Superplasticity and Microstructure Evolution of Electrodeposited Nanocrystalline Nickel

2007 ◽  
Vol 551-552 ◽  
pp. 539-544 ◽  
Author(s):  
S. Ding ◽  
Kai Feng Zhang ◽  
Guo Feng Wang
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Room Temperature ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Intergranular Cracking ◽  
Mean Grain Size ◽  
Electrodeposited Nickel ◽  
Superplastic Properties

Nanocrystalline pure nickel (nc-Ni) was produced by pulse electrodeposition and its superplastic properties at and above room temperature were investigated. The electrodeposited nickel has a narrow grain size distribution with a mean grain size of 70nm. Uniaxial tensile tests at room temperature showed that nc-Ni has a limited plasticity but high tensile strength up to 1GPa at strain rates between 10-5 and 10-2s-1. However, when the temperature increased to 420 and higher, test specimens showed uniform deformation and the elongation value was larger than 200%. A maximum elongation value of 380% was observed at 450°C and a strain rate of 1.67x10-3s-1, SEM and TEM were used to examine the microstructures of the as-deposited and deformed specimens. The results indicated that fracture was caused by intergranular cracking and most cracks were originated from the brittle oxide formed during the tensile test. Grain coarsening was observed in the deformed specimen. The role of temperature and strain on grain growth was evaluated by comparing the microstructure of deformed samples with that of samples statically annealed. Deformation mechanism was discussed based upon the deformed microstructure and strain rate jump tests.

Effect of Fast Annealing on Microstructure and Mechanical Properties of Non-Oriented Al-Si Low C Electrical Steels

2007 ◽  
Vol 560 ◽  
pp. 29-34 ◽  
Author(s):  
Emmanuel Gutiérrez C. ◽  
Armando Salinas-Rodríguez ◽  
Enrique Nava-Vázquez
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Room Temperature ◽  
Tensile Tests ◽  
Rate Of Change ◽  
Uniaxial Tensile ◽  
Electrical Steels ◽  
Offset Yield Strength ◽  
Microstructure And Mechanical Properties ◽  
Increasing Temperature

The effects of heating rate and annealing temperature on the microstructure and mechanical properties of cold rolled Al-Si, low C non-oriented electrical steels are investigated using SEM metallography and uniaxial tensile tests. The experimental results show that short term annealing at temperatures up to 850 °C result in microstructures consisting of recrystallized ferrite grains with sizes similar to those observed in industrial semi-processed strips subjected to long term batch annealing treatments. Within the temperature range investigated, the grain size increases and the 0.2% offset yield strength decreases with increasing temperature. It was observed that the rate of change of grain size with increasing temperature increases when annealing is performed at temperatures greater than Ac1 (~870 °C). This effect is attributed to Fe3C dissolution and rapid C segregation to austenite for annealing temperatures within the ferrite+austenite phase field. This leads to faster ferrite growth and formation of pearlite when the steel is finally cooled to room temperature. The presence of pearlite at room temperature decreases the ductility of samples annealed at T > Ac1.

Strain Rate Sensitivity of Ultrafine Grained FCC- and BCC-Type Metals

2006 ◽  
Vol 503-504 ◽  
pp. 781-786 ◽  
Author(s):  
Johannes May ◽  
Heinz Werner Höppel ◽  
Matthias Göken
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Room Temperature ◽  
Rate Sensitivity ◽  
Tensile Tests ◽  
Testing Temperature ◽  
Ultrafine Grain ◽  
Ultrafine Grain Size ◽  
Ultrafine Grained

The dependence of the strain rate sensitivity (SRS) of α-Fe and Al 99.5, as typical representatives of fcc- and bcc-type metals, on the testing temperature and with respect to the microstructure is investigated. In particular, the differences between conventional grain size (CG) and ultrafine grain size (UFG) are pointed out. UFG Al 99.5 generally shows an elevated SRS compared to CG Al 99.5. In case of α-Fe the SRS of the UFG state is decreased at room temperature, but increased at 200 °C, compared to the CG state. It is shown that the SRS also influences the ductility of UFG-metals in tensile tests.

