scholarly journals Nanoindentation-Induced Pile-Up in the Residual Impression of Crystalline Cu with Different Grain Size

2017 ◽  
Author(s):  
Jiangjiang Hu ◽  
Weiming Sun ◽  
Taihua Zhang ◽  
Yusheng Zhang
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Room Temperature ◽  
Indentation Depth ◽  
Dislocation Motion ◽  
Coarse Grained ◽  
Ultrafine Grained ◽  
Pile Up ◽  
Different Grain Size ◽  
Multiple Slips

At room temperature, the indentation morphologies of crystalline copper with different grain size including nanocrystalline (NC), ultrafine-grained (UFG) and coarse-grained (CG) copper were studied by nanoindentation at the strain rate of 0.04/s without holding time at indentation depth of 2000 nm. As the grain size increasing, the height of the pile-up around the residual indentation increases and then has a slightly decrease in the CG Cu, While the area of the pile-up increases constantly. Our analysis has revealed that the dislocation motion and GB activities in the NC Cu, some cross- and multiple-slips dislocation insides the larger grain in the UFG Cu, and forest dislocations from the intragranular Frank-Read sources in the CG Cu, would directly induce these distinct pile-up effect.

Strain Rate Sensitivity of Ultrafine Grained FCC- and BCC-Type Metals

2006 ◽  
Vol 503-504 ◽  
pp. 781-786 ◽  
Author(s):  
Johannes May ◽  
Heinz Werner Höppel ◽  
Matthias Göken
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Room Temperature ◽  
Rate Sensitivity ◽  
Tensile Tests ◽  
Testing Temperature ◽  
Ultrafine Grain ◽  
Ultrafine Grain Size ◽  
Ultrafine Grained

The dependence of the strain rate sensitivity (SRS) of α-Fe and Al 99.5, as typical representatives of fcc- and bcc-type metals, on the testing temperature and with respect to the microstructure is investigated. In particular, the differences between conventional grain size (CG) and ultrafine grain size (UFG) are pointed out. UFG Al 99.5 generally shows an elevated SRS compared to CG Al 99.5. In case of α-Fe the SRS of the UFG state is decreased at room temperature, but increased at 200 °C, compared to the CG state. It is shown that the SRS also influences the ductility of UFG-metals in tensile tests.

Deformation Mechanisms in Ultrafine-Grained Zn at Different Strain Rates and Temperatures

2013 ◽  
Vol 592-593 ◽  
pp. 313-316
Author(s):  
Péter Jenei ◽  
Guy Dirras ◽  
Jenő Gubicza ◽  
Hervé Couque
Keyword(s):  
Grain Size ◽  
Room Temperature ◽  
Strain Rate Range ◽  
Deformation Mechanisms ◽  
Coarse Grained ◽  
Strain Rates ◽  
Initial State ◽  
Rate Range ◽  
Hexagonal Close Packed ◽  
Ultrafine Grained

The deformation mechanisms in ultrafine-grained hexagonal close packed Zn were investigated at different strain rates and temperatures. The influence of grain size on the deformation mechanisms was revealed by comparing the results obtained on ultrafine-grained and coarse-grained Zn. It was found that for coarse-grained Zn at room temperature and strain rates lower than 10-2s-1twinning contributed to plasticity besides dislocation activity. For strain rates higher than 103s-1the plasticity in coarse-grained Zn was controlled by dislocation drag. In ultrafine-grained Zn the relatively large dislocation density (~1014m-2) and the small grain size (~250 nm) limit the dislocation velocity yielding the lack of dislocation drag effects up to 104s-1. For ultrafine-grained Zn, twinning was not observed in the entire strain rate range due to its very small grain size. During room temperature compression at strain rates higher than 0.35 s-1and in high temperature creep deformation of ultrafine-grained Zn besides prismatic and pyramidal <c+a> dislocations observed in the initial state, <a>-type basal and pyramidal dislocations as well as other <c+a>-type pyramidal dislocations were formed.

The effect of strain rates on tensile deformation of ultrafine-grained copper

2017 ◽  
Vol 31 (16-19) ◽  
pp. 1744014
Author(s):  
M. Li ◽  
Q. W. Jiang
Keyword(s):  
Strain Rate ◽  
Deformation Behavior ◽  
Room Temperature ◽  
Tensile Deformation ◽  
Strain Rates ◽  
Roll Bonding ◽  
Fracture Elongation ◽  
Tensile Deformation Behavior ◽  
Ultrafine Grained ◽  
Flow Stress Level

Tensile deformation behavior of ultrafine-grained (UFG) copper processed by accumulative roll-bonding (ARB) was studied under different strain rates at room temperature. It was found that the UFG copper under the strain rate of 10[Formula: see text] s[Formula: see text] led to a higher strength (higher flow stress level), flow stability (higher stress hardening rate) and fracture elongation. In the fracture surface of the sample appeared a large number of cleavage steps under the strain rate of 10[Formula: see text] s[Formula: see text], indicating a typical brittle fracture mode. When the strain rate is 10[Formula: see text] or 10[Formula: see text] s[Formula: see text], a great amount of dimples with few cleavage steps were observed, showing a transition from brittle to plastic deformation with increasing strain rate.

