽  
T. Yamazaki ◽  
Y Kikuchi ◽  
K. Watanabe
Keyword(s):  
Scanning Transmission Electron Microscope ◽  
Dark Field ◽  
Contrast Imaging ◽  
High Spatial Resolution Image ◽  
Transmission Electron ◽  
Eigen Value ◽  
Scanning Transmission ◽  
Annular Dark Field ◽  
Convergent Beam ◽  
Z Contrast

AbstractThe high-angle annular dark-field (HAADF) technique in a dedicated scanning transmission electron microscope (STEM) provides strong compositional sensitivity dependent on atomic number (Z-contrast image). Furthermore, a high spatial resolution image is comparable to that of conventional coherent imaging (HRTEM). However, it is difficult to obtain a clear atomic structure HAADF image using a hybrid TEM/STEM. In this work, HAADF images were obtained with a JEOL JEM-2010F (with a thermal-Schottky field-emission) gun in probe-forming mode at 200 kV. We performed experiments using Si and GaAs in the [110] orientation. The electron-optical conditions were optimized. As a result, the dumbbell structure was observed in an image of [110] Si. Intensity profiles for GaAs along [001] showed differences for the two atomic sites. The experimental images were analyzed and compared with the calculated atomic positions and intensities obtained from Bethe's eigen-value method, which was modified to simulate HAADF-STEM based on Allen and Rossouw's method for convergent-beam electron diffraction (CBED). The experimental results showed a good agreement with the simulation results.

A Study of Grain Boundaries in High TC Superconducting Yba2Cu3O7-x Thin Films Using High Resolution Analytical Stem

1989 ◽  
Vol 169 ◽  
Author(s):  
D. H. Shin ◽  
J. Silcox ◽  
S. E. Russek ◽  
D. K. Lathrop ◽  
R. A. Buhrman
Keyword(s):  
Thin Films ◽  
High Resolution ◽  
Grain Boundaries ◽  
Scanning Transmission Electron Microscope ◽  
Atomic Resolution ◽  
High Tc ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Transmission ◽  
Edx Microanalysis

AbstractGrain boundaries in thin films of high Tc YBa2Cu3O7-x superconductors have been investigated with high resolution scanning transmission electron microscope (STEM) imaging and nanoprobe energy dispersive x-ray (EDX) analysis. Atomic resolution images indicate that the grain boundaries are mostly clean, i.e., free of a boundary layer of different phase or of segregation, and are often coherent. EDX microanalysis with a 10 Å spatial resolution also indicates no composition deviation at the grain boundaries.

scholarly journals Hot bubbles of planetary nebulae with hydrogen-deficient winds

2018 ◽  
Vol 620 ◽  
pp. A98 ◽  
Author(s):  
R. Heller ◽  
R. Jacob ◽  
D. Schönberner ◽  
M. Steffen
Keyword(s):  
Chemical Composition ◽  
High Resolution ◽  
Thermal Conduction ◽  
Thermal Structure ◽  
Neutral Hydrogen ◽  
Planetary Nebulae ◽  
Chemical Compositions ◽  
Heat Conducting ◽  
X Ray ◽  
Similar Solutions

Context. The first high-resolution X-ray spectroscopy of a planetary nebula, BD +30° 3639, opened the possibility to study plasma conditions and chemical compositions of X-ray emitting “hot” bubbles of planetary nebulae in much greater detail than before. Aims. We investigate (i) how diagnostic line ratios are influenced by the bubble’s thermal structure and chemical profile, (ii) whether the chemical composition inside the bubble of BD +30° 3639 is consistent with the hydrogen-poor composition of the stellar photosphere and wind, and (iii) whether hydrogen-rich nebular matter has already been added to the bubble of BD +30° 3639 by evaporation. Methods. We applied an analytical, one-dimensional (1D) model for wind-blown bubbles with temperature and density profiles based on self-similar solutions including thermal conduction. We also constructed heat-conduction bubbles with a chemical stratification. The X-ray emission was computed using the well-documented CHIANTI code. These bubble models are used to re-analyse the high-resolution X-ray spectrum from the hot bubble of BD +30° 3639. Results. We found that our 1D heat-conducting bubble models reproduce the observed line ratios much better than plasmas with single electron temperatures. In particular, all the temperature- and abundance-sensitive line ratios are consistent with BD +30° 3639 X-ray observations for (i) an intervening column density of neutral hydrogen, NH = 0.20-0.10+0.05 × 1022cm−2, (ii) a characteristic bubble X-ray temperature of TX = 1.8 ± 0.1 MK together with (iii) a very high neon mass fraction of about 0.05, virtually as high as that of oxygen. For lower values of NH, we cannot exclude the possibility that the hot bubble of BD +30° 3639 contains a small amount of “evaporated” (or mixed) hydrogen-rich nebular matter. Given the possible range of NH, the fraction of evaporated hydrogen-rich matter cannot exceed 3% of the bubble mass. Conclusions. The diffuse X-ray emission from BD +30° 3639 can be well explained by models of wind-blown bubbles with thermal conduction and a chemical composition equal to that of the hydrogen-poor and carbon-, oxygen-, and neon-rich stellar surface.

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