Surface Roughness Characterization of al Films by Spectroscopic Ellipsometry

1985 ◽  
Vol 54 ◽  
Author(s):  
J. R. Blanco ◽  
K. Vedam ◽  
P. J. McMarr ◽  
J. M. Bennett

ABSTRACTWell characterized rough surfaces of aluminum films have been studied by the nondestructive technique of Spectroscopie Ellipsometry (SE). The roughness of the aluminum specimens had been characterized earlier by Total Integrated Scattering and Stylus Profilometry techniques to obtain numerical estimates of ras roughness and autocovariance lengths. The present SE measurements on these specimens were carried out at a number of angles of incidence in the range 30–80° and at a number of discrete wavelengths in the spectral range 300–650nm. The SE results were then analyzed by the scalar theory of diffraction from random rough surfaces by treating the surface as a simple random rough surface. The results of such analyses of the SE measurements are compared with the results of the earlier characterization techniques.

Author(s):  
H. Fukanuma

Abstract Thermal spray layers are formed on rough surfaces; however, the flattening process on rough surfaces has not yet been clarified. A mathematical flattening model which takes into account the roughness of the substrate or previously coated layers is proposed in this paper. As a result of surface roughness, the flattening degree and the flattening time decrease with increasing surface roughness in this model. In addition, the characterization of surface roughness is introduced for the flattening model. Several calculated cases of the flattening model are shown.


1970 ◽  
Vol 185 (1) ◽  
pp. 625-633 ◽  
Author(s):  
J. A. Greenwood ◽  
J. H. Tripp

Most models of surface contact consider the surface roughness to be on one of the contacting surfaces only. The authors give a general theory of contact between two rough plane surfaces. They show that the important results of the previous models are unaffected: in particular, the load and the area of contact remain almost proportional, independently of the detailed mechanical and geometrical properties of the asperities. Further, a single-rough-surface model can always be found which will predict the same laws as a given two-rough-surface model, although the required model may be unrealistic. It does not seem possible to deduce the asperity shape or deformation mode from the load-compliance curve.


Author(s):  
M. Izadi ◽  
D. K. Aidun ◽  
P. Marzocca ◽  
H. Lee

The effect of surface roughness on the fouling behavior of calcium carbonate is experimentally investigated. The real operating conditions of a tubular heat exchanger are simulated by performing prolonged experiments with duration of 3 to 7 days. The solution used is a mixture of sodium bicarbonate and calcium chloride in de-ionized water with the concentration of 0.4 g/l of each. An on-line fouling evaluation system was developed such that the fouling resistance for a selected solution could be measured in real time. The experiments are repeated with the same procedure for 90/10 Cu/Ni tubes with different internal surface roughness. After the experiment the surface is analyzed by analytical microscopy to investigate the morphology of the deposit layer. Comparison of the experimental results of smooth and rough surfaces shows that a combination of aragonite and calcite polymorphs are formed on rough surface while only dendritic porous aragonite crystals are formed on smooth surface. Accordingly, the deposit layer formed on rough surface is denser and has a higher thermal resistance comparing to that formed on smooth surface. The fouling factor-time curves of smooth and rough surfaces obtained by the current experimental study agree with the results found by the analytical microscopy of the surface and show higher fouling resistances for rough surface. Experimental data is significantly important for the design, and formulating operating, and cleaning schedules of the equipment.