scholarly journals New Approach In The Properties Evaluation Of Ultrafine-Grained OFHC Copper

2015 ◽  
Vol 60 (2) ◽  
pp. 605-614 ◽  
Author(s):  
T. Kvačkaj ◽  
A. Kováčová ◽  
J. Bidulská ◽  
R. Bidulský ◽  
R. Kočičko
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Tensile Tests ◽  
Coarse Grained ◽  
Wear Behaviour ◽  
Ofhc Copper ◽  
Strain Rates ◽  
Ultrafine Grained ◽  
Reduction Of Area ◽  
Pin On Disk

AbstractIn this study, static, dynamic and tribological properties of ultrafine-grained (UFG) oxygen-free high thermal conductivity (OFHC) copper were investigated in detail. In order to evaluate the mechanical behaviour at different strain rates, OFHC copper was tested using two devices resulting in static and dynamic regimes. Moreover, the copper was subjected to two different processing methods, which made possible to study the influence of structure. The study of strain rate and microstructure was focused on progress in the mechanical properties after tensile tests. It was found that the strain rate is an important parameter affecting mechanical properties of copper. The ultimate tensile strength increased with the strain rate increasing and this effect was more visible at high strain rates$({\dot \varepsilon} \sim 10^2 \;{\rm{s}}^{ - 1} )$. However, the reduction of area had a different progress depending on microstructural features of materials (coarse-grained vs. ultrafine-grained structure) and introduced strain rate conditions during plastic deformation (static vs. dynamic regime). The wear behaviour of copper was investigated through pin-on-disk tests. The wear tracks examination showed that the delamination and the mild oxidational wears are the main wear mechanisms.

Local Investigations of the Mechanical Properties of Ultrafine Grained Metals by Nanoindentations

2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Room Temperature ◽  
Rate Sensitivity ◽  
Strain Rates ◽  
Fcc Metals ◽  
Angular Pressing ◽  
Ultrafine Grained ◽  
Indentation Strain

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.

scholarly journals Aging Behaviour of Al-Mg-Si Alloys Subjected to Severe Plastic Deformation by ECAP and Cold Asymmetric Rolling

2011 ◽  
Vol 2011 ◽  
pp. 1-8 ◽  
Author(s):  
S. Farè ◽  
N. Lecis ◽  
M. Vedani
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Isothermal Aging ◽  
Room Temperature ◽  
Coarse Grained ◽  
Peak Shape ◽  
Asymmetric Rolling ◽  
Ultrafine Grained ◽  
Aging Kinetics ◽  
Reduced Intensity

A study was carried out on aging behaviour of a 6082 alloy processed by two different severe plastic deformation techniques: ECAP and asymmetric rolling. Both techniques were able to generate an ultrafine-grained structure in samples processed at room temperature. It was stated that severe straining promotes marked changes in the postdeformation aging kinetics. The peaks of β′′/β′ transition phases were anticipated and of progressively reduced intensity over the coarse grained alloy. A further peak accounting for onset of recrystallization also appeared in the most severely deformed samples. Full consistency in peak shape and position was found when comparing materials processed by ECAP and asymmetric rolling. Isothermal aging treatments performed at 180°C revealed that in the severely deformed samples, aging became so fast that the hardness curves continuously decreased due to overwhelming effects of structure restoration. On the contrary, aging at 130°C offers good opportunities for fully exploiting the precipitate hardening effects in the ultrafine-grained alloy.

scholarly journals Strain Rate Contribution due to Dynamic Recovery of Ultrafine-Grained Cu–Zr as Evidenced by Load Reductions during Quasi-Stationary Deformation at 0.5 Tm

Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1150 ◽  
Author(s):  
Wolfgang Blum ◽  
Jiři Dvořák ◽  
Petr Král ◽  
Philip Eisenlohr ◽  
Vaclav Sklenička
Keyword(s):  
Strain Rate ◽  
Dynamic Recovery ◽  
Tensile Deformation ◽  
Coarse Grained ◽  
Internal Stresses ◽  
Back Flow ◽  
Stationary Rate ◽  
Ultrafine Grained ◽  
High Fraction ◽  
And Storage

During quasi-stationary tensile deformation of ultrafine-grained Cu-0.2 mass%Zr at 673 K and a deformation rate of about e - 4 / s load changes were performed. Reductions of relative load by more than about 25% initiate anelastic back flow. Subsequently, the creep rate turns positive again and goes through a relative maximum. This is interpreted by a strain rate component ϵ ˙ - associated with dynamic recovery of dislocations. Back extrapolation indicates that ϵ ˙ - contributes the same fraction of ( 20 ± 10 ) % to the quasi-stationary strain rate that has been reported for coarse-grained materials with high fraction of low-angle boundaries; this suggests that dynamic recovery of dislocations is generally mediated by boundaries. The influence of anelastic back flow on ϵ ˙ - is discussed. Comparison of ϵ ˙ - to the quasi-stationary rate points to enhancement of dynamic recovery by internal stresses. Subtraction of ϵ ˙ - from the total rate yields the rate component ϵ ˙ + related with generation and storage of dislocations; its activation volume is in the order expected from the classical theory of thermal glide.