Effect of Small Addition of Si on Superplastic Elongation at Room Temperature in Zn-Al Eutectoid Superplastic Alloy

2014 ◽  
Vol 922 ◽  
pp. 328-331 ◽  
Author(s):  
Yuhei Kamiya ◽  
Masaki Ninomiya ◽  
Tokuteru Uesugi ◽  
Yorinobu Takigawa ◽  
Kenji Higashi
Keyword(s):  
Grain Size ◽  
Strain Rate ◽  
Room Temperature ◽  
Tensile Tests ◽  
Al Alloy ◽  
Superplastic Behavior ◽  
Superplastic Alloy ◽  
Average Grain Size ◽  
Before And After ◽  
Si Content

Recent experimental data have revealed that a small amount of impurity can significantly influence the superplastic behavior in Zn-Al eutectoid superplastic alloy. However, the effect of Si content on the superplastic behavior in Zn-Al alloy has not been reported. In this study, the superplastic behavior at a room temperature of two grades of the Zn-Al eutectoid superplastic alloy was studied under identical conditions of grain size, temperature, and strain rate. These two grades were prepared from high-purity Zn, Al and Al-Si alloy using the same procedure but different Si impurity levels; Zn-Al-10Si and Zn-Al-1000Si contain 10 and 900 wt. ppm of Si, respectively. As a result of annealing treatments, an average grain size of 0.6 μm in both grades. To investigate the effects of Si content on superplastic properties, the tensile tests were performed at a room temperature of 298 K and a constant strain rate of 1×10-3 s-1. Microstructures before and after the tensile tests was observed using a scanning electron microscope. The experimental results show that the elongations decreased with increasing the Si content. In contrast, the flow stress of Zn-Al alloys was not affected by the Si content. On the microstructure observation of the two grades of the Zn-Al alloy before and after the tensile tests, cavities existed at grain boundaries and strain enhanced grain growth was observed.

Superplastic Deformation Behavior of As-Received and Hydrogenated Ti2AlNb Alloy

2018 ◽  
Vol 385 ◽  
pp. 109-113
Author(s):  
Xi Feng Li ◽  
Guo Peng Jia ◽  
Xu Dong Cao ◽  
Jun Chen ◽  
Guo Hong Wu
Keyword(s):  
Strain Rate ◽  
Superplastic Deformation ◽  
Initial Strain Rate ◽  
Tensile Tests ◽  
Strain Rate Range ◽  
Initial Strain ◽  
Uniaxial Tensile ◽  
Hydrogen Addition ◽  
Effects Of Temperature ◽  
Superplastic Properties

In this paper, the effects of temperature and initial strain rate on the superplasticity of as-received Ti2AlNb alloy were studied by uniaxial tensile tests. Temperature from 870°C to 1030°C with an interval of 40°C and initial strain rate range of 10-2s-1to 10-4s-1were selected. The optimal superplasticity of 190.3% was obtained at 990°C with initial strain rate of 10-3s-1. The superplastic properties were deteriorated at 1030°C due to serious grain coarsening. In order to improve superplastic properties, the as-received alloy was hydrogenated with different hydrogen contents. It was found that hydrogen addition can significantly decrease flow stress and increase elongation. A higher elongation occurs at 910°C in hydrogenated alloy.

