scholarly journals Effect of Extraction Methods on Characteristic of SodiumAlginate from Brown Seaweed Sargassum fluitans

2018 ◽  
Vol 20 (3) ◽  
pp. 478 ◽  
Author(s):  
Annisa Ajeng Maharani ◽  
Amir Husni ◽  
Nurfitri Ekantari

Alginate is a primary metabolite that is needed in food and non food industries. Alginate extraction<br />method of seaweed affect on viscosity and yield of the alginate. This study aimed to determine the effect of<br />extraction methods on characteristic and quality of sodium alginate Sargassum fluitans and the extraction<br />cost needed. This study used two different extraction methods which wereacid alginate method and calcium<br />alginate method. Quality parameters observed include yield, moisture content, ash content, viscosity,<br />pH, whiteness index, and functional group analysis, also extraction cost analysis. The results showed that<br />alginate extraction of S. fluitans by alginic acid method produced better sodium alginate quality than using<br />calcium alginate method, but the cost higher. Sodium alginate produced by alginic acid method had high<br />viscosity (127.17±11.50 cps) with yield 9.95±0.31%. The moisture and ash content of the product was low or<br />9.35±0.31% and 21.88±0.41%, respectively.<br /><br />

2018 ◽  
Vol 21 (3) ◽  
pp. 532
Author(s):  
Ivana M. Diharningrum ◽  
Amir Husni

Seaweed is one of the marine biological resources of Indonesia that has a high potential to produce alginate, however, the most appropiate method to extract the alginate of high quality is still unknown. This study was aimed to determine the effects of extraction methods on the quality of alginate from seaweed Sargassum hystrix and compared the extraction cost. Two extraction methods were used in this study including acidic and calcium method. The yield, moisture content, viscosity, pH, whiteness degree, functional group, ash content and extraction cost were evaluated. The viscosity and whiteness degree of sodium alginate from acidic method was 126.00±7.21 cPs and 75.27±0.58 cPs, respectively. Meanwhile the calcium method produced sodium alginate with viscosity 7.23±1.50 cPs and whiteness degree 68.95±0.18 cPs. The yield, moisture content, and ash content of alginate produced by acidic method were lower compare to that of produced by calcium method. Cost analysis showed the acidic method required higher cost. Nevertheless, these resultssuggest that acidic method produce alginate with better quality than the calcium method.


2020 ◽  
Vol 9 (1) ◽  
pp. 75-80
Author(s):  
Adam Sojuangon Pasaribu ◽  
Sri Sedjati ◽  
Rini Pramesti

ABSTRAK: Padina sp. merupakan spesies rumput laut cokelat (Phaeophyta) penghasil alginat, namun kualitas alginat yang dihasilkan tergolong rendah dibandingkan alginofit lainnya. Metode ekstraksi jalur kalsium diduga dapat meningkatkan kualitas alginat sehingga penelitian ini perlu dilakukan. Tujuan penelitian ini untuk mengkaji apakah ekstraksi jalur kalsium dapat meningkatkan mutu alginat yang dihasilkan dari rumput laut Padina. Ekstraksi dilakukan dengan metode jalur kalsium konvensional dan jalur kalsium MAE (Microvawe Assisted Extraction). Metode penelitian yang digunakan adalah eksperimental laboratoris dengan 1 perlakuan (kosentrasi CaCl2) dan 3 taraf konsentrasi yaitu 0,5 M 1,0 M dan 1,5 M. Parameter kualitas yang dianalisis meliputi rendemen, kadar air, Kadar abu, viskositas, pH dan FTIR. Hasil uji two way ANOVA menunjukan terdapat signifikansi rendemen dengan nilai 0,007. Metode jalur kalsium MAE dengan konsentrasi 1,0 M CaCl2 menghasilkan kualitas terbaik dengan nilai rendemen (26,83%), kadar air (10,67%), kadar abu (21,83%), viskositas (11,42 cPs)  dan pH (6,77). Hasil analisis FTIR menunjukan ke-2 metode ekstraksi menghasilkan natrium alginat dengan adanya sidik jari guluronat dan manuronat pada bilangan gelombang 930-890 cm-1 dan 870-820 cm-1. ABSTRACT: Padina sp. is a species of brown seaweed (Phaephyta) producing alginates, but the quality of alginates produced is relatively low compared to other alginophytes. The calcium pathway extraction method is thought to improve the quality of alginates thus the reason of the research. This research aims to examine whether the calcium pathway extraction improves the quality of alginates produced from Padina. Seaweed extraction was carried out using conventional calcium pathways and MAE (Microwave Assisted Extraction) calcium pathways. The research method used was laboratory experimental with 1 treatment (CaCl2 concentration) and 3 concentration levels : 0.5 M, 1.0 M, 1.5 M. Quality parameters analyzed includes yield, moisture content, ash contetnt, viscosity, pH and FTIR. The two way ANOVA test results showed that there was a significance of yield value of 0.007. The MAE calcium pathway method with a concentration of 1.0 M CaCl2 produces the best quality with a yield value (26.83%), water content (10.67%), ash content (21.83%), viscosity (11.42 cPs) and pH (6.77). FTIR analysis results show that the two extraction methods produces sodium alginate in the presence of guluronate and manuronic fingerprints at wave numbers 930-890 cm-1 and 870-820 cm-1.