Author(s):  
Itzhak Green

Random rough surfaces appear in measurements as noisy signals varying spatially. Mathematically, there is no theoretical difference between such and time-varying signals. Hence, the extensive array of methods and analysis tools that have been developed for signal processing are available also for rough surfaces characterization. In both, the objective is to reduce the vast amount of data to just a few meaningful parameters that allow the application of other physical concepts. Particularly in contact mechanics, it is well known that the Greenwood–Williamson model requires three parameters for the calculation of the elastic deformation of rough surface asperities. The parameters are the roughness standard deviation, the equivalent asperity radius, and the asperity density. These parameters are byproducts of the spectral moments. The spectral moments have been employed for decades in many fields of engineering and science. For rough surfaces, for example, the work by McCool outlines a mathematical blueprint procedure on how to straightforwardly reduce the entire roughness data into the said three spectral moments. It is commonly claimed, however, that the said procedure inherently suffers from resolution problems, that is, a given surface shall have much different spectral moments depending on the sampling rate (or spacing). To study these issues, synthetic surfaces are generated herein using a harmonic waveform precisely as McCool had done. However, here the signals are contaminated by a white noise process with various magnitudes. A signal-to-noise ratio is defined and used to assess the quality of the signal, and the spectral moments are evaluated for various magnitudes of the noise. Since closed-from solutions are available for the spectral moments of the uncontaminated signal, the contaminated signals are evaluated vis-à-vis the exact anticipated values, and the errors are calculated. It is shown that using the common techniques (such as those outlined by McCool) can lead to enormous and unacceptable errors. Resolution is studied as well; it is shown to have an effect only in the presence of noise, but by itself it has no independent influence on the spectral moments. The venerable Savitzky–Golay smoothing filter is used on the noisy signals, showing some improvements, but the resulting spectral moments predicted still contain objectionable errors. A generalized exponential smoothing filter, G-EXP, is constructed, and it is shown to markedly moderate the errors and reduce them to acceptable levels, while effectively restoring the underlying surface physical characteristics. Moreover, the filtered signals do not suffer from resolution problems, where results, in fact, improve with higher (i.e., finer) resolutions. Fractal-generated signals are likewise discussed.


2018 ◽  
Vol 17 ◽  
pp. 1-9
Author(s):  
Luiz Carlos do Carmo Filho ◽  
Ana Paula Pinto Martins ◽  
Amália Machado Bielemann ◽  
Anna Paula da Rosa Possebon ◽  
Fernanda Faot

Aim: This study characterized the implant surfaces available on the Brazilian market in terms of topography, chemical composition, and roughness. Methods: The following brands were selected according to their surfaces: Kopp (Ko), Signo Vinces (Sv), Neodent (Ne), Osseotite (Os) NanoTite (Nt), SIN (Si), Titanium Fix (Tf), conventional Straumann (Str), Active SLA (SLA). The morphological analysis and the alloy impurities and implant surface contaminants were analyzed by SEM-EDS. Surface roughness parameters and 3-D reconstructions were obtained by laser microscopy (20x). Two distinct areas were evaluated: i) the cervical portion (no surface treatment), and ii) the middle third (treated surface). Results: The characterization of the implant surfaces by SEM showed morphological differences between the thread geometries and surface morphology at 800x and 2000x magnification. The EDS elemental analysis showed a predominance of titanium (Ti) for all implants. The SLA surface showed only peaks of Ti while other implants brands showed traces of impurities and contaminants including Al, C, PR, F, Mg, Na, Ni, O, P, and SR. The implant surface roughness in the cervical portion did not exceed Ra 0.5–1.0 μm, constituting a minimally rough surface and obtaining acceptable standards for this region. Only Nt, Str, and SLA presented Ra above 2 μm in the middle third area showing a rough surface favorable for osseointegration. Conclusion: This study concluded that there is no established standard for morphology, chemical composition and implant surface roughness that allows a safe comparison between the available dental implant surfaces. National implant brands generally contain more impurities and surface contaminants than their international counterparts and were consequently more sensitive to the surface treatment techniques.


Nanomaterials ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 2018
Author(s):  
Niloufar Pirouzfam ◽  
Kursat Sendur

Spectrally selective absorbers have received considerable interest due to their applications in thermophotovoltaic devices and as solar absorbers. Due to extreme operating conditions in these applications, such as high temperatures, thermo-mechanically stable and broadband spectrally selective absorbers are of interest. This paper demonstrates anisotropic random rough surfaces that provide broadband spectrally selective absorption for the thermo-mechanically stable Tungsten surfaces. Anisotropic random rough surface has different correlation lengths in the x- and y-directions, which means their topography parameters have directional dependence. In particular, we demonstrate that spectral absorptance of Tungsten random rough surfaces at visible (VIS) and near-infrared (NIR) spectral regions are sensitive to correlation length and RMS height variations. Our results indicate that by optimizing random rough surface parameters, absorption values exceeding 95% can be obtained. Moreover, our results indicate that anisotropic random rough surfaces broaden the bandwidth of the high absorption region. It is shown that in VIS and NIR regions, the absorption enhancements of up to 47% and 52% are achieved for the isotropic and anisotropic rough surfaces, respectively.


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