Grain boundary strengthening in copper/niobium multilayered foils and fine-grained niobium

2008 ◽  
Vol 23 (2) ◽  
pp. 376-382 ◽  
Author(s):  
A.C. Lewis ◽  
C. Eberl ◽  
K.J. Hemker ◽  
T.P. Weihs
Keyword(s):  
Grain Boundary ◽  
Strain Rate ◽  
Room Temperature ◽  
Tensile Tests ◽  
Dislocation Creep ◽  
Uniaxial Tensile ◽  
Significant Drop ◽  
Dislocation Glide ◽  
Fine Grained ◽  
Grain Boundary Strengthening

Uniaxial tensile tests were performed on Cu/Nb multilayered foils to investigate yield strength and grain boundary strengthening in the layered foils at room temperature and in fine-grained Nb at 600 °C. At room temperature, yielding in Cu/Nb multilayered foils is controlled by deformation in both layers, and grain boundary strengthening is observed with a Hall–Petch slope (kRT) of 198 ± 56 MPa·μm1/2 at a strain rate of 10−4 s−1. At 600 °C, yielding in Cu/Nb multilayered foils is controlled by deformation in just the Nb layers. Hall–Petch strengthening is observed over a range of strain rates, but the Hall–Petch slope decreases from 197 ± 71 MPa·μm1/2 for a strain rate of 10−4 s−1 to only 25 ± 40 MPa·μm1/2 for a strain rate of 10−6 s−1. The significant drop in the Hall–Petch slope for Nb with decreasing strain rate indicates a change in the controlling deformation mechanism from dislocation glide to dislocation creep.

Superplastic Behavior of a Cu-Cr-Zr Alloy Subjected to ECAP

2016 ◽  
Vol 838-839 ◽  
pp. 404-409
Author(s):  
Roman Mishnev ◽  
Iaroslava Shakhova ◽  
Andrey Belyakov ◽  
Rustam Kaibyshev
Keyword(s):  
Grain Size ◽  
Dislocation Density ◽  
Strain Rate ◽  
Temperature Interval ◽  
Rate Sensitivity ◽  
Tensile Tests ◽  
Superplastic Behavior ◽  
Average Grain Size ◽  
Gauge Section ◽  
Zr Alloy

A Cu-0.87%Cr-0.06%Zr alloy was subjected to equal channel angular pressing (ECAP) at a temperature of 400 °C up to a total strain of ~ 12. This processing produced ultra-fine grained (UFG) structure with an average grain size of 0.6 μm and an average dislocation density of ~4×1014 m-2. Tensile tests were carried out in the temperature interval 450 – 650 °C at strain rates ranging from 2.8´10-4 to 0.55 s-1. The alloy exhibits superplastic behavior in the temperature interval 550 – 600 °C at strain rate over 5.5´10-3 s-1. The highest elongation-to-failure of ~300% was obtained at a temperature of 575 °C and a strain rate of 2.8´10-3 s-1 with the corresponding strain rate sensitivity of 0.32. It was shown the superplastic flow at the optimum conditions leads to limited grain growth in the gauge section. The grain size increases from 0.6 μm to 0.87 μm after testing, while dislocation density decreases insignificantly to ~1014 m-2.

scholarly journals Influence of strain rate and heat treatments on tensile and creep properties of Zn-0.15Cu-0.07Ti alloys

DYNA ◽  
2016 ◽  
Vol 83 (195) ◽  
pp. 77-83 ◽  
Author(s):  
María José Quintana Hernández ◽  
José Ovidio García ◽  
Roberto González Ojeda ◽  
José Ignacio Verdeja
Keyword(s):  
Strain Rate ◽  
Room Temperature ◽  
Rolling Direction ◽  
Tensile Tests ◽  
Strain Rates ◽  
Creep Tests ◽  
Design Problems ◽  
Creep Properties ◽  
Heat Treated ◽  
Zn Alloys

The use of Cu and Ti in Zn alloys improves mechanical properties as solid solution and dispersoid particles (grain refiners) may harden the material and reduce creep deformation. This is one of the main design problems for parts made with Zn alloys, even at room temperature. In this work the mechanical behavior of a Zn-Cu-Ti low alloy is presented using tensile tests at different strain rates, as well as creep tests at different loads to obtain the value of the strain rate coefficient m in samples parallel and perpendicular to the rolling direction of the Zn strip. The microstructure of the alloy in its raw state, as well as heat treated at 250°C, is also analyzed, as the banded structure produced by rolling influences the strengthening mechanisms that can be achieved through the treatment parameters.