2017 ◽  
Vol 20 (2) ◽  
pp. 351 ◽  
Author(s):  
Ellya Sinurat ◽  
Retni Marliani

Indonesia is the largest producer of seaweed in the world, one of the potential marine biological resources is the brown seaweed (Sargassum crassifolium) known as an alginate producer. Alginate extraction through demineralization stage, neutralization, extraction, filtration, precipitation and bleaching. Filtration stage is a very influential process on the quality of alginate produced. In this research, filtering using different tools screen vibrator and hydraulic filter press was conducted to characterize Na-alginate seaweed Sargassum crassifolium using both filter tools. Quality of sodium alginate (yield, viscosity, gel strength, syneresis, whiteness, moisture content, ash, and pH) was determined. The result showed that the viscosity, gel strength, syneresis, and whiteness of alginate obtained using filter press showed the best result. The yield of sodium alginate produced by filter press was 10.91±4.33%, with characteristics of viscosity 82.66±112.46 cP, gel strength 353.54±184.51 g/cm2, syneresis 2.99±0.55%, whiteness 60.53±9.09%, moisture content 13.31±0.77%, ash 26.69±0.82% and pH 6.05±0.57.  Based on a parameter of alginate (yield, moisture content, ash, and pH) showed that vibrator method produced alginate with better characteristics. The sodium alginate produced has average yield 19.22±5.68%, viscosity 57.5±21.79 cP, whiteness 29.7±4.45%, gel strength 327.63±55.15 g/cm2, syneresis 4.34±0.78%, moisture content 10.23±1.68%, ash 24.94±4.41% and pH 7.03± 2.60. Operationally the filter press was more effective and efficient in filtering to result from Na-alginate compared to the screen vibrator.


2019 ◽  
Vol 22 (1) ◽  
pp. 164
Author(s):  
Rizqi Wahyu Herdianto ◽  
Amir Husni

Seaweed is one of Indonesia’s marine biological resources which has potential to produce alginate which can be used for food and non-food industries. Several studies had been carried out in an effort to improve the quality of alginate extraction. This study aims to determine the effect of extraction temperature on the quality of sodium alginate from Sargassum muticum. This study used variations in extraction temperatures, namely 30; 40; 50; 60 and 70°C. The parameters observed included yield (%), moisture content (%), ash content (%), pH, whiteness degree and functional groups of alginate. The results showed that the difference in extraction<br />temperature of sodium alginate had a significant effect on yield and viscosity, but did not significantly affect water content, ash content, and whiteness degree. Extraction temperature of 60°C produced the best yield<br />and viscosity, 14.90±2.26% and 236.10±36.61 cPs, respectively.


Author(s):  
S. Inoue ◽  
Y. Tanaka ◽  
S.C. Skoryna

Sodium alginate, a brown seaweed polysaccharide, is capable of preventing intestinal absorption of radioactive strontium and its radiotoxicological importance is now well established. Alginic acid was found to be composed of 1,4-linked poly-L-guluronic acid and poly-D-mannuronic acid chains with some glycosidic linkages between these uronic acids.Polyguluronic and polymannuronic acid were prepared by acid hydrolysis of alginic acid from Laminaria hyperborea followed by fractionation of the partially degraded sodium alginate at pH 2.8. These components consist almost exclusively of a single uronic acid (polyguluronic acid: man/gul = 0.27; polymannuronic acid: man/gul = 10.7). Sodium polyguluronate inhibits absorption of radiostrontium more effectively than sodium polymannuronate.


Discover Food ◽  
2022 ◽  
Vol 2 (1) ◽  
Author(s):  
G. D. T. M. Jayasinghe ◽  
B. K. K. K. Jinadasa ◽  
N. A. G. Sadaruwan

AbstractAlginates are natural polysaccharides that are extracted from brown seaweed varieties and it is widely used for their rheological properties. The main step in the extraction protocol of sodium alginate is alkaline extraction. Sodium alginate was produced by dipping the seaweed in 1% formaldehyde and 2.5% of sodium carbonate solution and properties were studied following the standard methods. The amount of sodium alginate yield was 31.7% in Sargassum wightii. The moisture content and the ash content were recorded at 16.82% and 5.20%, respectively. The viscosity and the gel strength were noted as 40 vcP, 4.54 × 10–2 kN with 0.1 M CaCl2 and 6.86 × 10–2 kN with 0.2 M CaCl2 respectively. This study of the extraction method and its properties reveal that Sargassum wightii brown seaweed species have a high affinity to extract the alginate.