Superplasticity and Microstructure Evolution of Electrodeposited Nanocrystalline Nickel

2007 ◽  
Vol 551-552 ◽  
pp. 539-544 ◽  
Author(s):  
S. Ding ◽  
Kai Feng Zhang ◽  
Guo Feng Wang
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Room Temperature ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Intergranular Cracking ◽  
Mean Grain Size ◽  
Electrodeposited Nickel ◽  
Superplastic Properties

Nanocrystalline pure nickel (nc-Ni) was produced by pulse electrodeposition and its superplastic properties at and above room temperature were investigated. The electrodeposited nickel has a narrow grain size distribution with a mean grain size of 70nm. Uniaxial tensile tests at room temperature showed that nc-Ni has a limited plasticity but high tensile strength up to 1GPa at strain rates between 10-5 and 10-2s-1. However, when the temperature increased to 420 and higher, test specimens showed uniform deformation and the elongation value was larger than 200%. A maximum elongation value of 380% was observed at 450°C and a strain rate of 1.67x10-3s-1, SEM and TEM were used to examine the microstructures of the as-deposited and deformed specimens. The results indicated that fracture was caused by intergranular cracking and most cracks were originated from the brittle oxide formed during the tensile test. Grain coarsening was observed in the deformed specimen. The role of temperature and strain on grain growth was evaluated by comparing the microstructure of deformed samples with that of samples statically annealed. Deformation mechanism was discussed based upon the deformed microstructure and strain rate jump tests.

Strain Rate Sensitivity of Ultrafine-Grained CP-Ti Processed by ECAP at Room Temperature

2010 ◽  
Vol 667-669 ◽  
pp. 707-712 ◽  
Author(s):  
Xiao Yan Liu ◽  
Xi Cheng Zhao ◽  
Xi Rong Yang
Keyword(s):  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Room Temperature ◽  
Rate Sensitivity ◽  
Strain Rate Range ◽  
Compression Tests ◽  
Ultrafine Grained ◽  
Die Set ◽  
Increasing Temperature ◽  
Cp Ti

Ultrafine-grained (UFG) commercially pure (CP) Ti with a grain size of about 200 nm was produced by ECAP up to 8 passes using route BC at room temperature. For ECAP processing a proper die set was designed and constructed with an internal channel angle Φ of 120° and an outer arc of curvature Ψ of 20°. Strain rate sensitivity of UFG CP-Ti and CG CP-Ti were investigated by compression tests in the temperature range of 298~673K and strain rate range of 10-4~100s-1 using Gleeble simulator machine. Evolution of the microstructure during compression testing was observed using optical microscopy (OM) and transmission electron microscopy (TEM). Strain rate sensitivity value m of the UFG CP-Ti has been measured and is found to increase with increasing temperature and decreasing strain rate, and is enhanced compared to that of CG CP-Ti. Result of the deformation activation energy determination of UFG CP-Ti indicates that the deformation mechanism in UFG CP-Ti is correlated to the grain boundaries.

Cavitation Behavior of Ultra-Fine Grained Ti-6Al-4V Alloy Produced by Equal-Channel Angular Pressing

2007 ◽  
Vol 551-552 ◽  
pp. 621-626
Author(s):  
Young Gun Ko ◽  
Yong Nam Kwon ◽  
Jung Hwan Lee ◽  
Dong Hyuk Shin ◽  
Chong Soo Lee
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Equal Channel Angular Pressing ◽  
Cavity Growth ◽  
Rate Sensitivity ◽  
Theoretical Models ◽  
Coarse Grained ◽  
Fine Grained ◽  
Angular Pressing ◽  
Cavitation Behavior

Cavitation behavior during superplastic flow of ultra-fine grained (UFG) Ti-6Al-4V alloy was established with the variation of grain size and misorientation. After imposing an effective strainup to 8 via equal-channel angular pressing (ECAP) at 873 K, alpha-phase grains were markedly refined from 11 μm to ≈ 0.3 μm, and misorientation angle was increased. Uniaxial-tension tests were conducted for initial coarse grained (CG) and two UFG alloys (ε = 4 and 8) at temperature of 973 K and strain rate of 10-4 s-1. Quantitative measurements of cavitation evidenced that both the average size and the area fraction of cavities significantly decreased with decreasing grain size and/or increasing misorientation. It was also found that, when compared to CG alloy, cavitation as well as diffused necking was less prevalent in UFG alloys, which was presumably due to the higher value of strain-rate sensitivity. Based on the several theoretical models describing the cavity growth behavior, the cavity growth mechanism in UFG alloys was suggested.

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