scholarly journals Experimental investigations of the human oesophagus: anisotropic properties of the muscular layer in large deformation

2021 ◽  
Author(s):  
Ciara Durcan ◽  
Mokarram Hossain ◽  
Gregory Chagnon ◽  
Djordje Peric ◽  
Lara Bsiesy ◽  
...  
Keyword(s):  
Strain Rate ◽  
Ex Vivo ◽  
Longitudinal Direction ◽  
Tensile Tests ◽  
Endoscopic Biopsy ◽  
Circumferential Direction ◽  
Experimental Investigations ◽  
Uniaxial Tensile ◽  
Rate Dependency ◽  
Muscular Layer

Technological advancements in the field of robotics have led to endoscopic biopsy devices able to extract diseased tissue from between the layers of the gastrointestinal tract. Despite this, the layer-dependent properties of these tissues have yet to be mechanically characterised using human tissue. In this study, the ex vivo mechanical properties of the passive muscularis propia layer of the human oesophagus were extensively investigated. For this, a series of uniaxial tensile tests were conducted. The results displayed hyperelastic behaviour, while the differences between loading the tissue in both the longitudinal and circumferential directions showcased its anisotropy. The anisotropy of the muscular layer was present at different strain rates, with the longitudinal direction being consistently stiffer than the circumferential one. The circumferential direction was found to have little strain-rate dependency, while the longitudinal direction results suggest pronounced strain-rate-dependent behaviour. The repeated trials showed larger variation in terms of stress for a given strain in the longitudinal direction compared to the circumferential direction. The possible causes of variation between trials are discussed, and the experimental findings are linked to the histological analysis which was carried out via various staining methods. Finally, the direction-dependent experimental data was simulated using an anisotropic, hyperelastic model.

Experimental and Numerical Investigations on Hot Deformation Behavior and Processing Maps for ASS 304 and ASS 316

2018 ◽  
Vol 37 (9-10) ◽  
pp. 873-888 ◽  
Author(s):  
Nitin Kotkunde ◽  
Hansoge Nitin Krishnamurthy ◽  
Swadesh Kumar Singh ◽  
Gangadhar Jella
Keyword(s):  
Experimental Data ◽  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Constitutive Models ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Processing Maps ◽  
Hot Deformation Behavior ◽  
Statistical Measures

AbstractA thorough understanding of hot deformation behavior plays a vital role in determining process parameters of hot working processes. Firstly, uniaxial tensile tests have been performed in the temperature ranges of 150 °C–600 °C and strain rate ranges of 0.0001–0.01s−1 for analyzing the deformation behavior of ASS 304 and ASS 316. The phenomenological-based constitutive models namely modified Fields–Backofen (m-FB) and Khan–Huang–Liang (KHL) have been developed. The prediction capability of these models has been verified with experimental data using various statistical measures. Analysis of statistical measures revealed KHL model has good agreement with experimental flow stress data. Through the flow stresses behavior, the processing maps are established and analyzed according to the dynamic materials model (DMM). In the processing map, the variation of the efficiency of the power dissipation is plotted as a function of temperature and strain rate. The processing maps results have been validated with experimental data.

Tensile Properties at High and Low Temperatures and at Room Temperature after High-Temperature Exposure

2004 ◽  
pp. 211-242
Keyword(s):  
High Temperatures ◽  
Room Temperature ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Data Set ◽  
Casting Alloys ◽  
Subzero Temperatures ◽  
Wide Range ◽  
Temperature Exposure ◽  
High And Low Temperatures

Abstract This data set contains the results of uniaxial tensile tests of a wide range of aluminum casting alloys conducted at high temperatures from 100 to 370 deg C, subzero temperatures from -269 to -28 deg C, and room temperature after holding at high temperatures from 100 to 370 deg C. In most cases, tests were made of several lots of material of each alloy and temper. The results for the several lots were then analyzed together graphically and statistically, and the averages were normalized to the room-temperature typical values. For some alloys, "representative" values (raw data) rather than typical values are provided.

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