scholarly journals IMPROVEMENT OF METROLOGICAL CHARACTERISTICS OF AES-ICP DETERMINATION OF IMPURITY ELEMENTS IN ZIRCONIUM CERAMIC MATERIALS FOR MEDICAL PURPOSES

2019 ◽  
Vol 3 ◽  
pp. 43-56
Author(s):  
V.A. Volchenkova ◽  
◽  
E.K. Kazenas ◽  
N.A. Andreeva ◽  
A.A. Fomina ◽  
...  
2020 ◽  
Vol 1688 ◽  
pp. 012011
Author(s):  
V A Volchenkova ◽  
E K Kazenas ◽  
N A Andreeva ◽  
A A Fomina ◽  
O A Ovchinnikova ◽  
...  

2020 ◽  
Vol 65 (7-8) ◽  
pp. 37-41
Author(s):  
E. N. Semenova ◽  
S. I. Kuleshova ◽  
E. I. Sakanyan

A method for the quantitative determination of streptomycin sulfate in medicines by the turbidimetric method has been developedand validated. Based on the results of the experiments, it was found that the metrological characteristics of such validation parameters of the method as linearity, precision, and correctness do not exceed the validation criteria. Linearity was noted in the range of streptomycin concentrations from 3.75 to 8.43 μg/ml. The results of validation tests of the method for the quantitative determination of streptomycin indicate the prospects and feasibility of introducing the turbidimetric method into the domestic system for standardization and quality assessment of aminoglycoside antibiotics.


1986 ◽  
Vol 72 ◽  
Author(s):  
Theresa L. Baker ◽  
Stephen W. Freiman

AbstractThis study involved the determination of the effects of composition and microstructure on the fracture toughness and susceptibility to environmentally enhanced crack growth of several ceramic materials used in multilayer capacitors. Indentation-fracture procedures were used to measure KIC as well as to assess the possible effects of internal stresses on the fracture behavior of these materials and to correlate dielectric aging phenomena with strength. The environmentally enhanced crack growth behavior of these materials was determined by conducting dynamic fatigue tests in water.


1978 ◽  
Vol 21 (2) ◽  
pp. 158-163
Author(s):  
I. V. Abuladze ◽  
A. I. Belyaevskii ◽  
A. A. Dzhevdet

Author(s):  
Petr S. Gulyaev ◽  
Alexander N. Teplykh ◽  
Andrey Y. Dyachenko

Most of the failures of turbine flow converters (TFC) used in the Russian system of main oil pipelines and oil product pipelines are caused by abrupt changes in the viscosity of the transported medium. In studies related to determination of the influence of the rheological properties of the pumped oil on the metrological characteristics of TFC that have a calibration curve in the form of a piecewise approximation without taking into account the correlation of TFC rotor speed with the viscosity of the pumped liquid in the flow rate subrange, the instability of the metrological characteristics in the operating range is observed. Taking into account the tendency to increase the volume of production and pumping of high-viscosity oils it can be assumed that the irregularity of the metrological characteristics of TFC, expressed in the change in the conversion factor will remain, which will negatively affect the reliability of accounting operations using oil quality control system (OQCS). Accordingly there is a need to maintain the error of TFC within the set limits in the subranges and throughout the entire range of flow rates. According to the results of the study performed by the authors it was confirmed that for the TFC of MVTM type the use of the calibration curve in the form of a piecewise-parabolic approximation with the dependence of the conversion factor on the ratio of TFC pulse frequency to the oil viscosity makes it possible to minimize the effect of changes in the parameters of the pumped medium on the measurement accuracy and as a consequence to stabilize the metrological characteristics of TFC in the recalibration interval, eliminate the costs of performing out-of-turn verifications, increase the accuracy and metrological reliability of the OQCS. Большинство отказов турбинных преобразователей расхода (ТПР), используемых в российской системе магистральных нефтепроводов и нефтепродуктопроводов, обусловлено резкими изменениями вязкости транспортируемой среды. В исследованиях по определению влияния реологических свойств перекачиваемой нефти на метрологические характеристики ТПР, имеющих градуировочную характеристику в виде кусочно-линейной аппроксимации без учета корреляции частоты вращения ротора ТПР с вязкостью перекачиваемой жидкости в поддиапазоне расхода, отмечается нестабильность метрологических характеристик в рабочем диапазоне. Учитывая тенденцию увеличения объема добычи и перекачки высоковязких нефтей, можно предположить, что непостоянность метрологических характеристик ТПР, выражаемая в изменении коэффициента преобразования, сохранится, что негативно скажется на достоверности учетных операций с применением систем измерений количества и показателей качества нефти (СИКН). Соответственно, возникает потребность в поддержании погрешности ТПР в установленных пределах в поддиапазонах и во всем диапазоне расходов. По результатам проведенного авторами исследования подтверждено, что для ТПР типа MVTM использование градуировочной характеристики в виде кусочно-параболической аппроксимации с зависимостью коэффициента преобразования от отношения частоты импульсов ТПР к вязкости нефти позволяет минимизировать влияние изменений параметров перекачиваемой среды на точность измерений и, как следствие, стабилизировать метрологические характеристики ТПР в межповерочном интервале, исключить затраты на выполнение внеочередных поверок, повысить точность и метрологическую надежность СИКН.


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