2017 ◽  
Vol 20 (2) ◽  
pp. 36 ◽  
Author(s):  
Rani Laksanawati ◽  
U. Ustadi ◽  
Amir Husni

Indonesia has a lot of high potential seaweed as a source of an alginate, but the extraction method had been used was not suitable. The aim of this research is to develop alginate extraction method from Turbinaria ornata seaweed with calcium method and compare the cost of extraction with an acid method as a control. In this research, various concentration of calcium chloride (CaCl2) was used in the separation of alginate from the extracted filtrate. The concentration of CaCl2 used varies from 0.50; 0.75; 1.00; 1.25; and 1.50 M. For comparison, alginate extraction with acid (control) method was used. Alginate quality parameters observed included alginate yield, product color degree, and gel viscosity. The results showed that the yield of alginate produced by calcium method was 36.89; 44.00; 56.00; 52.89 and 53.11% and for control 22.45%. From the degree of product color, CaCl2 concentration did not significantly affect the color of alginate but was darker when compared to the product extracted by the acid method. The viscosity of alginate produced by calcium method was 27,69; 26,57; 24.50; 22.41 and 19.92 cP while for control 32.88 cP. The extraction of Na-alginate with calcium method can decrease the need for Na-alginate extraction cost by 85% from the amount of  Na-alginate extraction cost requirement by the acid method.


2018 ◽  
Vol 3 (1) ◽  
pp. 7
Author(s):  
Yuska Novi Yanti ◽  
Hepiyansori Hepiyansori

<p>Indonesia daerah tropis yang baik untuk perkembangan jenis nyamuk sehingga membahayakan kesehatan. Indonesia kaya tanaman tradisional untuk  pengobatan. Salah Satunya Mahoni (Swietenia mahogany (L.)Jacq) pada bagian biji yang digunakan masyarakat untuk pengobatan malaria, diabetes, dan darah tinggi. Kandungan pada biji Mahoni yaitu saponin dan flavanoid dapat digunakan sebagai sediaan obat anti nyamuk. Sampel penelitian ini adalah biji mahoni yang diambil dari Taman Remaja Kota Bengkulu lalu di maserasi menggunakan pelarut metanol p.a dan etanol 96% selanjutnya ekstrak dibuat menjadi 3 konsentrasi ekstrak yaitu 1%, 3% dan 5%. Kemudian dibuat keping anti nyamuk dan di buat obat anti nyamuknya, dilanjutkan dengan pengujian evalusi ekstrak meliputi uji organoleptis, uji kadar abu dan uji rendemen kemudian pengujian evalusi sediaan yang meliputi uji organoleptis, uji keping anti nyamuk dan uji ketahanan sediaan. Hasil penelitian didapatkan, ekstrak metanol biji mahoni dapat mempengaruhi sifat fisik sediaan keping nyamuk, Ekstrak biji mahoni berwarna coklat sampai kemerahan, memiliki bau khas (aroma kacang tanah), konsistensi cukup padat sedikit berminyak dan berasa pahit. Uji parameter standar menghasilkan data untuk rendemen sebesar 0,8235% untuk metanol dan 0,6747% untuk etanol, kadar abu untuk metanol 1,249% dan untuk etanol 1,022%. sehingga ekstrak metanol biji mahoni dapat dibuat menjadi sediaan keping anti nyamuk.</p><p><em>Indonesia tropical region places the development  some mosquitoes that endanger health. Indonesia traditional crops can used for treatment. Mahoni (Swietenia mahogany (L.)Jacq)  a plant which usually treatment. Especially   part of the seed malaria drugs, diabetes and high blood pseasure.That in the seeds of mahoni there is saponin and flavonid can be used as a mosquito repellent. The sample this research is seeds mahoni taken from the Remaja Bengkulu Pares. Processed  maserasi with methanol solvent p.a and ethanol 96% next methanol made to 3 concentration an extract that 1%, 3% and 5%. Created pieces of mosquito repellent and mosquito repellent that followed terts the evaluation of extract. covers organoleptis, ash content and rendemen and testing performed and evaluation dosage, includes organoleptis, pieces  mosquito repellent and dosage resutance.Result experiment is extract methanol seeds mahoni 82,35 gram and extract ethanol seeds mahoni 67,47 gram. Extract colored from dark brown to reddish, have peanut like aroma, adequate compact consistency, bitter taste and not sticky in hand. The result of standard quality parameters rendemen extract methanol 0,8235% and rendemen extract ethanol 0,6747%, ash content extract methanol 1,247% and ash content extract ethanol 1,022%. so that the extract of methanol mahogany seeds can  made into anti-mosquito </em></p>


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